• Title/Summary/Keyword: low temperature firing

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A Study on Characteristics of Temperature Independent Propellant Using Di-nitro-diaza-alkane Series Energetic Plasticizers(I) (Di-nitro-diaza-alkane 계열 에너지 가소제를 활용한 온도 둔감 추진제 특성 연구(I))

  • Joo, Hyun-Hye;Joo, Hyung-Uk;Kwon, Tae-Soo;Kwon, Sun-Kil
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2011.11a
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    • pp.698-701
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    • 2011
  • Over recent several years, researches for the less sensitive gun propellant development have been carried out with promising the product of propellants which have temperature independent characteristics using the new energetic plasticizing mixture as Di-nitro-diaza-alkanes. During this study, the promising propellant formulation having temperature ballistic properties as well as better behaviors concerning the cold brittleness of the materials was confirmed by results in tests of a closed bomb and 40mm Gun firing. On-going research on the optimized shape, formulation and processes of the propellant is progressing. From now on it should be done present study to establish the better composition and processes.

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A Study on the Ignition Characteristics of Liquid Rocket Engine Thrust Chamber with Regenerative Cooling (액체로켓엔진 재생냉각 연소기의 점화 특성 연구)

  • Lee, Kwang-Jin;Han, Yeoung-Min;Kim, Jong-Gyu;Choi, Hwan-Seok
    • Journal of the Korean Society of Propulsion Engineers
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    • v.16 no.6
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    • pp.73-78
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    • 2012
  • The ignition characteristics of liquid rocket engine thrust chambers which have been developed by domestic technology were analyzed through hot-firing tests. Thrust chambers used in hot-firing tests have different characteristics in terms of the injector for ignition, film cooling method and the position of the oxidizer inlet. Also, these thrust chambers used their respective startup sequences. Analysis results showed that according to temperature profiles of the oxidizer manifold, low frequency fluctuation was appeared in ignition area. This low frequency fluctuation didn't give rise to violent malfunction of the thrust chamber, but the continuous observation as a concern parameter in the side of interfaces with engine system and launch vehicle should be demanded.

Fabrication of Anode-Supported SOFC Single Cells via Tape-Casting of Thin Tapes and Co-Firing (박막 테이프캐스팅과 동시소성에 의한 연료극 지지형 SOFC 단전지 제조)

  • Moon, Hwan;Kim, Sun-Dong;Hyun, Sang-Hoon;Kim, Ho-Sung
    • Journal of the Korean Ceramic Society
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    • v.43 no.12 s.295
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    • pp.788-797
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    • 2006
  • An anode-supported SOFC single cell having $5{\mu}m$ thin electrolyte was fabricated cost-effectively by tape casting, laminating, and co-filing of anode (NiO-YSZ), cathode (LSM-YSZ), and electrolyte (YSZ) components. The optimal slurry compositions of the green tapes for SOFC components were determined by an analysis of the mean diameter, the slurry viscosity, the tensile strength/strain of the green tapes, and their green microstructures. The single cells with a dense electrolyte and porous electrodes could be co-fired successfully at $1325\sim1350^{\circ}C$ by controlling the contents of pore former and the ratio of coarse YSZ and fine YSZ in the anode and the cathode. The single cell co-fired at $1350^{\circ}C$ showed $100.2mWcm^{-2}$ of maximum power density at $800^{\circ}C$ but it was impossible to apply it to operate at low temperature because of low performance and high ASR, which were attributed to formation of the secondary phases in the cathode and the interface between the electrolyte and the cathode.

Warpage of Co-fired High K/Low K LTCC Substrate (고유전율/저유전율 LTCC 동시소성 기판의 휨 현상)

  • Cho, Hyun-Min;Kim, Hyeong-Joon;Lee, Chung-Seok;Bang, Kyu-Seok;Kang, Nam-Kee
    • Journal of the Microelectronics and Packaging Society
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    • v.11 no.3 s.32
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    • pp.77-82
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    • 2004
  • In this paper, warpages of heterogeneous LTCC substrates comprised of high K/low K hi-layered structure were investigated. The effect of glass content in high K LTCC layer on the warpage of substrate during co-firing process was examined. Shrinkage and dielectric properties of high K and low K green sheets were measured. In-situ camber observation by hot stage microscopy showed different camber development of heterogeneous LTCC substrates according to glass content in high K green sheet. High K green sheet containing $50\%$ glass was matched to low K green sheet in the shrinkage. Therefore, LTCC substrate of Low K/High K+$50\%$ glass structure showed flat surface after sintering.

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Effect of the shape of the micro punching on the stacked antennas characteristics (미세 펀칭 형상이 적층형 안테나 특성에 미치는 영향)

  • Hong, J.P.;Han, J.N.;Chung, H.W.;Yoon, S.M.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.71-74
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    • 2007
  • Substitution of the stacked antenna for the normally pressed antenna in the mobile phone was tried for the purpose of decreasing its size. However, reduced size resulted in the difficulties obtaining the targeted characteristics with the bandwidth over 70MHz. The cross-section of the vias in the low temperature co-firing ceramics process was studied to find out effects on the bandwidth characteristics. Circular and rectangular cross-section of the via beneath different types of antenna patterns were simulated. Better bandwidth characteristics were acquired for the larger diameter of the circular section and for the rectangular section as the cross-section area increased. From the viewpoint of the shape of the cross-section, rectangular area showed better characteristics than the circular area with the same longest length in the cross-section.

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유전체 재료를 활용한 이동통신 필터 기술

  • 김준철;방규석;이형규
    • The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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    • v.12 no.3
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    • pp.25-34
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    • 2001
  • There are many kinds of dielectric materials in microwave dielectric filters for mobile telecomunication. But It is need to new dielectric materials for IMT200O, Bluetooth, wireless LAN to miniaturize the dielectric filters. These kinds of materials should have high dielectric constants, high Q, and low firing sintering temperature(<900˚C ). Multilayer monolithic dielectric filters are manufactured by BiNb04, dielectric ceramics cofired at 875˚C .

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A Study on the Fast-firing Body with Natural Wollastoitne (천연 규회석을 이용한 신속소성소지 구성에 관한 연구)

  • 안영필;최의석;김복희
    • Journal of the Korean Ceramic Society
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    • v.19 no.2
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    • pp.101-108
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    • 1982
  • As raw materials wollastonite, kaolin and pyrophyllite were used to synthesize mullite, anorthite and pseudowoll-astonite which were known as low thermal expansion substance. Increasing the amount of wollastonite in the composition resulted in a linear thermal expansion behavior. However, the increases of pyrophyllite indicated the relatively unstable themmal expansion behavior, because the phase transition occured in quartz of the pyrophyllite compositon. To lowering sintering temperature feldspar (Kebook and Anyang) were added in the composition that showed the linear thermal expantion behavior, and over 50'C were lowered.

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Phase Transition and Thermal Expansion Behavior of Zirconia Setter Fabricated from Fused CaO Stabilized Zirconia

  • Park, Ji-Hoon;Bang, Il-Hwan;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.56 no.2
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    • pp.184-190
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    • 2019
  • To improve resistance in thermal shock of zirconia setter which is frequently and repeatedly exposed to high temperature, high degree of porosity and control of thermal expansion are needed for which the fused CSZ (CaO stabilized zirconia) is used to produce the zirconia setter. In the present study, the effects of sintering temperature, cool down condition, addition of CaO stabilizer, and addition of other additives on phase transition and thermal expansion behavior of the fabrication process of zirconia setter, were examined. The zirconia setter, fabricated with fused CSZ at 1550℃, exhibited 20.4 MPa of flexural strength, 6.8% of absorbance, and 27.9% of apparent porosity. The rapid change in thermal expansion of zirconia setter is observed at temperature around 800℃, and it was reduced by low firing temperature, slowed cooled down, and addition of CaO.

Preparation of Lead-free Silver Paste with Nanoparticles for Electrode (나노입자를 첨가한 전극용 무연 silver 페이스트의 제조)

  • Park, Sung Hyun;Park, Keun Ju;Jang, Woo Yang;Lee, Jong Kook
    • Journal of the Korean Society for Heat Treatment
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    • v.19 no.4
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    • pp.219-224
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    • 2006
  • Silver paste with low sintered temperature has been developed in order to apply electronic parts, such as bus electrode, address electrode in PDP (Plasma Display Panel) with large screen area. In this study, nano-sized silver particles with 10-30 nm were synthesized from silver nitrate ($AgNO_3$) solution by chemical reduction method and silver paste with low sintered temperature was prepared by mixing silver nanoparticles, conventional silver powder with the particle size 1.6 um and Pb-free frit. Conductive thick film from silver paste was fabricated by screen printing on alumina substrate. After firing at $540^{\circ}C$, the cross section and surface morphology of the thick films were analyzed by FE-SEM. Also, the sheet resistivity of the fired thick films was measured using the four-point technique.

Low Temperature Sintering Mg-Zn Ferrites (Mg-Zn Ferrites의 저온소결화)

  • Kwon Oh-Heung
    • Resources Recycling
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    • v.12 no.6
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    • pp.8-12
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    • 2003
  • According to the recent trend to raise the horizontal scan frequency to increase the image refinement of the High Definition TV and High Resolution Display, material with low core loss is required for the ferrite core for deflection yoke, which is secured even in the high frequency range. liking notice of the influence on the fine structure of Mg-Zn ferrite by the chemical com position and process, low temperature sintering was proceeded. Cu was added to the low loss Mg-Zn system ferrite. After select-ing MgO, ZnO, $Fe_2$$O_3$, CuO, MgO was substituted for CuO while varying the composition ratio. Then the sample was sintered for 3 hours between $980~1350^{\circ}C$ Magnetic permeability, power consumption, shrinkage rate, core loss were measured. The start-ing temperature to test the shrinkage of the sample was nearby $900^{\circ}C$, it increased according to the substitution process of Cu, and the firing temperature was lowered about $-50~-75^{\circ}C$ alongside of the process.