• Title/Summary/Keyword: low temperature firing

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Development of 100N class $H_{2}O_2$ Mono-propellant Rocket Engine (100N급 $H_{2}O_2$ 단일 추진제 로켓 엔진의 개발)

  • Lee Su-Lim;Park Joo-Hyuk;Lee Choog-Won
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • v.y2005m4
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    • pp.159-167
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    • 2005
  • Considering the increase of interest in $H_{2}O_2$ as a rocket propellant, a test facility and a rocket engine have been developed to research in areas of $H_{2}O_2$ mono-propellant propulsion. A detailed design-study of a $H_{2}O_2$ mono-propellant rocket engine of 100-N thrust is presented. Several firings attempted in early stage had some problems with misfire and chamber pressure decrease. Low environmental temperature and impurities included in hydrogen peroxide were considered to be the reasons. Addressing these points resulted in successful firing of the rocket engine and obtained thrust about $100\sim107-N.$

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The Oxidation and Sintering of $Al-Al_2O_3$ Powder Mixture by using Microwave (Hybrid) Heating (마이크로파 혼합 가열에 의한 $Al-Al_2O_3$ 분말성형체의 산화와 소결)

  • 박정현;안주삼
    • Journal of the Korean Ceramic Society
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    • v.32 no.3
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    • pp.331-340
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    • 1995
  • Microwave (Hybrid) Heating (MHH) was used to oxidize and sinter Al-Al2O3 powder mixture. For 25 v/o Al specimen and 35 v/o Al specimen, the total processing to produce low-shrinkage reaction bonded alumina was carried out within 1 hour even though conventional furnace process took more than 10 hours. Compared with conventional fast firing process, MHH process increased more than 40% oxidation at the same temperature, and these high oxidation rates were thought to be caused by the surface ohmic current on Al particles.

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A Basic Research for Development of $H_2O_2$ Mono-propellant Rocket Engine ($H_2O_2$ 단일 추진제 로켓 엔진 개발에 대한 기초연구)

  • Lee Su-Lim;Park Joo-Hyuk;Lee Choog-Won
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2006.05a
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    • pp.110-117
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    • 2006
  • Considering the increase of interest in $H_2O_2$ as a rocket propellant, a test facility and a rocket engine have been developed to research in areas of $H_2O_2$ mono-propellant propulsion. A detailed design-study of a $H_2O_2$ mono-propellant rocket engine of 100-N thrust is presented. Several firings attempted in early stage had some problems with misfire and chamber pressure decrease. Low environmental temperature and impurities included in hydrogen peroxide were considered to be the reasons. Addressing these points resulted in successful firing of the rocket engine and obtained thrust about $100\sim107-N$.

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Low temperature firing and electrical properties of PZT ceramics prepared from partial oxalate method derived powders (부분수산법에 의한 PZT 세라믹스의 저온소성과 전기적 제특성)

  • 남효덕;이희영
    • Electrical & Electronic Materials
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    • v.6 no.2
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    • pp.168-174
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    • 1993
  • 두가지 부분수산법, 즉 부분수산법(1)과 수정된 부분수산법에 의해 합성한 미분말을 사용하여 PZT 세라믹스를 저온소성하고 그 전기적 제특성을 조사하였다. 두가지 부분수산법에 의해 합성한 분말의 소결거동을 조사해본 결과 고상반응법보다 훨씬 낮은 소결온도인 950.deg.C에서도 단일상의 페로브스카이트상이 얻어지고 치밀화가 이루어졌을 뿐만 아니라 비유전율, 전기기계 결합계수, 압전정수 등 유전 및 압전특성이 고상반응법에 비해 손색이 없었다. 특히 두가지의 부분수산법에 의해 얻어진 PZT 세라믹스는 물리적 전기적 제특성이 서로 비슷하게 나타났으며 이 결과로부터 부분수산법(1)에서 수반되는 ZTO 분말을 따로 합성하는 공정이 불필요한 수정된 부분수산법이 편리함을 알았다.

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The structure and properties of $50SnO_2-(50-x)P_2O_5-xB_2O_3$ for component materials of PDP

  • An, Yong-Tae;Choi, Byung-Hyun;Ji, Mi-Jung;Ko, Young-Soo;Kim, Hyung-Sun
    • 한국정보디스플레이학회:학술대회논문집
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    • 2008.10a
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    • pp.359-361
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    • 2008
  • Glasses in the $SnO_2-(50-x)P_2O_5-xB_2O_3$ system were examined as potential replacement for the PbO glass frits with low firing temperature for component materials of a plasma display panel. The glasses were evaluated for their structural and the thermal expansion coefficient, glass transition and glass softening temperatures and Vickers hardness as a function of the $B_2O_3$ content.

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Effect of $Al_{2}O_{3}$ filler addition on sintering behavior of low-firing $BaO-B_{2}O_{3}-ZnO$ glass ceramic system

  • Kim, Young-Nam;Kim, Byung-Sook;Lee, Joon-Hyung;Kim, Jeong-Joo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.814-817
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    • 2003
  • The sintering behavior of $BaO-B_{2}O_{3}-ZnO$, which is Pb-free glass-ceramic system, was examined as functions of the composition and the amount and particle size of $Al_{2}O_{3}$ filler. Different kinds of modifiers were added and $Al_{2}O_{3}$ fillers with different particle sizes ($1.5{\mu}m$ and $4.5{\mu}m$) were added. The glass frit-filler composites were sintered in the temperature range $520{\sim}580^{\circ}C$. X-ray diffraction results revealed that some of the composites crystallized during sintering. Dielectric constant and thermal expansion coefficient the glass-ceramics were analyzed.

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Preparation and properties of PbO free dielectric paste for PDP barrier rib (PDP 격벽용 무연 유전체 paste의 제조 및 특성)

  • Son, Myung-Mo;Lee, Heon-Soo;Lee, Sang-Geun;Park, Hee-Chan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.876-879
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    • 2003
  • The principal problems in development of dielectric paste materials for PDP(plasma display panel)are PbO free paste and low melting temperature. We prepared PbO free paste from glasses in the system $BaO-ZnO-B_2O_3-V_2O_5$. DTA, XRD and SEM were used to study and characterize $BaO-ZnO-B_2O_3-V_2O_5$ glasses. PbO free paste developed at this paper has thermal expansion of $74{\times}10^{-7}/^{\circ}C$, DTA transformation point of $460^{\circ}C$, and firing condition of $560^{\circ}C$, 10min.

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Design and fabrication of multilayer LTCC BPF using DGS structure (DGS 구조를 이용한 적층 LTCC 대역통과 필터의 설계 및 제작)

  • Cho, Y.K.;Kim, H.S.;Song, H.S.;Park, K.H.
    • Proceedings of the Korea Electromagnetic Engineering Society Conference
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    • 2003.11a
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    • pp.333-337
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    • 2003
  • In this paper, 5.2 GHz WLAN BPF(Band Pass Filter) using LTCC(Low temperature co-firing ceramic) Multilayer technology was simulated and manufactured. A DGS(Defected Ground structure) resonator with spiral ground pattern is used to shorten resonator size and improve circuit Q factor. And the equivalent circuit of BPF was suggested. The measured result shows good agreement with simulated data. Experimental results show the center frequency of 5.25GHz, the insertion loss of 0.14dB, and the 3-dB bandwidth of 350MHz (6%). The center frequency of BPF is 5.25GHz which is available for wireless LAN.

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A study on the Passivation film by Electrophoretic method using Borosilicate glasses (전기영동법을 이용한 붕규산계 유리의 Passivation막 연구)

  • Huh, Chang-Su;Park, In-Bae
    • Proceedings of the KIEE Conference
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    • 1996.07c
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    • pp.1642-1644
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    • 1996
  • Passivation must prevent ionic charge movement on the surface of the junction, thereby minimizing the junction leakage and maximizing the breakdown voltage of the devices. Borosilicate glasses are widely used as surface passivants for such silicon power devices as thyristors, transistor, and diodes. Since these 91asses are electrically stable at high temperatures and in high electric fields, they can readily be applied as a thick film, and they are resistant to humidity and have low ionic mobility. A deposition technique of glass film on the silicon surface by electrophoresis in which acetone is used as a suspension medium has been investigated. The purpose of this paper is to describe electrophoretic deposition method for glass passivation and characteristics of glass films which were compared using DTA, SEM, XRD, as a function of firing temperature.

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Thermal Property of Phosphate Glasses for Low Firing Temperature in PDP

  • Park, Jun-Hyun;Jung, Byung-Hae;Kim, Hyung-Sun
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.795-798
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    • 2002
  • Replacing Pb-free glass composition for the dielectric materials is expected in PDP industry. In this study, phosphate glasses, $P_2O_5$- ZnO- SnO (PZS), $P_2O_5$-ZnO-BaO (PZB) were selected for a new transparent dielectric. Thermal properties (Tg, CTE) were measured with differential thermal analyzer and thermal mechanical analyzer. The glass transition of the glasses was ranged at $365{\sim}405^{\circ}C$ for the PZS system and $5.9{\sim}9.5{\times}\;10^{-6}$ of thermal expansion were found. The PZB system showed $445{\sim}470^{\circ}C$ of glass transition. Thus, the glass compositions would be a potential candidate for a transparent dielectric layer in plasma display panel.

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