• Title/Summary/Keyword: linear correlation coefficient

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Development of Analytical Method for Sodium Alginate in Foods (식품 중 알긴산나트륨의 분석법 개발)

  • Kim, Hee-Yun;Hong, Ki-Hyoung;Choi, Jang-Duck;Park, Sung-Kwan;Jung, Si-Sub;Choi, Woo-Jeong;Ahn, Yeong-Sun;Hong, Yeong-Pyo;Song, Ok-Ja;Moon, Dong-Chul;Lee, Shin-Ho;Shin, Il-Shik
    • Korean Journal of Food Science and Technology
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    • v.38 no.1
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    • pp.1-4
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    • 2006
  • Method of analyzing sodium alginate in foods was developed using high performance liquid chromatography (HPLC). HPLC conditions for sodium alginate were: column, MCI GEL $(8\;mm\;i.d{\times}300\;mm)$; mobile phase, deionized water; detector, refractive index detection (sensitivity = 16). Separation of sodium alginate was achieved within 15 min. Sodium alginate showed good linear relationship at 0.1-2.0% range. Correlation coefficient of calibration curve for sodium alginate exceeded 0.999, and detection limit was 0.005%. Recovery rate of sodium alginate in wheat flour dough was 106.67%. This method was successfully applied to analyses of cereals, saccharides, and ice cream, etc. Sodium alginate was detected in chocolate, noodles, and kelp at 0-44.8% range.

Determination of Chloramphenicol by Differential Pulse Polarography (미분 펄스 폴라로그래피에 의한 Chloramphenicol의 정량분석)

  • Younghee Hahn;Jung-Sun Jeon
    • Journal of the Korean Chemical Society
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    • v.36 no.4
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    • pp.552-557
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    • 1992
  • Chloramphenicol was studied by differential pulse polarography (DDP). A reduction peak which is dependent on pH of the solution appeared in the voltage range between zero and -1.50 volt vs. Ag/AgCl (sat. KCl) reference electrode. A plot of peak potentials (Ep) measured at room temperature (20$^{\circ}C$) vs. pH of the chloramphenicol solutions showed linear relationship changing slope (Ep/pH) at pH 8.9. The slope was -59.7 mV/pH in pH 2.7∼8.9 and -24.3 mV/pH in pH 8.9∼11.2, respectively. A log plot of peak currents (ip) vs. concentrations showed a linearity at the concentrations between 4.8 ${\times}$ 10$^{-7}$ M and 6.2 ${\times}$ 10$^{-5}$ M (0.16 ppm∼20 ppm) chloramphenicol in pH 8.0 ammonium buffer. Between the DPP method and the reference method measuring absorbance at 278 nm, the correlation coefficient was 0.996, which means an excellent linearity. The DPP method was able to detect degradation products of chloramphenicol in mild alkaline solution (pH = 8.0) more distinctly than the spectrophotometric method.

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The Effects of Road Geometry on the Injury Severity of Expressway Traffic Accident Depending on Weather Conditions (도로기하구조가 기상상태에 따라 고속도로 교통사고 심각도에 미치는 영향 분석)

  • Park, Su Jin;Kho, Seung-Young;Park, Ho-Chul
    • The Journal of The Korea Institute of Intelligent Transport Systems
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    • v.18 no.2
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    • pp.12-28
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    • 2019
  • Road geometry is one of the many factors that cause crashes, but the effect on traffic accident depends on weather conditions even under the same road geometry. This study identifies the variables affecting the crash severity by matching the highway accident data and weather data for 14 years from 2001 to 2014. A hierarchical ordered Logit model is used to reflect the effects of road geometry and weather condition interactions on crash severity, as well as the correlation between individual crashes in a region. Among the hierarchical models, we apply a random intercept model including interaction variables between road geometry and weather condition and a random coefficient model including regional weather characteristics as upper-level variables. As a result, it is confirmed that the effects of toll, ramp, downhill slope of 3% or more, and concrete barrier on the crash severity vary depending on weather conditions. It also shows that the combined effects of road geometry and weather conditions may not be linear depending on rainfall or snowfall levels. Finally, we suggest safety improvement measures based on the results of this study, which are expected to reduce the severity of traffic accidents in the future.

Utilization of Work-Family Balance Support Policy and Factors Associated with Retention Intention among Married Female Officers with Preschool Children (미취학 자녀를 둔 기혼 여군 장교의 일·가정 양립 지원제도 활용 정도와 재직의도 영향요인)

  • Kwon, Jo Eun;Kim, Gwang Suk;Park, Jeongok;Kim, Sue
    • Women's Health Nursing
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    • v.25 no.3
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    • pp.329-344
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    • 2019
  • Purpose: This study aimed to identify utilization of the work-family support policy (WFSP) and factors affecting retention intention among Korean female military officers. Methods: This cross-sectional survey recruited 103 married female officers from the Korean Army, Navy, and Air force with preschool-aged children through convenience and snowball sampling. Via online surveys from June to November, 2018, the participants self-reported retention intention, work-family conflict, job satisfaction, and utilization of the WFSP. The data were analyzed using descriptive statistics, independent t-tests, one-way analysis of variance, Pearson's correlation coefficient, and multiple linear regression. Results: Retention intention ($22.29{\pm}5.98$) was reported at the mid-level, lower than scores reported in the literature for female workers. Work-family conflict ($32.51{\pm}5.29$) and job satisfaction ($63.10{\pm}7.45$) were above the midpoint levels. Use of maternity leave (100.0%) and parental leave (92.2%) was high, especially compared to the rates of child-care day off (20.4%) and parenting time (20.4%). 'Noticeable increases in childcare services within the army' (22.8%) was reported as the supportive measure needed the most by female military officers. Job satisfaction (${\beta}=.43$, $p{\leq}.001$), the use of parenting time (${\beta}=-0.29$, p=.002), living type (${\beta}=-.18$, p=.043), and service type (${\beta}=-.16$, p=.035) significantly influenced retention intention. Conclusions: The findings highlight the priority areas of importance within the WFSP and suggest that a family-friendly culture can improve female officers' retention intention. Accordingly, policy changes at the Ministry of National Defense improving the system to enhance a family-friendly culture in the military is expected to strengthen the retention intention of female officers and contribute to excellence in the military workforce.

A Study on the Satisfaction with Life for the Elderly - Comparison Study of volunteer work group and economic activities group - (노년기 삶의 만족도에 관한 연구 - 자원봉사활동 집단과 경제활동집단의 비교를 중심으로 -)

  • Kwon, Mi Ae;Kim, Tae Hyun
    • 한국노년학
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    • v.28 no.4
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    • pp.1089-1111
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    • 2008
  • The purpose of this study was to research the effects of socio-demographic factors and values in each group on satisfaction with life by categorizing the activity types of the elderly into volunteer work and economic activities. The subjects of this study were 60 years an old higher. The questionnaires were categorized depending on activity types and collected. The voluntary work group consisted of 201 people (76 males, 36.8% and 125 females, 62.2%), The economic activity group consisted of 219 people (127 males, 58.0% and 92 females, 42.0%). The SPSS 14.0 Windows program was used to analyze data. Frequency, average, standard deviation, factor analysis, Pearson correlation coefficient, t-test, One-Way ANOVA analysis, and hierarchical multiple linear regression were analyzed. The major findings of this study indicate that the elderly in the voluntary work group have a high collectivism value, higher income earned by performing economic activities, and good cognitive health affected by a high satisfaction with life. From these research results, it was proved that a collectivism value is a common factor that affects satisfaction with life in both of the economic activity group. Those who were older had a traditional collectivism value. The voluntary work group showed a stronger collectivism value and higher satisfaction with life than the economic activity group. Thus, the diverse types of voluntary work should be developed and a systematic system should be established as methods for improving quality of life and satisfaction.

Estimation of Leaf Area Using Leaf Length, Leaf width, and Lamina Length in Tomato (엽장, 엽폭, 엽신장을 이용한 토마토의 엽면적 추정)

  • Lee, Jae Myun;Jeong, Jae Yeon;Choi, Hyo Gil
    • Journal of Bio-Environment Control
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    • v.31 no.4
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    • pp.325-331
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    • 2022
  • One of the most important factors in predicting tomato growth and yield is the leaf area. Estimating leaf area accurately is the beginning of an effective tomato plant growth assessment model. To this end, this study was conducted to identify the most effective model for estimating plant leaf area through the measurement of tomato plant leaves. Leaf area (LA), leaf length (L), leaf width (W), and lamina length (La) were measured for all leaves of 5 plants at two-week intervals. The correlation between LA and tomato-leaf-independent variables showed a strong positive relationship with the formulas La × W, L × W, La + W, and L + W. For LA estimation, a linear model using the formula LA = a + b (La2 + W2) gave the most accurate estimation (R2 = 0.867, RMSE = 88.76). After examining the positions of upper, middle, and lower leaves from September to December, the coefficient of determination (R2) values for each model were 0.878, 0.726, and 0.794 respectively. The most accurate estimation came from the model that used the upper leaves of the plants. The high accuracy of the upper-leaf-based model is judged by the 50% defoliation performed by farmers after October.

Changes in the Chlorophyll of Garlic Chives (Allium tuberosum) Resulting fromFertilizer and Drought Stress (비료와 가뭄 스트레스에 의한 부추의 엽록소 변화)

  • Huh, Man Kyu;Lee, Byeongryong
    • Journal of Life Science
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    • v.32 no.10
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    • pp.743-748
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    • 2022
  • The garlic chive (Allium tuberosum Rotter) is a prominent herb species in Asia and other nations of the world. Garlic chives is a favorite vegetable and used to garnish noodles in Korea. The effects of various doses of N, P, and K fertilizers and drought stress on the chlorophyll content in the leaves of garlic chives were investigated. The evaluations showed that chlorophyll a content was 0.386 at 10 mg/l N fertilizer and 0.584 at 50 mg/l N fertilizer. The treatment group showed a significant difference with regard to the contents of chlorophylls a and b and total chlorophyll at the 5% level (p<0.05). Pearson's correlation coefficient (Pearson's r) for chlorophylls a and b and total chlorophyll were 0.940, 0.966, and 0.971, respectively. The highest content of chlorophylls a and b and total chlorophyll in the leaves was recorded at 40 mg/l P fertilizer, while the values corresponding to 50 mg/l P fertilizer were lower than those for 40 mg/l P fertilizer. The content of total chlorophyll evaluated at 10 mg/l K fertilizer was 0.312 and that at 50 mg/l was 0.589. The simple linear regression showed the relationship between chlorophyll efficiency aand moisture. The slope factors of the dark-level fluorescence yield (Fo), the maximum fluorescence yield (Fm), the quenched state (Fv), and the maximal PSII quantum yield (Fv/Fm) for chlorophyll-efficient indicators were -0.931, 0.972, 972, and 0.950, respectively. NPK fertilizers and drought stress affected the chlorophyll content and efficiency of A. tuberosum.

Physicochemical Changes of Vinegars Obtained from Bamboo and Wood during Long Term Aging (장기간 숙성에 따른 죽초 및 목초액의 이화학적 변화)

  • Ku, Chang-Sub;Mun, Sung-Phil;Park, Sang-Bum;Kwon, Su-Duk
    • Journal of the Korean Wood Science and Technology
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    • v.30 no.4
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    • pp.74-79
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    • 2002
  • Three different kinds of the crude vinegars obtained from oak(Quercus serrata), bamboo(Phyllostachys pubescens) and pine(Pinus densiflora) species were stored for approximately one year and periodically analyzed to monitor their physicochemical changes. Small changes in physical properties, such as the pH, specific gravity and amount of organic acids as well as water-soluble tar were observed in the entire course of aging period. However, the color difference of the vinegars showed a remarkable change between 7 and 10 months. In addition, these vinegars' colors changed from light yellowish orange to much deeper purple and orange during this period. The amount of organic acids and neutral compounds(dihydro-2(3H)-furanone, furfural, furfuryl alcohol, 2-hydroxy-1-methyl-1-cyclopenten-3-one, 1-hydroxy-2-propanone and methanol) in the vinegars increased or decreased periodically every three months. A good linear relationship (correlation coefficient of ca. 0.92) was obtained between the amount of organic acids and the amount of neutral compounds in such changes. However, although the amount of phenols increased or decreased periodically, its amount was decreased over the entire aging.

Optimization of mix design of micro-concrete for shaking table test

  • Zhou, Ji;Gao, Xin;Liu, Chaofeng
    • Advances in concrete construction
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    • v.13 no.3
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    • pp.215-221
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    • 2022
  • Considering their similar mass densities, an attempt was made to optimize the mix design of micro-concrete that used barite sand as an aggregate by substituting marble powder (5%, 10%, 20%, 30%, 40%, 50%, 70%), clay brick powder (30%, 50%, 70%), and fly ash (30%, 50%, 70%) for the concrete (by mass) to form specimens for shaking table tests. The test results showed that for these three groups of materials, the substitutions had little effect on the density. The barite sand played a decisive role in the density, and the overall density of the specimens reached approximately 2.9 g/cm3. The compressive strength and elastic modulus decreased with an increase in the substitution rates for the three types of materials. Among them, the 28 day compressive strength values of the 40% and 50% marble powder groups were 11.73 MPa and 8.33 MPa, respectively, which were 58.7% and 70.7% lower than the control group, respectively. Their elastic modulus values were 1.33×104 MPa and 1.42×104 MPa, respectively, which were 39.1% and 35% lower than those of the control group, respectively. The 28 day compressive strength values of the 50% and 70% clay brick powder groups were 13.13 MPa and 5.8 MPa, respectively, which were 53.8% and 79.6% lower than the control group, respectively. Their elastic modulus values were 1.54×104 MPa and 1.19×104 MPa, respectively, which were 29.7% and 45.4% lower than those of the control group, respectively. The 28 day compressive strength values of the 50% and 70% fly ash groups were 13.5 MPa and 7.1 MPa, respectively, which were 52.5% and 75% lower than those of the control group, respectively. Their elastic modulus values were 1.36×104 MPa and 0.95×104 MPa, respectively, which were 37.9% and 56.6% lower than those of the control group, respectively. There was a linear relationship between the 28 day compressive strength and elastic modulus, with the correlation coefficient reaching a value higher than 0.88. The test results showed that the model materials met the high density, low compressive strength, and low elastic modulus requirements for shaking table tests, and the test data of the three groups of different alternative materials were compared and analyzed to provide references and assistance for relevant model testers.

Simultaneous GC/MS Analyses of Organic acids and Amino acids in Urine using TMS-TFA derivative (TMS-TFA 유도체화를 이용한 소변여지 중 유기산과 아미노산의 GC/MS 동시분석)

  • Yoon, Hye-Ran
    • Analytical Science and Technology
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    • v.19 no.1
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    • pp.107-114
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    • 2006
  • Early diagnosis and medical intervention are critical for the treatment of patients with metabolic disorders. A rapid analytical method was developed for simultaneous quantification of organic acids and amino acids in urine without labor-intensive pre-extraction procedure showing high sensitivity and specificity. A new method consisted of simple two-step trimethylsilyl (TMS)-trifluoroacetyl (TFA) derivatization using GC/MS-selective ion monitoring (SIM). Filter paper urine specimens were dried under nitrogen after being fortified with internal standard (tropate) in a mixture of distilled water and methanol. Methyl orange was added to the residue as indicator reagent. Silyl derivative of carboxylic functional group was followed by trifluoroacetyl derivative for amino functional group. N-methyl-N-(trimethylsilyl-trifluoroacetamide) and N-methyl-bistrifluoroacetamide were consecutively added and heated for 15-20 min at $65^{\circ}C-70^{\circ}C$, for TMS-TFA derivative, respectively. This reactant was analyzed by GC/MS-SIM. Linear dynamic range showed 0.001-50 mg with the detection limit of (S/N=3) 10-200 ng, and the quantification limit of 80-900 ng in urine. Correlation coefficient of regression line was 0.994-0.998. When the method was applied to the patients 'urine, it clearly differentiated the normal from the patient with metabolic disorder. The study showed that the developed method could be the method of choices in rapid and sensitive screening for organic aciduria and amino acidopathy.