• 분석과학
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• 제22권1호
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• pp.82-91
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• 2009

국내산 석회석을 이용하여 석회석 시료의 RRT 시험용 시료를 제조하여 XRF 및 습식 분석, ICP-OES를 이용한 기기 분석을 수행하였고 그 결과를 통계적 방법에 의하여 시료의 균질도를 평가하였다. 분석 결과 몇몇 시료의 경우 예상치 못했던 정규 분포로부터의 이상성이 발견되었으며 이상치를 제거한 후 측정한 모든 성분에 대하여 정규 분포 곡선에서 95% 신뢰 구간에서의 신뢰성 있는 표준 시료를 얻을 수 있었다.

• 한국안전학회지
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• 제34권5호
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• pp.111-118
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• 2019

Recently, a variety of special concrete structures have been designed in domestic and overseas construction markets and more advanced construction technology is required. Therefore, it is necessary to secure quantitative construction technology. For this purpose, it is essential to develop a standard reference material having a constant flow performance and quality to evaluate quantitative performance. On the other hand, the flowability of the concrete is greatly influenced by the flowability of the cement paste. Also, in consideration of design strength and workability, mix design is carried out at various mixing ratios according to the purpose of the site. Therefore, in this study, based on the derived components of standard reference materials for cement paste, we suggested mixing ratio of standard reference materials that can uniformly simulate the flow characteristics of cement paste according to W/C. As a result, it was found that the yield stress was determined by the ratio of water and glycerol but plastic viscosity was controled by limestone content. Finally, the ratio of standard reference materials to simulate the rheological range of cement paste by W/C was suggested.

• Advances in concrete construction
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• 제9권6호
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• pp.547-556
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• 2020

This study aimed to develop reference materials (RMs) that are chemically stable and can simulate the flow characteristics of cement paste. To this end, the candidate components of RMs were selected considering the currently required properties of RMs. Limestone, slag, silica, and kaolin were selected as substitutes for cement, while glycerol and corn syrup were selected as matrix fluids. Moreover, distilled water was used for mixing. To select the combinations of materials that meet all the required properties of RMs, flow characteristics were first analyzed. The results revealed that silica and kaolin exhibited bilateral nonlinearity. When an analysis was conducted over time, slag exhibited chemical reactions, including strength development. Moreover, fungi were observed in all mixtures with corn syrup. On the other hand, the combination of limestone, glycerol, and water exhibited a performance that met all the required properties of RMs. Thus, limestone, glycerol, and water were selected as the components of the RMs. When the influence of each component of the RMs on flow characteristics was analyzed, it was found that limestone affects the yield value, while the ratio of water and glycerol affects the plastic viscosity. Based on this, it was possible to select the mixing ratios for the RMs that can simulate the flow characteristics of cement paste under each mixing ratio. This relationship was established as an equation, which was verified under various mixing ratios. Finally, when the flow characteristics were analyzed under various temperature conditions, cement paste and the RMs exhibited similar tendencies in terms of flow characteristics. This indicated that the combinations of the selected materials could be used as RMs that can simulate the flow characteristics of cement paste with constant quality under various mixing ratio conditions and construction environment conditions.

• 화약ㆍ발파
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• 제36권2호
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• pp.1-9
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• 2018

폴리머 겔의 발파 효과를 평가하기 위해 AUTODYN을 이용한 단일 발파공 모델 시뮬레이션을 수행하였다. 발파공 내부 에멀젼 폭약과 공벽간의 채움재는 공기와 폴리머 겔을 적용하여 서로 결과를 비교하였으며, 디커플링 지수 1.0인 밀장전과 디커플링 지수 1.25, 1.56에 대해 각각 해석하였다. 폴리머 겔의 발파 효과 평가를 위한 기준은 밀장전 case를 기준으로 하였다. 해석 결과로서 석회석 모델의 파쇄 및 균열 발생에서 공기보다 폴리머 겔 적용의 경우가 높은 파쇄 정도를 나타냈고, 지정 게이지에서의 최고압력 또한 공기의 경우보다 폴리머 겔 적용이 높은 수치를 보였다.