• The Journal of the Korean dental association
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• v.58 no.5
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• pp.276-283
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• 2020

Objectives: The aim of this study was to evaluate the efficacy of CK files as an ultrasonic instrument, and to determine most efficient file size for smear layer removal. Materials and Methods: Thirty-six extracted human mandibular premolars with single, straight root canals and mature apices were mechanically prepared and randomly divided into three groups. Group 1 (Control) underwent conventional needle irrigation, Group 2 (CKS) underwent passive ultrasonic irrigation with a #20 CK file, and Group 3 (CKL) underwent passive ultrasonic irrigation with a #30 CK file. After preparation and irrigation, all teeth were dried and split with a chisel to obtain the mesial and distal half of their roots. Each sample was evaluated using a scanning electron microscope, and data were analyzed using the Kruskal-Wallis and Mann-Whitney rank sum tests (p<0.05). Results: The CKS group showed less debris in the apical third than the other groups (p<0.05). In this section, no significant difference was observed among the other groups. And, there was no significant difference among any groups for the middle third section. Conclusion: This study showed that PUI with #20 CK file removed more smear layer compared to using #30 CK file at the apical third of the root canal.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.44 no.4
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• pp.16-24
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• 2012

To characterize the coating structure, diverse methods such as mercury intrusion, nitrogen adsorption and oil absorption methods have been developed and widely employed. These indirect techniques, however, have some limitation to explain the actual coating structure. Recently microscopic observation methods have been tried for analyzing structural characteristics of coating layers. Preparation of the undamaged cross section of a coating layer is essential for obtaining high quality image for analysis. In this study, distortion-free cross-section of the coating layer was prepared using a grinding and polishing technique. The coated paper was embedded in epoxy resin and cured. After curing the resin block it was ground with abrasive papers and then polished with diamond particle suspension and nylon cloth. Polished coating layer was sufficient enough to obtain undamaged cross sectional images with scanning electron microscope under backscattered electron image mode. In addition, the SEM images allowed distinction of the coating layer components. Also S/B latex film formed between pigment particles was visualized by osmium tetroxide staining. Pore size distribution and pore orientation were evaluated by image analysis from SEM cross-sectional images.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.17 no.6
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• pp.144-150
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• 2018

In this study, the freezing process of L-shaped pipe exposed to the outside was investigated numerically by considering the mushy zone of freezing water. From the numerical results, it was found that the flow was outwardly directed due to the influence of the L-shaped bending part in the outside exposed part of the pipe, and the ice was formed in the shape of longitudinal corrugation on the wall surface of the pipe after the bending part. It is confirmed that this phenomenon is caused by the venturi effect due to the freezing as seen in connection with the velocity distribution in the pipe. It is found that the remelting phenomenon at the end of the freezing section occur simultaneously during the process of forming the ice in the pipe section. In regard of the factors affecting freezing, it was found that the thickness of the freezing layer is increased as the exposed pipe surface temperature is decreased, and the pipe surface temperature had a significant effect on the change of the freezing layer thickness. At the same time, it was found that the freezing layer becomes relatively thin when the water inflow rate is increased. This phenomenon was caused by reducing the exposure time of freezing water due to the vigorous flow convection of the water fluid.

• Korean Journal of Materials Research
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• v.14 no.1
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• pp.52-58
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• 2004

The surface property and formation behavior of a boride layer formed on Ni-Cr-Mo steel in a plasma paste boronizing treatment were investigated. The plasma paste boronizing treatment was carried out at 973～1273 K for 1-7 hrs under the gas ratio of Ar:H$_2$ (2:1). The thickness of the boride layer increased with increasing temperature and time in the boronizing treatment. The cross-section of the boride layer was a tooth structure and the hardness was Hv 2000～2500. XRD analysis revealed that the compound was identified as FeB, $Fe_2$B, and mixed phase of FeB/$Fe_2$B in the boride layer formed at 973～1073 K, 1173K, and 1273K, respectively. The Ni-Cr-Mo alloy boronized at 1173-1273 K showed the best excellent wear resistance against the sand. As a results of corrosion test in 1 M $H_2$$SO_4$ solution, $Fe_2$B formed on the matrix alloy exhibited higher corrosion resistance than FeB.

• Journal of Information Processing Systems
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• v.12 no.1
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• pp.73-82
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• 2016

In cognitive radio networks (CRNs), the performance of the transmission control protocol (TCP) at the secondary user (SU) severely drops due to the mistrigger of congestion control. A long disruption is caused by the transmission of primary user, leading to the mistrigger. In this paper, we propose a cross-layer approach, called a CR-aware scheme that enhances TCP performance at the SU. The scheme is a sender side addition to the standard TCP (i.e., TCP-NewReno), and utilizes an explicit cross-layer signal delivered from a physical (or link) layer and the signal gives an indication of detecting the primary transmission (i.e., transmission of the primary user). We evaluated our scheme by implementing it onto a software radio platform, the Universal Software Radio Peripheral (USRP), where many parts of lower layer operations (i.e., operations in a link or physical layer) run as user processes. In our implementation, we ran our CR-aware scheme over IEEE 802.15.4. Furthermore, for the purpose of comparison, we implemented a selective ACK-based local recovery scheme that helps TCP isolate congestive loss from a random loss in a wireless section.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.67 no.10
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• pp.1317-1321
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• 2018

PVDF as a semicrystal polymer, having a structure with C-F dipole moments, has been widely investigated because of its excellent chemical stability, mechanical strength, and ferroelectricity. In this study, ferroelectic ${\beta}$ type - PVDF layer was prepared by using an electrostatic spray deposition method and the effects of the addition of Ni-nitrate in precursor solution on the properties of PVDF layer were evaluated. Crystallinity and chemical structure of the PVDF layer were analyzed by a X-ray diffraction and Fourier Transform Infrared Spectrophotometer. Surface structure and fractured cross section of the layer were examined by a field emission-scanning electron microscope. LCR meter was used to obtain the dielectric properties of the layer. As the addition of an inorganic metal salt in PVDF sol, ${\beta}$ type - PVDF crystals were appeared in the hydrated metal salts doped-layer since the strong hydrogen bondings $(O-H{\cdots}F-C)_n$ due to high polarity of OH- were formed.

• Journal of Korean Association for Spatial Structures
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• v.16 no.4
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• pp.45-52
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• 2016

The single layer latticed domes have attracted many designers and researchers's attention all of the world, because these structures as spatial structure are of great advantage in not only mechanical rationality but also function, fabrication, construction and economic aspect. But single layer latticed domes are apt to occur the unstable phenomena that are called "buckling" because of the lack of strength of members, instability of structural shape, etc. In the case of latticed dome, there are several types of buckling mode such as overall buckling, local buckling, and member buckling according to the shape of dome, section type of member, the size of member, junction's condition of member and so on. There are many methods to increase the buckling strength of the single layer latticed dome, that is, with the change of geometrical shape of dome, the reinforcement of buckled member, etc. Therefore, the purpose of this study is to verify the reinforcement effect of buckled member when designers reinforce the buckled member to increase the buckling strength of single layer latticed dome with 3-way grid.

• Electrical & Electronic Materials
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• v.10 no.7
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• pp.645-650
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• 1997

We manufactured CoNbZr/Cu/CoNbZr multi-layer films by rf magnetron sputtering methods and formed the patterns on the deposited multi-layer films. In this study, we fabricated a new etchant for forming the patterns by the wet etching with etchant and we searched for the best etching conditions and the etchant composition. Cu was etched selectively independent on the concentration of iron chloride solution, but amorphous CoNbZr thin film did not. The etchant was achieved by iron chloride solution(17.5 mol%) mixed with HF (20 mol%) during 150 sec, which etched CoNbZr/Cu/CoNbZr multi-layer films at the same time. Also, the etchant etched CoNbZr/Cu/CoNbZr multi-layer films by the three-step. It was shown that the cross-section had the isotropic structure and excellent etching characteristics with the above etchant.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2008.11a
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• pp.15-16
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• 2008

In case manufacturing COF, through hole should be made to be used for a pathway connecting the conductive layers of its both faces. In case Cu-plating inside of through hole with electroless plating way, contact between Cu and PI film gets bad to be fell apart from PI by the impact of applying to the electric devices. Therefore, after sputtering is applying on inner through hole, then a method to perform electroplating process. In this study, after changing sputtering condition to manufacture FCCL, we looked the changeability of the upper PI and inner hole Cu layers. Making use of RF Magnetron sputtering equipment, we coated Cu thin film and Cu-plated on it through electroplating. After cold-mounting the completed FCCL, we examined hole section through an optical microscope. From the result of test, with parameters deposition pressure and deposition time, both the thickness of the hole plated layer and PI plated upper layer increased at regular rate, increasing the thickness of Cu sputter layer. However, from the result of test in increasing RF-power, we could know the increment rate of hole plated layer is considerably greater than that of PI plated upper layer. Therefore, we finally acquired good result; if you want only to increase the plated layer of inner hole, it's much better to increase RF-power.

• Journal of Conservation Science
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• v.35 no.1
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• pp.33-40
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• 2019

During the conservation and maintenance of the birthplace center yard of President Asan Yoon Bosun, four porcelain enamel dishware were excavated from the central yard well. The glaze layer of excavated enamel was severely damaged; hence, the conservation process was done rapidly. In addition, scientific investigation and analysis were conducted to confirm the material properties of the glaze layer. It was confirmed that the outer surface was inverted and dried, while the inner surface was upright and fired during the glazing and drying process by measuring the film thickness. By examining the breakup phenomenon, the breaking up of the white enamel on the colored enamel was confirmed. This indicates that the colored glaze rose to the surface depending on the density of the colored glaze and white glaze. The investigation of the cross-section of the film confirmed that the lower layer formed according to the bonding properties with metal during the glazing process. Analysis of the constituents of the identified lower layer confirmed that there are differences between the specific components of the metal oxide of the lower layer and the surface color development of the upper layer.