• 제목/요약/키워드: large area synthesis

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ACOUSTIC FEATURES DIFFERENTIATING KOREAN MEDIAL LAX AND TENSE STOPS

  • Shin, Ji-Hye
    • 대한음성학회:학술대회논문집
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    • 대한음성학회 1996년도 10월 학술대회지
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    • pp.53-69
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    • 1996
  • Much research has been done on the rues differentiating the three Korean stops in word initial position. This paper focuses on a more neglected area: the acoustic cues differentiating the medial tense and lax unaspirated stops. Eight adult Korean native speakers, four males and four females, pronounced sixteen minimal pairs containing the two series of medial stops with different preceding vowel qualities. The average duration of vowels before lax stops is 31 msec longer than before their tense counterparts (70 msec for lax vs 39 msec for tense). In addition, the average duration of the stop closure of tense stops is 135 msec longer than that of lax stops (69 msec for lax vs 204msec for tense). THESE DURATIONAL DIFFERENCES ARE 50 LARGE THAT THEY MAY BE PHONOLOGICALLY DETERMINED, NOT PHONETICALLY. Moreover, vowel duration varies with the speaker's sex. Female speakers have 5 msec shorter vowel duration before both stops. The quality of voicing, tense or lax, is also a cue to these two stop types, as it is in initial position, but the relative duration of the stops appears to be much more important cues. The duration of stops changes the stop perception while that of preceding vowel does not. The consequences of these results for the phonological description of Korean as well as the synthesis and automatic recognition of Korean will be discussed.

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Crystal growing of NaX type zeolite

  • Ha, Jong-Pil;Seo, Dong-Nam;Jung, Mi-Jeong;Moon, In-Ho;Cho, Sang-Joon;Park, Hyun-Min;Kim, Ik-Jin
    • 한국결정성장학회지
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    • 제9권4호
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    • pp.371-376
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    • 1999
  • A large NaX type zeolite crystal of a uniform particle size of 20$\mu\textrm{m}$ are grown with various {{{{{H}_{2}O}}}} content by hydrothermal reaction and added seed crystal (2~3$\mu\textrm{m}$) to reactant solution as a function of different adding seed levels from 3 to 15%. The result that increased purity of NaX zeolite above 95% and homogeneity of crystal size by increasing adding seed levels, also decreased crystallization time. It was explained that adding seed to synthesis solution leaded out increase of surface area for physical contact reaction and directed growth of seed crystal, so more rapid consumption of reaction gel as increase seeding levels.

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마이크로웨이브 플라즈마 화학기상증착장비를 사용한 유리기판상의 탄소나노튜브의 합성 (GROWTH OF CARBON NANOTUBES ON GLASS BY MICROWAVE PLASMA CHEMICAL VAPOR DEPOSITION)

  • 이재형;최성헌;최원석;홍병유;김정태;임동건;양계준
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 추계학술대회 논문집 Vol.18
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    • pp.99-100
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    • 2005
  • We have grown carbon nanotubes (CNTs) with a microwave plasma chemical vapor deposition (MPECVD) method, which has been regard as one of the most promising candidates for the synthesis of CNTs due to the vertical alignment, the low temperature and the large area growth. We use methane ($CH_4$) and hydrogen ($H_2$) gas for the growth of CNTs. 60 nm thick Ni catalytic layer were deposited on the TiN coated glass substrate by RF magnetron sputtering method. In this work, we report the effects of pressure on the growth of CNTs. We have changed pressure of processing (10 $\sim$ 20 Torr) deposition of CNTs. SEM (Scanning electron microscopy) images show diameter, length and cross section state CNTs.

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모호집합론을 사용한 에너지계통 설계의 최적선택 (Optimal Selection of Energy System Design Using Fuzzy Framework)

  • 김성호;문주현
    • 한국에너지공학회:학술대회논문집
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    • 한국에너지공학회 1998년도 추계 학술발표회 논문집
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    • pp.3-8
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    • 1998
  • The present work proposes the potential fuzzy framework, based on fuzzy set theory, for supporting decision-making problems, especially, selection problems of a best design in the area of nuclear energy system. The framework proposed is composed of the hierarchical structure module, the assignment module, the fuzzification module, and the defuzzification module. In the structure module, the relationship among decision objectives, decision criteria, decision sub-criteria, and decision alternatives is hierarchically structured. In the assignment module, linguistic or rank scoring approach can be used to assign subjective and/or vague values to the decision analyst's judgment on decision variables. In the fuzzification module, fuzzy numbers are assigned to these values of decision variables. Using fuzzy arithmetic operations, for each alternative, fuzzy preference index as a fuzzy synthesis measure is obtained. In the defuzzification module, using one of methods ranking fuzzy numbers, these indices are defuzzified to overall utility values as a cardinality measure determining final scores. According these values, alternatives of interest are ranked and an optimal alternative is chosen. To illustrate the applicability of the framework proposed to selection problem, as a case example, the best option choice of four design options under five decision criteria for primary containment wall thickening around large penetrations in an advanced nuclear energy system is studied.

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INTERSTELLAR ENVIRONMENTS IN THE LARGEMAGELLANIC CLOUD

  • KIM SUNGEUN
    • 천문학회지
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    • 제37권4호
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    • pp.211-216
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    • 2004
  • We present the results of an H I aperture synthesis mosaic of the Large Magellanic Cloud (LMC), made by combining data from 1344 separate pointing centers using the Australia Telescope Compact' Array (ATCA) and the Parkes multibeam receiver. The resolution of the mosaiced images is 50" (<15 pc, using a distance to the LMC of 55kpc). This mosaic, with a spatial resolution .15 times higher than that which had been previously obtained, emphasises the turbulent and fractal structure of the ISM on the small scale, resulting from the dynamical feedback of the star formation processes with the ISM. We also have done a widefield panoramic survey of H$\alpha$ emission from the Magellanic Clouds with an imager mounted on the 16-inch telescope at Siding Spring Observatory. This survey produced H$\alpha$ images which are equal to the ATCA survey in area coverage and resolution. This survey allows us to produce a continuum-subtracted image of the entire LMC. In contrast with its appearance in the H$\alpha$ image, the LMC is remarkably symmetric in H I on the largest scales, with the bulk of the H I residing in a disk of diameter 8. $^{\circ}4$ (7.3 kpc) and a spiral structure is clearly seen. The structure of the neutral atomic ISM in the LMC is dominated by H I filaments combined with numerous shells and holes.

표면특성이 제어된 기능성 나노 입자의 전자 및 의공학적 응용

  • 박영준;이준영;김중현
    • 한국결정학회:학술대회논문집
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    • 한국결정학회 2002년도 정기총회 및 추계학술연구발표회
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    • pp.54-55
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    • 2002
  • The fabrication, characterization and manipulation of nanoparticle system brings together physics, chemistry, materials science and biology in an unprecedented way. Phenomena occurring in such systems are fundamental to the workings of electronic devices, but also to living organisms. The ability to fabricate the surface of nanoparticles Is essential in the further development of functional devices that incorporate nanoscale features. Even more essential is the ability to introduce a wide range of chemical and materials flexibility into these structures to build up more complex nanostructures that can ultimately rival biological nanosystems. In this respect, polymers are potentially ideal nanoscale building blocks because of their length scale, well-defined architecture, controlled synthesis, ease of processing and wide range of chemical functionality that can be incorporated. In this presentation, we will look at a number of promising polymer-based nanoparticle fabrication strategies that have been developed recently, with an emphasis on those techniques that incorporate nanostructured polymeric particles into electronic devices or biomedical applications. And functional nanoparticles deliberately designed using several powerful process methods and their application will be discussed. Nanostructured nanoparticles, what we called, implies dispersed colloids with the size ranged from several nanometers to hundreds of nanometer. They have extremely large surface area, thus it is very important to control the morphology or surface functionality fitted for adequate objectives and properties. Their properties should be controlled for various kind of bio-related technologies, such as immunomagnetic cell separation, drug delivery systems, labeling and identification of lymphocyte populations, extracorporeal and hemoperfusion systems, etc. Well-defined polymeric nanoparticles can be considered as smart bomb or MEMS.

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수열합성을 이용한 나노분말 합성 및 연료감응태양전지 응용 (Synthesis of Nanopowders by Hydrothermal Method and their Application to Dye-sentisized Solar Cell Materials)

  • 임진영;안정석;안중호
    • 한국분말재료학회지
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    • 제25권4호
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    • pp.309-315
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    • 2018
  • In the present work, we synthesize nano-sized ZnO, $SnO_2$, and $TiO_2$ powders by hydrothermal reaction using metal chlorides. We also examine the energy-storage characteristics of the resulting materials to evaluate the potential application of these powders to dye-sensitized solar cells. The control of processing parameters such as pressure, temperature, and the concentration of aqueous solution results in the formation of a variety of powder morphologies with different sizes. Nano-rod, nano-flower, and spherical powders are easily formed with the present method. Heat treatment after the hydrothermal reaction usually increases the size of the powder. At temperatures above $1000^{\circ}C$, a complete collapse of the shape occurs. With regard to the capacity of DSSC materials, the hydrothermally synthesized $TiO_2$ results in the highest current density of $9.1mA/cm^2$ among the examined oxides. This is attributed to the fine particle size and morphology with large specific surface area.

동시 전기 폭발법에 의한 나노 합금 분말 제조에 관한 연구 II - Fe-Al alloy 분말 제조 (A Study on the Nano Alloy Powders Synthesized by Simultaneous Pulsed Wire Evaporation (S-PWE) method II - Synthesis of Ee-Al Nano Alloy Powders)

  • 이근희;이창규;김흥회;;;권영순
    • 한국분말재료학회지
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    • 제11권2호
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    • pp.105-110
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    • 2004
  • In this study the possibility to obtain a homogeneous mixture and to produce solid solutions and intermetallic compounds of Fe and Al nano particles by simultaneous pulsed wire evaporation (S-PWE) have been investigated. The Fe and Al wires with 0.45 mm in diameter and 35 mm in length were continuously co-fed by a special mechanism to the explosion chamber and simultaneously exploded. The characteristics, e.g., phase composition, particle shape, and specific surface area of Fe-Al nano powders have been analyzed. The synthesized powders, beside for Al and $\alpha$-Fe, contain significant amount of a high-temperature phase of $\gamma$-Fe, Fe Al and traces of other intermetallics. The phase composition of powders could be changed over broad limits by varying initial explosion conditions, e.g. wire distance, input energy, for parallel wires of different metals. The yield of the nano powder is as large as 40 wt % and the powder may include up to 46 wt % FeAl as an intermetallic compound.

탄화규소 휘스커의 (II): 적층결함 (Synthesis of Silicon Carbide Whiskers (II): Stacking Faults)

  • 최헌진;이준근
    • 한국세라믹학회지
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    • 제36권1호
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    • pp.36-42
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    • 1999
  • 2단계 열탄소환원법으로 탄화규소 휘스커를 기상-고상, 2단계, 기상-액상-고상 성장기구로 각각 합성하였다. 그리고 휘스커에 있는 적층결합을 X-ray와 투과전자현미경을 이용하여 분석하였다. 탄화규소 휘스커에 있는 적층결함은 휘스커의 지름과 상관관계가 있는 것으로 나타났다. 즉, 기상-고상, 2단계 성장, 기상-액상-고상 성장기구에 상관없이 지름이 1$\mu\textrm{m}$이하로 작아지는 경우 적층결합이 많아지고, 기상-액상-고상 기구로 성장한 지름이 2$\mu\textrm{m}$보다 큰 경우 적층결함이 거의 없는 것으로 나타났다. 이같은 현상은 휘스커 지름이 작아짐에 따라 휘스커의 비표면적이 증가하는 때문인 것으로 판단되었다.

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Electrospun Metal Oxide Composite Nanofibers Gas Sensors: A Review

  • Abideen, Zain Ul;Kim, Jae-Hun;Lee, Jae-Hyoung;Kim, Jin-Young;Mirzaei, Ali;Kim, Hyoun Woo;Kim, Sang Sub
    • 한국세라믹학회지
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    • 제54권5호
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    • pp.366-379
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    • 2017
  • Nanostructured materials have attracted considerable research interest over the recent decades because of their potential applications in nanoengineering and nanotechnology. On the other hand, the developments in nanotechnology are strongly dependent on the availability of new materials with novel and engineered morphologies. Among the novel nanomaterials reported thus far, composite nanofibers (NFs) have attracted considerable attention in recent years. In particular, metal oxide NFs have great potential for the development of gas sensors. Highly sensitive and selective gas sensors can be developed by using composite NFs owing to their large surface area and abundance of grain boundaries. In composite NFs, gas sensing properties can be enhanced greatly by tailoring the conduction channel and surface properties by compositional modifications using the synergistic effects of different materials and forming heterointerfaces. This review focuses on the gas sensing properties of composite NFs synthesized by an electrospinning (ES) method. The synthesis of the composite NFs by the ES method and the sensing mechanisms involved in different types of composite NFs are presented along with the future perspectives of composite NFs.