• Composites Research
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• v.34 no.5
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• pp.305-310
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• 2021

Mechanical properties of fiber reinforced composites were affected to fiber volume fractions (FVF) and interfacial property by sizing agent conditions. An optimum interface can relieve stress concentration by transferring the mechanical stress from the matrix resin to the reinforcements effectively, and thus can result in the performance of the composites. The interfacial properties and wettability between the epoxy resin and glass fiber (GF) were evaluated for different sizing agent conditions and FVFs. The surface energies of epoxy resin and different sizing agent treated GFs were calculated using dynamic and static contact angle measurements. The work of adhesion, W_a was calculated by using surface energies of epoxy matrix and GFs. The wettability was evaluated via the GF tow capillary test. The interfacial shear strength (IFSS) was evaluated by microdroplet pull-out test. Finally, the optimized GFRP manufacturing conditions could be obtained by using wettability and interfacial property.

• Korean Journal of Metals and Materials
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• v.46 no.10
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• pp.672-682
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• 2008

The resistance spot welding of TRIP590 steels was investigated to enhance understanding of weld fracture during tensile-shear strength (TSS) test. The main failure modes for spot welds of TRIP590 steels were nugget pullout and interfacial fracture. The peak load to cause a weld interfacial failure was found to be related to fracture toughness of the weld and the weld diameter. Although interfacial fracture occurred in the samples, the load carrying capacity of the weld was high and not significantly affected by the fracture mode. Substantial part of the weld exhibits the characteristic dimple (or elongated dimple) fractures on interfacial fractured surface, in spite of the high hardness values associated with the martensite microstructures. The high load-bearing ability of the weld is directly associated with the area of ductile fracture occurred in weld. Therefore, the judgment of the quality of resistance spot welds in TRIP590 steels, the load carrying capacity of the weld should be considered as an important factor than fracture mode.

• Journal of Adhesion and Interface
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• v.7 no.2
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• pp.1-11
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• 2006

Interfacial evaluation of the untreated and treated Jute and Hemp fibers reinforced different matrix polypropylene-maleic anhydride polypropylene copolymer (PP-MAPP) composites were investigated by micromechanical technique and dynamic contact angle measurement. For the statistical tensile strength of Jute and Hemp fibers, bimodal Weibull distribution was fitted better than the unimodal distribution. The acid-base parameter on the interfacial shear strength (IFSS) of the natural fiber composites was characterized by calculating the work adhesion, $W_a$. The effect of alkaline, silane coupling agent on natural fibers were obtained with changing MAPP content in PP-MAPP matrices. Alkaline treated fibers made the surface energy to be higher due to removing the weak boundary layers and thus increasing surface area, whereas surface energy of silane treated Jute and Hemp fibers decreased due to blocked high energy sites. MAPP in the PP-MAPP matrix caused the surface energy to increase due to introduced acid-base sites. Microfailure modes of two natural fiber composites were observed clearly differently due to different tensile strength of natural fibers.

• Composites Research
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• v.24 no.4
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• pp.11-16
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• 2011

Retention of interfacial shear strength (IFSS) of polymer composites at cryogenic temperature application is very important. In this work, single carbon tiber reinforced epoxy compositc was used to evaluate IFSS and apparent modulus under room and cryogenic temperatures. The property change of carbon and selected epoxy for particularly cryogenic temperature application were tested in tension and compression. Tensile strength and elongation of carbon fiber decreased at cryogenic temperature, whereas tensile modulus was almost same. On the other hand, epoxy matrix showed the increased tensile strength but decreased elongation. It can be due to maximum thermal contraction existing free volume in cryogenic temperature. IFSS increased up to $-10^{\circ}C$ and then decreased steadily. However, IFSS at cryogenic temperature was still similar to that at room temperature. This result is very useful to cryogenic application since selected epoxy toughness and interfacial adhesion can keep at such low temperature.

• Composites Research
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• v.32 no.2
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• pp.96-101
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• 2019

Interfacial adhesion between fiber and resin are related to composites performance, so it is very important to evaluate them accurately. In this study, the interfacial properties of microdroplets under fatigue loading conditions were evaluated. The mechanical properties and interfacial adhesion of epoxy resin with dopamine were studied. Tensile specimens were prepared to evaluate mechanical properties and epoxy microdroplets specimens were used for the evaluation of interfacial adhesion. In addition, in the microdroplet fatigue test, the same diameter of the microdroplet was used and the experiment was performed under the same conditions. As a result, it was confirmed that mechanical and interfacial properties were improved when dopamine was applied to epoxy resin through tensile and microdroplet experiments. It is considered that dopamine improves the degree of curing of the epoxy resin and imparts hydroxyl groups to the epoxy resin to increase the mechanical properties and the interfacial adhesion between the glass fibers.

• Proceedings of the KSR Conference
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• 2011.10a
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• pp.951-956
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• 2011

As the evaluation of loading characteristic on tilting mechanism is the most important one of the function test of tilting mechanism, the changing characteristic of load must be investigated on tilting of carbody for both the static and running condition of train. In this study, we reduced the load of tilting mechanism by adjusting the interface of carbody and bogie such as the weight balance, level of underframe, height of leveling valve, height of axle box and center position of tilting actuator with the characteristic curve of load for optimal condition of the tilting mechanism obtained in the previous study. Furthermore, the factor and effect of the interfacial structures respecting the load of tilting mechanism was evaluated by analyzing the changing characteristic of load obtained in the process of adjustment of interfaces. From these data, we will propose the maintenance standards for interfacial structures and tilting mechanism in order to minimize the load of tilting mechanism by analyzing in detail the characteristic of load for the main factors of the interfacial structure effecting on the load of tilting mechanism.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.04a
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• pp.159-162
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• 2000

Interfacial and microfailure properties of carbon fiber/epoxy matrix composites were evaluated using both tensile fragmentation and compressive Broutman tests with acoustic emission (AE). Amino-silane and maleic anhydride polymeric coupling agents were used via the dipping and electrodeposition (ED), respectively. Both coupling agents exhibited higher improvements in interfacial shear strength (IFSS) under tensile tests than compressive cases. However, ED treatment showed higher IFSS improvement than dipping case under both tensile and compressive test. The typical microfailure modes including fiber break, matrix cracking, and interlayer failure were observed during tensile test, whereas the diagonal slippage in fiber ends was observed during compressive test. For both the untreated and treated cases AE distributions were separated well under tensile testing. On the other hand, AE distributions were rather closer under compressive tests because of the difference in failure energies between tensile and compressive loading. Under both loading conditions, fiber breaks occurred around just before and after yielding point. Maximum AE voltage fur the waveform of carbon or basalt fiber breakage under tensile tests exhibited much larger than those under compressive tests.

• Composites Research
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• v.26 no.5
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• pp.303-308
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• 2013

Carbon fiber (CF) reinforced polypropylene (PP) compositeis was increased to amount consumed. In this study, recycle of composites by recycle times. CF was containing 20%. Mechanical and interfacial propertis of CF/PP was evaluation for number of recycle time. Mechanical assessment of CF/PP was tension, bending, fatigue tension test and izod test method. Interfacial assessment of CF/PP was wettability test and FE-SEM of fracture surface method. Fiber and matrix was changed to recycle time. The more recycle of CF/PP, the more interfacial bonding was decreased. Because fiber and matrix was damaged to thermal damage. And then reinforced CF was shorter than original shape.

• Journal of the Society of Cosmetic Scientists of Korea
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• v.22 no.2
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• pp.167-173
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• 1996

The stability of gel structured emulsion and the effect of polyols on it have been studied by rheological property and interfacial tension. In this paper, three types of gel structured emulsions were prepared by using three polyols respectively(glycerine for sample 1, 1.3 BG for sample 2, PG for sample 3). And both complex modulus($G^*$) and loss angle[$\delta$ = tan-1(G"/G')] of samples were investigated against oscillating shear stress and frequency($\omega$). The results show sample 1 is most highly consistent with oscillating shear stress. And the results were compared with those of accelerated tests concerning storage stability of gel structured emulsion. To correlate consistency of rheological property with storage stability, interfacial tension from which adsorption efficiency of surfactant(Octyldodecyl Ether) could be known was measured. Sample 1 showed the largest value of [$d{\gamma}/dIn_{Cconc. of surfactant}$] in Gibbs equation. In summary, the prediction of stability could be correctly made by the consistency of rheological property(G*,$\gamma$) of gel structured emulsion against oscillating shear stress and it could be supported by measuring interfacial tension. And polyol affected the value of [$d{\gamma}/dIn_{Cconc. of surfactant}$], consequently affected the stability.lity.

• Proceedings of the Korean Nuclear Society Conference
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• 2001.05a
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• pp.168-168
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• 2001