• Title/Summary/Keyword: interface topography

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Surface Observation of Mg-HA Coated Ti-6Al-4V Alloy by Plasma Electrolytic Oxidation

  • Yu, Ji-Min;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.198-198
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    • 2016
  • An ideal orthopedic implant should provide an excellent bone-implant connection, less implant loosening and minimum adverse reactions. Commercial pure titanium (CP-Ti) and Ti alloys have been widely utilized for biomedical applications such as orthopedic and dental implants. However, being bioinert, the integration of such implant in bone was not in good condition to achieve improved osseointegraiton, there have been many efforts to modify the composition and topography of implant surface. These processes are generally classified as physical, chemical, and electrochemical methods. Plasma electrolytic oxidation (PEO) as an electrochemical route has been recently utilized to produce this kind of composite coatings. Mg ion plays a key role in bone metabolism, since it influences osteoblast and osteoclast activity. From previous studies, it has been found that Mg ions improve the bone formation on Ti alloys. PEO is a promising technology to produce porous and firmly adherent inorganic Mg containing $TiO_2$($Mg-TiO_2$ ) coatings on Ti surface, and the amount of Mg introduced into the coatings can be optimized by altering the electrolyte composition. In this study, a series of $Mg-TiO_2$ coatings are produced on Ti-6Al-4V ELI dental implant using PEO, with the substitution degree, respectively, at 0, 5, 10 and 20%. Based on the preliminary analysis of the coating structure, composition and morphology, a bone like apatite formation model is used to evaluate the in vitro biological responses at the bone-implant interface. The enhancement of the bone like apatite forming ability arises from $Mg-TiO_2$ surface, which has formed the reduction of the Mg ions. The promising results successfully demonstrate the immense potential of $Mg-TiO_2$ coatings in dental and biomaterials applications.

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Post Annealing Effect on the Characteristics of Al2O3 Thin Films Deposited by Aerosol Deposition on 4H-SiC (4H-SiC기판 위에 Aerosol Deposition으로 증착된 Al2O3박막의 후열처리 효과)

  • Yu, Susanna;Kang, Min-Seok;Kim, Hong-Ki;Lee, Young-Hie;Koo, Sang-Mo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.8
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    • pp.486-490
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    • 2014
  • $Al_2O_3$ films on silicon carbide were fabricated by Aerosol deposition with annealing temperature at $800^{\circ}C$ and $1,000^{\circ}C$. The effect of thermal treatment on physical properties of $Al_2O_3$ thin films has been investigated by XRD (X-ray diffraction), AFM (atomic force microscope), SEM (scanning electron microscope), and AES (auger electron spectroscopy). Also electrical properties have been investigated by Keithley 4,200 semiconductor parameter analyzer to explain the interface trapped charge density ($D_{it}$), flatband voltage ($V_{FB}$) and leakage current ($I_o$). $Al_2O_3$ films become crystallized with increasing temperature by calculating full width at half maximum (FWHM) of diffraction peaks, also surface morphology is observed by topography measurement in non-contact mode AFM. $D_{it}$ was $2.26{\times}10^{-12}eV^{-1}.cm^{-2}$ at $800^{\circ}C$ annealed sample, which is the lowest value in all samples. Also the sample annealed at $800^{\circ}C$ has the lowest leakage current of $4.89{\times}10^{-13}A$.

Two-phase Finite Volume Analysis Method of Debris Flows in Regional-scale Areas (2상 유한체적모델 기반의 광역적 토석류 유동해석기법)

  • Jeong, Sangseom;Hong, Moonhyun
    • Journal of the Korean Geotechnical Society
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    • v.38 no.4
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    • pp.5-20
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    • 2022
  • To analyze the flow and density variations in debris flows, a two-phase finite volume model simplified with momentum equations was constructed in this study. The Hershel-Buckley rheology model was employed in this model to account for the internal and basal friction of debris flows and was utilized to analyze complex topography and entrainments of basal soil beds. In order to numerically solve the debris flow analysis model, a finite volume model with the Harten-Lax-van Leer-Contact method was used to solve the conservation equation for the debris flow interface. Case studies of circular dam failure, non-Newtonian fluid dam failure, and multiple debris flows were analyzed using the proposed model to evaluate shock absorption capacity, numerical isotropy, model accuracy, and mass conservation. The numerical stability and correctness of the debris flow analysis of this analysis model were proven by the analysis results. Additionally, the rate of debris flow with various rheological properties was systematically simulated, and the effect of debris flow rheological properties on behavior was analyzed.

Assessing the repeatability of reflection seismic data in the presence of complex near-surface conditions CO2CRC Otway Project, Victoria, Australia (복잡한 천부구조하에서 반사법 탄성파자료의 반복성에 대한 평가, 호주, 빅토리아, CO2CRC Otway 프로젝트)

  • Al-Jabri, Yousuf;Urosevic, Milovan
    • Geophysics and Geophysical Exploration
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    • v.13 no.1
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    • pp.24-30
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    • 2010
  • This study utilises repeated numerical tests to understand the effects of variable near-surface conditions on time-lapse seismic surveys. The numerical tests were aimed at reproducing the significant scattering observed in field experiments conducted at the Naylor site in the Otway Basin for the purpose of $CO_2$ sequestration. In particular, the variation of elastic properties of both the top soil and the deeper rugose clay/limestone interface as a function of varying water saturation were investigated. Such tests simulate the measurements conducted in dry and wet seasons and to evaluate the contribution of these seasonal variations to seismic measurements in terms of non-repeatability. Full elastic pre-stack modelling experiments were carried out to quantify these effects and evaluate their individual contributions. The results show that the relatively simple scattering effects of the corrugated near-surface clay/limestone interface can have a profound effect on time-lapse surveys. The experiments also show that the changes in top soil saturation could potentially affect seismic signature even more than the corrugated deeper surface. Overall agreement between numerically predicted and in situ measured normalised root-mean-square (NRMS) differences between repeated (time-lapse) 2D seismic surveys warrant further investigation. Future field studies will include in situ measurements of the elastic properties of the weathered zone through the use of 'micro Vertical Seismic Profiling (VSP)' arrays and very dense refraction surveys. The results of this work may impact on other areas not associated with $CO_2$ sequestration, such as imaging oil production over areas where producing fields suffer from a karstic topography, such as in the Middle East and Australia.

Development of a user-friendly information system for river water quality using Web GIS (Web GIS를 이용한 수요자 중심의 하천수질 정보시스템 구현)

  • 엄정섭;신소은
    • Spatial Information Research
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    • v.10 no.1
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    • pp.45-59
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    • 2002
  • The author argues that the current Government Information System for river water quality appears to be non-user friendly due to lack of the cartographic representation for the field monitoring data. Acknowledging these constraints, an operational, user-friendly information system has been developed by combining Internet technology with GIS. A digital map for water quality has been generated by overlaying monitoring data on existing cartographic data such as road, topography and administrative boundary etc. A user interface was designed to address the need to querry the large spatial databases by non-GIS and non-environmental experts. The system has been checked experimentally and enabled the users to querry data required simply. And detailed visual maps for water quality can be generated over large areas quickly and easily. A visual mapping system for water quality was developed by reframing the monitoring data as graphic symbols and it was ideally suited to exploring area-wide water quality at a user-friendly manner due to extensibility and scalability along the various survey points. This system based on Web GIS could be accessed anywhere if internet is available. It would play a crucial role in improving the quality of public information service if it is operationally introduced into the Government since the highly user-friendly interface provides a completely new means for disseminating information far water pollution in a visual and interactive manner to the general public.

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Two Layer Modelling with Applications to Exchange Flow and Internal Tide (이층류 모델링의 교환류와 내부조석파 연구에의 적용)

  • Kang, Sok-Kuh;Abbott, Michael-B.;Heung, Jae-Lie;Yum, Ki-Dai
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.9 no.1
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    • pp.9-23
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    • 1997
  • A numerical study of a two-layer, stratified flow is investigated, using the implicit finite difference method in one dimension. The results of computational method have been tested and, in case of lock exchange flow, compared with the results of experimental data. The results of model experiments with various interfacial, bottom friction coefficients along with various time weighting factor of numerical scheme and dissipative interface are shown and discussed. Two-layer model experiment has been also carried out to investigate the generation and propagation characteristics of internal tidal wave over the steep bottom topography under stratified condition. The internal wave seems to well radiate through the downstream boundary under the experiments adopting radiation conditions both at two layers and only at upper layer, confirming the applicability of radiational boundary condition in stratified flows. It is also shown that the internal wave through the downstream boundary propagates more actively with increasing thickness of lower layer in the downstream. This implies that the potential tidal energy in the interface will depend upon the thickness of lower layer for the constant thickness of upper layer.

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Cellular activities of osteoblast-like cells on alkali-treated titanium surface (알칼리 처리된 타이타늄 표면에 대한 골아 유사세포의 세포 활성도)

  • Park, Jin-Woo;Lee, Deog-Hye;Yeo, Shin-Il;Park, Kwang-Bum;Choi, Seok-Kyu;Suh, Jo-Young
    • Journal of Periodontal and Implant Science
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    • v.37 no.sup2
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    • pp.427-445
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    • 2007
  • To improve osseointegration at the boneto-implant interface, several studies have been carried out to modify titanium surface. Variations in surface texture or microtopography may affect the cellular response to an implant. Osteoblast-like cells attach more readily to a rougher titanium surface, and synthesis of extracellular matrix and subsequent mineralization were found to be enhanced on rough or porous coated titanium. However, regarding the effect of roughened surface by physical and mechanical methods, most studies carried out on the reactions of cells to micrometric topography, little work has been performed on the reaction of cells to nanotopography. The purpose of this study was to examme the response of osteoblast-like cell cultured on blasted surfaces and alkali treated surfaces, and to evaluate the influence of surface texture or submicro-scaled surface topography on the cell attachment, cell proliferation and the gene expression of osteoblastic phenotype using ROS 17/2.8 cell lines. In scanning electron micrographs, the blasted, alkali treated and machined surfaces demonstrated microscopic differences in the surface topography. The specimens of alkali treatment had a submicro-scaled porous sur-face with pore size about 200 nm. The blasted surfaces showed irregularities in morphology with small(<10 ${\mu}m$) depression and indentation among flatter-appearing areas of various sizes. Based on profilometry, the blasted surfaces was significantly rougher than the machined and the alkali treated surfaces (p$TiO_2$) were observed on alkali treated surfaces, whereas not observed on machined and blasted surfaces. The attachment morphology of cells according to time was observed by the scanning electron microscope. After 1 hour incubation, the cells were in the process of adhesion and spreading on the prepared surfaces. After 3 hours, the cells on all prepared surfaces were further spreaded and flattened, however on the blasted and alkali treated surfaces, the cells exhibited slightly irregular shapes and some gaps or spaces were seen. After 24 hours incubation, most cells of the all groups had a flattened and polygonal shape, but the cells were more spreaded on the machined surfaces than the blasted and alkali treated surfaces. The MTT assay indicated the increase on machined, alkali treated and blasted surfaces according to time, and the alkali treated and blasted surfaces showed significantly increased in optical density comparing with machined surfaces at 1 day (p<0.01). Gene expression study showed that mRNA expression level of ${\alpha}\;1(I)$ collagen, alkaline phosphatase and osteopontin of the osteoblast-like cells showed a tendency to be higher on blasted and alkali treated surfaces than on the machined surfaces, although no siginificant difference in the mRNA expression level of ${\alpha}\;1(I)$ collagen, alkaline phosphatase and osteopontin was observed among all groups. In conclusion, we suggest that submicroscaled surfaces on osteoblast-like cell response do not over-ride the one of the surface with micro-scaled topography produced by blasting method, although the microscaled and submicro-scaled surfaces can accelerate osteogenic cell attachment and function compared with the machined surfaces.

Attachment of Human Gingival Fibroblast to Various Subgingival Restorations;A Comparative Study in Vitro (다양한 치은 연하 수복물에 대한 치은 섬유아 세포 부착 연구)

  • Lee, Eun-Suk;Song, In-Taeck;Lim, Jeong-Su;Kim, Hyung-Seop
    • Journal of Periodontal and Implant Science
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    • v.29 no.3
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    • pp.621-636
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    • 1999
  • When mucoperiosteal flaps are positioned and sutured to desirable position, the wound contains several interface between tissues which differ fundamentally in composition & biological reaction. Thus the C-T surface of the flap will, on one hand, oppose another vascularized surface, and on the other, the avascular dental material for example, when root resoptions, fractured root, endodontic perforation, deep root carious lesions were filled with amalgam, glass ionomer, resin etc. Recently, a number of case report described the successful treatment of a subgingival root lesion with restorative material & free gingival graft, open flap surgery, but more objective research was needed . Most of study on restorative materials were concerned for cytotoxicity not for actual healing event on that materials and its influencing factors such as biocompatibility, surface wettability, surface topography . The aim of this in vitro study was to evaluate the effect of amalgam, resin modified glass ionomer, composite resin per se, and their surface roughness on the growth of human gingival fibroblast. The cells were obtained and placed on culture flask and incubated for 3 days with the prepared test materials. Then count the attached cell number with hemocytometer,(n=12) and 2 samples were examined with SEM about attachment cell morphology . Another 4 samples were evaluated on their surface roughness with Talysurf and average surface roughness value(Ra) were obtained. Statistical difference in attached cell number, roughness value were analyzed using ANOVA. The number of attached cell was as follows, for root dentin specimen 16.7${\pm}$4.41, resin modified glass ionomer 14.0${\pm}$4.15, resin 8.13${\pm}$3.63, amalgam 0.72${\pm}$3.33(${\times}10^3$). Between root dentin and resin-modified glass ionomer, no significant difference was observed, but resin, amalgam showed a significant less cell numbers than for root dentin, resin modified glass ionomer cement. SEM examination expressed many cell surface attachment apparatus in root dentin and resin modified glass ionomer specimens. For resin specimen, cell attachment was observed but exposed less appratus. The average surface roughness value are following results. Dentin specimen 0.6972${\pm}$ 0.104, resin modified glass ionomer 0.0822${\pm}$0.009, resin 0.0875${\pm}$0.005, amalgam 4.2145${\pm}$0.985(${\mu}m$). Between root dentin, resin-modified glass ionomer, and resin, no significant difference was observed, but amalgam showed a significant more rough surface than other groups. When evlauated the interrelationship between cell attachment and surface roughness, therefore, there was weak reverse correlation.(pearson correlation : - 0.593) These results suggest that resin modified glass ionomer have the favorable healing potential when used for subgingival restoration. And for relationship between cell attachment and surface characteristics, further investigations were needed.

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Effect of Electropolishing on Surface Quality of Stamped Leadframe (Stamped Leadframe의 표면 품질에 미치는 전해연마 효과)

  • 남형곤;박진구
    • Journal of the Microelectronics and Packaging Society
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    • v.7 no.3
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    • pp.45-54
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    • 2000
  • The effect of electropolishing far stamped leadframe on the removal of the edge burr and residual stress relief was examined. The present study showed that the electropolishing could be used for enhanced surface quality of stamped leadframes. The electropolishing was performed at the condition of 60% phosphoric acid electrolyte, 5 ampere of current and 3 cm electrode gap at $70^{\circ}C$ for 2 minutes for Alloy42 type leadframe, and $50^{\circ}C$ for 1.5 minutes for C-194 type leadframe. The FWHM values from X-ray diffraction showed that residual stress of electropolished leadframe recovered to the level of as-received raw materials and surface roughness measured by using AFM tuned out to be improved by 0.079 $\mu\textrm{m}$ and 0.014 $\mu\textrm{m}$ ($R_{rms}$) far alloy 42 and C-194 type leadframes, respectively. The plated thickness using XRF showed the improved uniformity in thickness variation by 0.4~0.5 $\mu\textrm{m}$ and grain growth, which is favorable for interface adhesion, was also observed from the bake test samples. We could certify dimensional stability of leadframe with inspection by means of 3D-topography and hardness measurements.

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Constructing Forest Information Management System using GIS and Aerial Orthophoto (GIS와 항공정사사진을 이용한 산림정보 관리시스템 구축)

  • Kim, Joon-Bum;Jo, Myung-Hee;Kwon, Tae-Ho;Kim, In-Ho;Jo, Yun-Won;Shin, Dong-Ho
    • Journal of the Korean Association of Geographic Information Studies
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    • v.7 no.2
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    • pp.57-68
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    • 2004
  • Recently in order to more effectively and scientifically process forest official tasks, which have been focused on documents and inventories, they should be applied with the up-to-date spatial information technologies. Especially, the forest resource information management based on GIS(geographic information system) and aerial orthophoto is expected not only to play an important role as DSS(decision support system) for domestic forest conservation policy and forestry development industry but also to service forest resource information toward people such as the owners of a mountain rapidly. In this study, the important forest information such as digital topography map, digital forest type map, digital forest cadastral map, digital aerial photographs and attribute data were first reprocessed and constructed in DBMS(data base management system). In addition, forest officials could analyze and retrieve forest information by using detail sub-application systems such as forest cadastral retrieval, forest land development information management, reserved forest information management and forest resource information retrieval. For this, the user interface is developed by using Visual Basic 6.0 and MapObjects 2.1 of ESRI based on CBD(component based development) technology. The result of developing this system will not only perform constructing economical forest and better environment but also be the foundation of domestic spatial technology for forest resource management.

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