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검색결과 1,273건 처리시간 0.024초

Oxidation of carbohydrates and A corbon-13 n. m. r. study of the keto sugars

  • An, Seung-Ho
    • Archives of Pharmacal Research
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    • 제9권4호
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    • pp.229-232
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    • 1986
  • Three inexpensive oxidation reagents, namely pyridinium chlorochromate, chromium trioxide-dipyridine and nicotinium dichromate were utilized for oxidation of carbohydrates in 78-92% yield. Hydration could be eliminated in the oxidation of pentopyranosides and hexopyranosides, while pentofuranosides had a tendency to be easily hydrated during the oxidation. In the carbon-13 n. m. r. study, the carbonyl function resulted from the oxidation affected on the chemical shifts of $\alpha$- and $\beta$-carbons of methyl 3. 4-O-isopropylidene-$\beta$-D-arabinopyranosid-2-ulose (8) and 1,2 : 4, 5-di-O-isopropylidene-$\beta$-D-erythro-2, 3-hexodiulo-2, 6-pyranose (10) to slightly down fields (0.7-2.6 p. p. m.) compared with the chemical shifts before oxidation. While the carbonyl groups of 1. 2-O-isopropylidene-5-O-ethyloxycarbonyl-$\alpha$-D-erythro-pentofuran-3-ulose (4) and methyl 3, 5-0-isopropylidene-$\alpha$-D-threo-pentofuranosid-2-ulose (6) pushed the $\alpha$-carbons to up fields (3, 2-18.3 p. p. m. However, the order of signals on the spectra before and after oxidation remained unaltered.

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수포작용제(HD) 분석을 위한 단일방울 미세농축법 연구 (Single Drop Microextraction for Analysis of Mustard Gas(HD))

  • 박양기;김성기;손병훈;박명주
    • 한국군사과학기술학회지
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    • 제11권2호
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    • pp.95-100
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    • 2008
  • A fast, simple, inexpensive, and reproducible sample preparation for extraction and analysis of HD in water was studied using single-drop microextraction(SDME) and GC-MS. Operation parameters, such as extraction solvent, extraction time were optimized. The optimized conditions were $1\{mu}L$ trichloroethylene and 10 min extraction time. In these conditions, about 42 times higher enrichment factor(EF) was obtained. The detection limit of HD was $1\{mu}g/L$, and the precision expressed as relative standard deviation was about 9.0%.

구동 커패시터의 용량에 따른 단상유도전동기 출력특성에 관한 연구 (Output Characteristics of Capacitor-run type Single Phase Induction Motor considering Capacitance)

  • 김철진;이달은;진용선;최철용;백수현
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2002년도 하계학술대회 논문집 B
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    • pp.848-850
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    • 2002
  • Single phase induction motor is directly used usual source, it can be a source of an appliance such as mechanical fan, refrigerator, washing machine, etc. Especially capacitor-run single phase induction motor is suitable to make more inexpensive and high efficient products because it is more high efficiency, and good to start than other single phase induction motors. Generally, voltage and current of capacitor-run single phase induction motor transfer to the part of positive phase and negative phase based on two motor theory. In this paper, we simulate the torque characteristics to capacitance variation from single phase induction motor's equivalent circuit. Through the test using the real motor, we compare and investigate the maximum torque of run state related with capacitance and the adequacy of the converted model.

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MULTI-SHAPE ERYTHROCYTE IMAGING AND THEIR DEFORMABILITY ANALYSIS IN A MICROFLUIDIC ENVIRONMENT

  • Jayavanth, Sanjay;Pak, Bock-Choon
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회B
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    • pp.2791-2796
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    • 2007
  • In their long journey through the cardiovascular circuit, erythrocytes are coerced to shape transform and assume different shapes on account of varying flow conditions in different blood vessels. The present work was aimed to visualize these erythrocyte shape transformations by an invitro microcirculatory model, and assess multi-shape erythrocyte deformability. The model uses an in-house fabricated, inexpensive disposable micro flow channel to mimic certain invivo conditions and a fast frame video microscopic system for imaging the shape changes in erythrocytes. Results show the multi-shape transformation of erythrocyte christened as discoidal shape, the asymmetrically deformed 'hat' and 'bullet-like' shapes, and the axially deformed 'slipper' and 'spindle-like' shapes. Specific erythrocyte showed the shape transition and transformation while passing through the observed window. The obtained erythrocyte shapes very analyzed for deformability index using image processing techniques that varied significantly (p <0.001) for different shapes as compared with the resting shape.

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BioMEMS 기반의 조기 질병 진단 기술에 관한 연구 (BioMEMS-EARLY DISEASE DETECTION)

  • 카나카싱;김경천
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회B
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    • pp.2781-2784
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    • 2007
  • Early detection of a disease is important to tackle treatment issues in a better manner. Several diagnostic techniques are in use, these days; for such purpose and tremendous research is going on to develop newer and newer methods. However, more work is required to be done to develop cheap and reliable early detection techniques. Micro-fluidic chips are also playing key role to deliver new devices for better health care. The present study focuses on a review of recent developments in the interrogation of different techniques and present state-of-the-art of microfluidic sensor for better, quick, easy, rapid, early, inexpensive and portable POCT (Point of Care testing device) device for a particular study, in this case, bone disease called osteoporosis. Some simulations of the microchip are also made to enable feasibility of the development of a blood-chip-based system. The proposed device will assist in early detection of diseases in an effective and successful manner.

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디지털 카메라를 이용한 구조물의 3차원 좌표 추출에 관한 연구 (A Study on 3D-Coordinate Extraction of Structure by Using The Digital Camera)

  • 김감래;김학준;박용
    • 한국측량학회:학술대회논문집
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    • 한국측량학회 2003년도 추계학술발표회 논문집
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    • pp.219-224
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    • 2003
  • Recently, the number of the use of Digital Photogrammetry is increasing, the Digital Photogrammetry is used for the acquisition of images, remote sensing and three dimension location. Especially, the three dimension location is more activated to use digital camera for the Digital Photogrammetry. The reason is that it is cheap and easy to use and also it has high confidence. Using non-metric digital camera not metric camera, in this research, to get images and apply the images to the Direct Liner Transformation which is one of the techniques in Digital Photogrammetry to get three dimensional location of a point. Ⅰ programmed the procedure with Visual C++ to get the position of points speedly and I tested possibility whether it can analyze the displacement and the existence of structure with measurement system which is structured by a inexpensive non-metric digital camera.

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지형도 공급단가 결정에 관한 연구 (A study on the Decision of the Map Price)

  • 박경식;박지언;김창우;이재기
    • 한국측량학회:학술대회논문집
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    • 한국측량학회 2004년도 춘계학술발표회논문집
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    • pp.413-418
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    • 2004
  • The purpose of this research calculates the map manufacture cost and there are we even though we determine proper map price. We distinguished the budget item of NGI in 2003 with the direct cost to the overhead cost. A map manufacture cost classified a direct and overhead cost as a nap manufacture cost commonness cost and no relation cost and was calculated. The result to analyze the item of the charge, It is impossible to withdraw the map manufacture cost selling the map. This is because a map sale price inexpensive than the map manufacture price. We presented a two alternative in research to see consequently about a map price raising.

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PMM for Surface Treatment of Concrete with the Utilization of By-Products

  • Drochytka, Rostislav;Zizkova, Nikol
    • International Journal of Concrete Structures and Materials
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    • 제2권1호
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    • pp.49-55
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    • 2008
  • The disadvantage of PMM's (polymer-modified mortars) that are currently on the market is the utilization of expensive polymer additives and also the cost of the other components. One of the possibilities how to decrease this price is the effective utilization of waste materials which are very inexpensive in spite of their good properties. The combinations of different degree in polymer adhesiveness and waste secondary raw materials - fly ash - are experimentally verified in the paper. The use of fly ash in adhesive materials for ceramic tiles is limited by unsatisfactory initial adhesiveness to sintered ceramic sherd as a result of a running pozzolanic reaction that lowers the efficiency of polymer additives. On the other hand, the use of adhesive and backfill coating materials for gluing ETICS board insulation materials has brought very good results.

두경부영역에서의 초음파촬영을 이용한 진단 (DIAGNOSTIC ULTRASONOGRAPHY IN HEAD AND NECK REGION)

  • 조병욱;이용찬;고백진;최창완
    • Maxillofacial Plastic and Reconstructive Surgery
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    • 제12권1호
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    • pp.96-102
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    • 1990
  • Diagnostic ultrasound has the advantages of being noninvasive without any known deleterious biologic effect, rapid, painless, inexpensive and easily reproducible. The author used a real time sector scanner (Picker, Artis USA:5-7.5 MHz) for examing of lipoma, abscess, hematoma, lymphnode enlargement etc. and evaluated ultrasonograph as a diagnostic aid in head and neck region.

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Atmospheric Pressure Plasma Research Activity in Korea

  • Uhm, Han S.
    • 한국표면공학회지
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    • 제34권5호
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    • pp.367-377
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    • 2001
  • Plasma is generated by electrical discharge. Most plasma generation has been carried out at low-pressure gas typically less than one millionth of atmospheric pressure. Plasmas are in general generated from impact ionization of neutral gas molecules by accelerated electrons. The energy gain of electrons accelerated in an electrical field is proportional to the mean free path. Electrons gain more energy at low-pressure gas and generate plasma easily by ionization of neutrals, because the mean free path is longer. For this reason conventional plasma generation is carried out at low pressures. However, many practical applications require plasmas at high-pressure. In order to avoid the requirement for vacuum pumps, researchers in Korea start to develop plasmas in high-pressure chambers where the pressure is 1 atmosphere or greater. Material processing, environmental protection/restoration and improved energy production efficiency using plasmas are only possible for inexpensive bulk plasmas. We thus generate plasmas by new methods and plan to set foundations for new plasma technologies for $21^{st}$ / century industries. This technological research will play a central role in material processing, environmental and energy production industries.

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