• 제목/요약/키워드: in situ method

검색결과 1,601건 처리시간 0.032초

Effects of Hydrogen on the PWSCC Initiation Behaviours of Alloy 182 Weld in PWR Environments

  • Kim, H.-S.;Hong, J.-D.;Lee, J.;Gokul, O.S.;Jang, C.
    • Corrosion Science and Technology
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    • 제14권3호
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    • pp.113-119
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    • 2015
  • Alloy 82/182 weld metals had been extensively used in joining the components of the PWR primary system. Unfortunately, there have been a number of incidents of cracking caused by PWSCC in Alloy 82/182 welds during the operation of PWR worldwide. To mitigate PWSCC, optimization of water-chemistry conditions, especially dissolved hydrogen (DH) and Zn contents, is considered as the most promising and effective remedial method. In this study, the PWSCC behaviours of Alloy 182 weld were investigated in simulated PWR environments with various DH content. Both in-situ and ex-situ oxide characterizations as well as PWSCC initiation tests were performed. The results showed that PWSCC crack initiation time was shortest in PWR water (DH: 30cc/kg). Also, high stress reduced crack initiation time. Oxide layer showed multi-layered structures consisted of the outer needle-like Ni-rich oxide layer, Fe-rich crystalline oxide, and inner Cr-rich inner oxide layers, which was not altered by the level of applied stress. To analyse the multi-layer structure of oxides, EIS measurement were fitted into an equivalent circuit model. Further analyses including TEM and EDS are underway to verify appropriateness of the equivalent circuit model.

In situ Hybridization of a Megalocytivirus Using Nucleic Acid Probes against ATPase and the Major Capsid Protein of Rock Bream Iridovirus

  • Lee, Nam-Sil;Do, Jeong-Wan;Jung, Sung-Ju;Park, Mi-Seon;Kim, Jin-Woo;Kim, Yi-Cheong
    • Fisheries and Aquatic Sciences
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    • 제9권4호
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    • pp.146-152
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    • 2006
  • Systemic infections of maricultured fishes by Megalocytivirus species have occurred over a broad area in South Korea, causing extensive economic loss. We developed digoxigenin-labeled nucleic acid probes against the 230-bp ATPase and 311-bp major capsid protein (MCP) of rock bream Oplegnathus fasciatus iridovirus (RBIV) using polymerase chain reaction, and an in situ hybridization (ISH) method to detect Megalocytivirus in formalin-fixed tissues of mariculture species (rock bream, sea bass, and olive flounder). ISH-positive cells were abundant in the hematopoietic and connective tissues of various organs, while brain tissue showed little or no signal. The ISH procedure can become an important diagnostic tool in complement with histopathological methods, and advances epidemiological studies on the origin and distribution of Megalocytivirus in mariculture.

Channel Electrode Voltammetric and In Situ Electrochemical ESR Studies of Comproportionation of Methyl Viologen in Acetonitrile

  • 이지우
    • Bulletin of the Korean Chemical Society
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    • 제17권2호
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    • pp.162-167
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    • 1996
  • Two redox processes of methyl viologen (+2/+, +/0) in acetonitrile were investigated by using channel electrode voltammetric and in situ electrochemical ESR methods. Two separated unequal plateau currents of the first (+2/+) and second (+/0) redox processes of the viologen were observed in the channel electrode voltammograms and showed a cube-root depedndence on the electrolyte flow rate, respectively. The simple Levich analysis resulted in two different diffusion coefficients of $D_{+2}=2.2{\times}10^{-5}\;cm^2/s$ and $D_+=3.0{\times}10^{-5}cm^2/s$ from the limiting currents. In situ electrochemical ESR studies were performed for the monocation radicals generated at the potentials of the two plateau currents in the electrolyte flow range $1.3{\times}10^{-1}{\geq}v_f{\geq}2.7{\times}10^{-3}\;cm^3/s$. Backward implicitfinite difference method was employed to simulate the electrochemical kinetic problem of two sequential electron transfers ($MV^{+2}+e{\leftrightarrows}MV^+,\;MV^{+}+e{\leftrightarrows}MV^0$) coupled with reversible comproportionation ($MV^{2+}+MV^0{{\leftrightarrows}^{k_f}_{k_b}}2MV^+$). $k_f$ was found to be greater than ($10^6M^{-1}s^{-1}.

수소/산소/TEOS 확산화염 중 직접포집을 이용한 실리카 입자의 성장특성에 관한 연구 (Growth Characteristics of Silica Particles Using In situ Sampling from $H_2/O_2TEOS$ Diffusion Flame)

  • 정창훈;안강호;최만수;이준식
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2000년도 춘계학술대회논문집B
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    • pp.404-409
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    • 2000
  • Growth characteristics of silica particles have been studied experimentally using in situ sampling technique from $H_2/O_2TEOS$ diffusion flame with carefully devised sampling probe. Verification of sampling result was done through new method and effects of flame condition and TEOS flow rate on growth characteristics of silica particles were investigated. By comparing particles sampled by thermophoretic sampling in flame with those by collector sampling after probe, particles do not change before and after probe sampling, which was clearly proved from the fact that the result of TEM image analysis makes good agreement with that of SMPS measurement. As flame temperature increases, the effect of coalescence or sintering becomes important mechanism during growth of silica particles, resulting in canceling the effect of coagulation, which makes mean diameter of silica particles increase slowly. With increase in TEOS flow rate, the number concentration of generated silica particle increases but residence time of particles in flame decreases. As a result, there exists upper limit to which the diameter of silica particle increases under same flame condition.

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지반의 교란을 최소화 한 원위치시험법 개발 및 적용 : 스크류재하시험 (Low-Soil Disturbance In-Situ Test Method Development and Its Application : Screw Plate Loading Test)

  • 이용수;황웅기;최용규;김태형
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2009년도 춘계 학술발표회
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    • pp.977-986
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    • 2009
  • Sampling disturbance can introduce considerable errors in the laboratory estimation of geotechnical properties of soils, and the results obtained from sophisticated sampling and careful laboratory testing are not matching with field behavior. Therefore, it is advantage to adopt in-situ testing techniques for the estimation of geotechnical parameters. Therefore, Screw plate loading test, one of new field test technologies, has been investigated in this study. This test can be utilized to find out important properties of soils such as load-displacement, elastic modulus, and shear strength. The screw plate loading test modified from the plate loading test is an experiment underneath ground by inserting a spiral type of auger screw. The structure and characteristics of the screw plate loading test device was examined in detail. In addition, The new screw plate loading test device was manufactured to refer the previous studies. The reliability of developing screw plate loading test was examined through the analysis of the laboratory test.

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단순 선형열원 모델을 이용한 지중 유효 열전도도와 보어홀 유효 열저항 산정 (Evaluation of Ground Effective Thermal Conductivity and Borehole Effective Thermal Resistance from Simple Line-Source Model)

  • 손병후
    • 설비공학논문집
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    • 제19권7호
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    • pp.512-520
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    • 2007
  • The design of a ground-source heat pump system includes specifications for a ground loop heat exchanger where the heat transfer rate depends on the effective thermal conductivity of the ground and the effective thermal resistance of the borehole. To evaluate these heat transfer properties, in-situ thermal response tests on four vertical test boreholes with different grouting materials were conducted by adding a monitored amount of heat to circulating water. The line-source method is applied to the temperature rise in an in-situ test and extended to also give an estimate of borehole effective thermal resistance. The effect of increasing thermal conductivity of the grouting materials from 0.818 to $1.104W/m^{\circ}C$ resulted in overall increases in effective thermal conductivity by 15.8 to 56.3% and reductions in effective thermal resistance by 13.0 to 31.1%.

Thermal behavior of groundwater-saturated Korean buffer under the elevated temperature conditions: In-situ synchrotron X-ray powder diffraction study for the montmorillonite in Korean bentonite

  • Park, Tae-Jin;Seoung, Donghoon
    • Nuclear Engineering and Technology
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    • 제53권5호
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    • pp.1511-1518
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    • 2021
  • In most countries, the thermal criteria for the engineered barrier system (EBS) is set to below 100 ℃ due to the possible illitization in the buffer, which will likely be detrimental to the performance and safety of the repository. On the other hand, if the thermal criteria for the EBS increases, the disposal density and the cost-effectiveness for the high-level radioactive wastes will dramatically increase. Thus, fundamentals on the thermal behavior of the buffer under the elevated temperatures is of crucial importance. Yet, the behaviors at the elevated temperatures of the bentonite under groundwater-saturated conditions have not been reported to-date. Here, we have developed an in-situ synchrotron-based method for the thermal behavior study of the buffer under the elevated temperatures (25-250 ℃), investigated dspacings of the montmorillonite in the Korean bentonite (i.e., Ca-type) at dry and KURT (KAERI Underground Research Tunnel) groundwater-saturated conditions (KJ-ii-dry and KJ-ii-wet), and compared the behaviors with that of MX-80 (i.e., Na-type, MX-80-wet). The hydration states analyzed show tri-, bi-, and mono-hydrated at 25, 120, and 250 ℃, respectively for KJ-ii-wet, whereas tri-, mono-, and de-hydrated at 25, 150, and 250 ℃, respectively for MX-80-wet. The Korean bentonite starts losing the interlayered water at lower temperatures; however, holds them better at higher temperatures as compared with MX-80.

Double Cantilever Beam 방법을 이용한 다결정 알루미나의 Bridging 응력효과 해석 III. 다결정 알루미나의 Bridging 응력분포 (Analysis of bridging Stress Effect of Polycrystlline Aluminas Using Double Cantilever Beam Method)

  • 손기선;이성학;백성기
    • 한국세라믹학회지
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    • 제33권5호
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    • pp.602-615
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    • 1996
  • The purpose of the present study is to investigate the microstructural effect on the R-curve behavior in three aluminas with different grain size distributions by analyzing the bridging stress distribution. The crack opening displacement (COD) according to the distance behind the stationary crack tip was measured using an in situ SEM fracture method. The measured COD values in the fine-grained alumina agreed well with Wiederhorn's sollution while they deviated from Wiederhorn's solution in the two coarse-grained aluminas because of the increase of the crack closure due to the grain interface bridging in the crack wake. A numerical fitting procedure was conducted by the introduction of the power-law relation and the current theoretical model together with the measured COD's in order to obtain the bridging stress distribution. The results indicated that the bridging stress function and the R-curve computed by the current model were consistent with those computed by the power-law relation providing a reliable evidence for the bridging stress analysis of the current model. The strain-softening exponent in the power-law relation n, was calculated to be in the range from 2 to 3 and was closely related to the grain size distribution. Thus it was concluded from the current theoretical model that the grain size distribution affected greatly the bridging stress distribution thereby resulting in the quantitative analysis of microfracture of polycrystalline aluminas through correlating the local-fracture-cont-rolling microstructure.

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Determination of HER2 Gene Amplification in Breast Cancer using Dual-color Silver Enhanced in situ Hybridization (dc-SISH) and Comparison with Fluorescence ISH (FISH)

  • Unal, Betul;Karaveli, Fatma Seyda;Pestereli, Hadice Elif;Erdogan, Gulgun
    • Asian Pacific Journal of Cancer Prevention
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    • 제14권10호
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    • pp.6131-6134
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    • 2013
  • Background: The two basic methods that are currently accepted to identify the HER2 status are immunohistochemistry and flyorescence in situ hybridization (FISH). The aim of this study was to perform the dual-color silver in situ hybridization (dc-SISH) technique as an alternative to FISH. Materials and Methods: A total of 40 invasive breast carcinoma cases were assessed for HER2 gene amplification by FISH and dual-color SISH. Results: Significant correlation was found in the HER2 expression results obtained with the two approaches (p=0.001, p<0.05). The concordance rate was 92.3%. Conclusions: Foutine practical use of the dc-SISH method, which is much easier to apply, score, and evaluate, has many advantages. HER2 and CEN17 status can be evaluated simultaneously with the newly developed "Dual-Color Probe". All these specifications and the reliable results obtained support the widespread use of SISH technique in clinical practice.

암반균열망-개별요소법 수치실험을 통해 살펴본 스웨덴 포쉬마크지역 암반의 역학적 및 수리적 물성에 초기응력이 미치는 영향 (The DFN-DEM Approach Applied to Investigate the Effects of Stress on Mechanical and Hydraulic Rock Mass Properties at Forsmark, Sweden)

  • 민기복;우베 스테판손
    • 터널과지하공간
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    • 제21권2호
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    • pp.117-127
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    • 2011
  • 균열암반의 역학적 및 수리적 성질에 암반 초기응력이 미치는 영향을 고찰하였다. 지질 데이터는 스웨덴 원전원료 및 방사성 폐기물 관리회사(SKB)에 의해 수행된 포쉬마크지역의 부지조사로부터 획득되었으며 암반균열망-개별요소법 수치실험(Discrete Fracture Network - Discrete Element Method) 을 통하여 암반의 등가역학적 및 등가수리적 물성을 결정하였다. 수치실험결과 균열 강성의 응력의존성, 균열 방향에 따른 상이한 변형거동, 균열거동에 따른 수리유동 경로의 변화 등의 원인에 의하여 등가역학적 및 등가수리적 물성은 응력의존성이 큰 것을 확인하였다. 본 연구의 결과는 암반 초기응력의 정확한 예측이 특정 부지에서의 경계조건으로서뿐만 아니라 균열암반의 역학적 및 수리적 물성을 이해하는 데도 중요한 역할을 한다는 것을 보여준다.