• Title/Summary/Keyword: hot-pressing time

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Improvement of two stage sintering method by using graphite mould (Graphite mould의 사용에 의한 2단소성법의 개선에 관한 연구(투명 PLZT를 제작함에 있어서))

  • Park, Il-Kyu;Lee, Jae-Yeol;Paik, Dong-Su;Lee, Kae-Myung;Park, Chang-Yup
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1988.05a
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    • pp.88-91
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    • 1988
  • In this paper, PLZT Ceramics were fabricated by two stage sintering method whose first stage vacuum hot pressing and second stage PbO atmosphere sintering. Using Graphite Mould instead of Alumina Mould in first stage prevented the adhision between PLZT substrate and the mould. The grain sizes of PLZT Ceramics were controlled by varying the hot pressing time and second sintering time.

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Cold Rolling Process for the Matrix Fabrication of the Mcfc (용융탄산염형 연료전지의 전해질 매트릭스에 관한 연구)

  • Park, Sang-Kill;Rho, Chang-Joo
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.27 no.2
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    • pp.125-131
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    • 1991
  • Electrolyte matrix fabrication process can be classifed as hot pressing, tape casting, callendering, electrophoretic deposition. however, these have limits in practice. Hot pressing is cumbersome method, because of careful heating and cooling. Furthermore, the perfected tile is so fragile that it is difficult to fit in a cell. Therefore this method is not adequate for mass production of the electrolyte matrix. Using electrophoretic deposition method, a very thin matrix can be made, but many attempts of the electrolyte embeding were found to be failure. Tape casting and callendering methods are employed in most of the matrix fabrication for the present. But these methods require lots of water as a solvent, so that coating of the LiAlO sub(2) with electrolyte is difficult. Recently, hot roll milling method has been developed and the perfected matrix was proved to be free from crack. The method, however, needs a roller to make a matrix and a perfected matrix is carefully striped off from the cooled roller. Therefore, this method requires a long time due to the cooling process. The author proposes a cold rolling process. On this method, heated slurry of the LiAlO sub(2) mixed with binder, is rolled with a cold roller. The heated slurry dose not adhere to the roller, since contacted hot slurry is rapidly solidified. Therefore fabrication speed is increased, without getting rid of merits of the hot rolling process.

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Thermoelectric Properties of the (Pb$_{1-x}$Sn/$_{x}$)Te Sintered by AC Applied Hot Pressing (AC 통전식 Hot Press 법에 의해 제조된 (Pb$_{1-x}$Sn/$_{x}$)Te 열전반도체의 물성)

  • 신병철;황창원;오수기;최승철;백동규
    • Journal of the Microelectronics and Packaging Society
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    • v.7 no.4
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    • pp.1-5
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    • 2000
  • Properties of AC applied hot pressed ($Pb_{1-x}Sn_{x}$) Te thermoelectrics were investigated. Mechanical alloying process used to produce alloyed powder to reduce the inhomogeneity and to avoid vaporization of constituents. It showed an increase in the mechanical alloying time with increasing of Sn contents in ($Pb_{1-x}Sn_{x}$)Te. ($Pb_{1-x}Sn_{x}$)Te were sintered at 873 to 923K for 1-4 minutes, under 150 kgf/$\textrm{cm}^2$ by AC applied hot pressng method. The short sintering time of AC applied hot pressing process could reduce the vaporization of Te. The density of ($Pb_{1-x}Sn_{x}$) Te was more dependent on the sintering temperature than the sintering time. The p-n transition was observed at x=0.1 but only p type conduction behavior was observed at more than 20 mol% of Sn compositions. The maximum value of Seebeck coefficient is 250 $\mu$V/K for x=0.2 at 500K. As the amount of Sn increases, the peak value of Seebeck coefficient drops and shifts to higher temperature and the peak value of electrical conductivity decreased with increasing temperature.

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Research on Two Sintered Techniques of Nanometer WC-Co Powder

  • Sun, Lan;Jia, Chengchang;Tang, Hua
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.529-530
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    • 2006
  • This paper concerned with SPS (spark plasma sintering), hot pressing of sinter nanometer WC-Co powder and discussed the density, hardness, microstructures and grain sizes of the alloys sintered. The results showed that the two sintered techniques could produce high density alloys and play well on the grain growth, but SPS could lower the sintering temperature and shorten sintering time. Besides, the hardness of the sintered cemented alloys that was dependent on the grain size and densification could also be improved.

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Development of Rice Hull Insulation Board using Urea Formaldehyde Resin (요소수지(尿素樹脂) 연질(軟質) 왕겨보드의 개발(開發))

  • Lee, Hwa-Hyoung;Kang, Chun-Won
    • Journal of the Korean Wood Science and Technology
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    • v.26 no.4
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    • pp.50-55
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    • 1998
  • This study was carried out to develop low density board made of rice hull which needs proper use. Urea formaldehyde adhesive(UF) was used. The raw materials were the mixtures of the rice hulls from IllFum, DongGin, ChuChong, etc. The physical and mechanical properties of rice hull insulation board were examined. The results are as follows : For the thickness of 15mm of the low density rice hull board bonded with UF resin, proper manufacturing conditions were $171^{\circ}C$ of hot pressing temperature with thickness bar for optimum density, 12 percent of resin solid contents of rice hull ovendry weight, and 20 minutes of hot pressing time. These conditions meet Korean standards(KS 3201-1982) in relation to free formaldehyde emission, bending strength, water absorption and heat resistance.

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Development of New Micro Pattern Fabrication Process by U sing Isostatic Pressing (정수압을 이용한 미세 패턴 전사 신공정 개발)

  • Seol, J.W.;Joo, B.Y.;Rhim, S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.267-270
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    • 2009
  • In the present investigation, we are newly developing a new forming process which can fabricate micro patterns on large-area polymeric substrates for high speed mass production. The key idea of the new process is to pressurize multiple vacuum-packed substrate-mold stacks above the glass transition temperature ($T_g$) of the polymeric substrates. The new process is thought to be promising micro-pattern fabrication technique in three aspects; firstly, isostatic pressing ensures the uniform micro-pattern replicating condition regardless of the substrate area. Secondly, the control of forming condition such as temperature and pressure can realize well-defined process condition exploited in the conventional hot embossing research field. Thirdly, multiple substrates can be patterned at the same time. A prototype forming machine for the new process was developed with the design consideration realizing the present idea. With a developed machine, micro prismatic array patterns with 50 um in size were successfully made on the $380{\times}300{\times}6\;mm$ PMMA plate.

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Phase Transformation During Hot Consolidation and Heat Treatments in Mechanically Alloyed Iron Silicide (기계적 합금화 Iron Silicide의 열간성형 및 열처리에 의한 상변화)

  • Eo, Sun-Cheol;Kim, Il-Ho;Hwang, Seung-Jun;Jo, Gyeong-Won;Choe, Jae-Hwa
    • Korean Journal of Materials Research
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    • v.11 no.12
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    • pp.1068-1073
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    • 2001
  • An n-type iron$silicide(Fe_{0.98}Co_{0.02}Si_2)$has been produced by mechanical alloying process and consolidated by vacuum hot pressing. Although as-milled powders after 120 hours of milling did not show an alloying progress,${\beta}-FeSi_2$phase transformation was induced by isothermal annealing at$830{\circ}C$for 1 hour, and the fully transformed${\beta}-FeSi_2$phase was obtained after 4 hours of annealing. Near fully dense specimen was obtained after vacuum hot pressing at$ 1100{\circ}C$with a stress of 60MPa. However, as-consolidated iron silicides were consisted of untransformed mixture of ${\Alpha}-Fe_2Si_5$and ${\varepsilon-FeSi$phases. Thus, isothermal annealing has been carried out to induce the transformation to a thermoelectric semiconducting${\beta}-FeSi_2$phase. The condition for${\beta}-FeSi_2$transformation was investigated by utilizing DTA, SEM, and XRD analysis. The phase transformation was shown to be taken place by a vacuum isothermal annealing at$830{\circ}C$and the transformation behaviour was investigated as a function of annealing time. The mechanical properties of${\beta}-FeSi_2$materials before and after isothermal annealing were characterized in this study.

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Coarsening of Dispersoid and Matrix Phase in Mechanically Alloyed ODS NiAl (기계적 합금화된 ODS NiAl에서 분산상 및 기지상의 조대화 거동)

  • 어순철
    • Journal of Powder Materials
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    • v.4 no.1
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    • pp.48-54
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    • 1997
  • NiAl powders containing oxide dispersoids have been produced by mechanical alloying process in a controlled atmosphere using high energy attrition mill. The powders have been consolidated by hot extrusion and hot pressing followed by isothermal annealing to induce microstructure coarsening to improve high temperature properties. Grain growth and dispersoid coarsening kinetics have been investigated as functions of annealing time and temperature. Coarsening of dispersion strengthen NiAl and dispersoid has been discussed. Some clues of secondary recrystallization have been investigated. Mechanical property measurements have been also made and correlated with the microstructures.

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Effect of Hot Isostatic Pressing on Elimination of Internal Defects in IN738LC Superalloy for Gas Turbine Blade (HIP 처리에 의한 가스터빈 블레이드용 IN738LC 초합금의 내부결함 소멸 효과)

  • Park, Young-Kyu;Kim, Soo-Hyung;Kim, Jae-Cheol;Lee, Young-Chan;Kim, Doo-Soo;Choi, Cheol;Kim, Gil-Moo
    • Journal of Korea Foundry Society
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    • v.19 no.5
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    • pp.427-432
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    • 1999
  • Most investment castings contain some porosities and microcavities. In this study, we investigated the elimination trends of various internal defects in IN738LC investment castings for industrial gas turbine blade by hot isostatic pressing. The results showed that cylindrical defects which are under $0.6mm{\Phi}{\times}7mm$ size are mostly eliminated and aspect ratio of defects is more sensitive factor than their cross section shape in removing these defects. Increasing hot isostatic pressure and holding time doesn't affect the elimination trend of cylindrical defects over $0.6mm{\Phi}{\times}7mm$ size because first step(plastic deformation) of HIP densification doesn't occur under these HIPping conditions.

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Electrical Current Applied Hot Pressing Processing of $Bi_2Te_3$- $Bi_2Se_3$ Thermoelectrics

  • Park, S.C.;D.G.Baik;Hwang, C.W.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06a
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    • pp.516-518
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    • 1996
  • Bimuth telluride type thermoelectrics are prepared by AC current applied got pressing method. It is possible to minimize the defects arising from the vaporization of Te, because of the very short processing time. The optimum conditions for the got pressing of 95mol% $Bi_2Te_3$-5mol%$Bi_2Se_3$ themoelectrics are sintered at $400^{\circ}C$, for 2min. with 1500 kgf/$cm^2$ from the particle size of 125 to 250 $\mu$m rang of powder. the resulted Z value (figure of merit) was 2.2$\times$10-3deg-1.

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