• Title/Summary/Keyword: high pressure-temperature

Search Result 4,141, Processing Time 0.028 seconds

Simultaneous Consolidation of Titanium Diboride with Self-Propagating High-Temperature Synthesis, Direct Contact-Heating, and Pressure: Modeling of Temperature Distribution and the Relationship between Applied Energy and Densification ($TiB_2$ SHS 및 직접 접촉가열에 의한 동시 가압법 : 온도분포 모델링 및 공급에너지와 치밀화 관계)

  • Chung, G.K.;Cho, K.;Lee, H.B.
    • Journal of the Korean Ceramic Society
    • /
    • v.32 no.7
    • /
    • pp.817-824
    • /
    • 1995
  • TiB2 was simultaneously synthesized and densified with concurrent self-propagating high-temperature synthesis and direct contact-heating by electrcial power input and pressure. Density of TiB2 synthesized by self-propagating high-temperature synthesis and consolidated simultaneously by direct contact-heating and pressure was maximum 80% of the theoretical density (4.52g/㎤). Temperature profile was analyzed by solving heat balance equation with numerical method (FTCS method). The temperature of the sample was sufficiently raised to that temperature sufficient to be densified. It was ascertained that the density of the SHS synthesized TiB2 is exponentially proportinal to the input thermal energy per mass.

  • PDF

Effect of High Temperature and Pressure Conditions on the Combustion Characteristics of n-butanol and n-heptane Fuel (고온, 고압의 분위기 변화가 n-butanol 및 n-heptane 연료의 연소 특성에 미치는 영향)

  • Lim, Young Chan;Suh, Hyun Kyu
    • Journal of ILASS-Korea
    • /
    • v.21 no.1
    • /
    • pp.29-36
    • /
    • 2016
  • The effect of high ambient temperature and pressure conditions on the combustion performance of n-butanol, n-heptane and its mixing fuel (BH 20) were studied in this work. To reveal this, the closed homogeneous reactor model applied and 1000-1200 K of the initial temperature, 20-30 atm of initial pressure and 1.0 of equivalence ratio were set to numerical analysis. It was found that the results of combustion temperature was increased and the ignition delay was decreased when the ambient conditions were elevated since the combustion reactivity increased at the high ambient conditions. On the contrary, under the low combustion temperature condition, the combustion pressure was more influenced by the ambient temperature in the same ambient conditions. In addition, the total mass and the mass density of tested fuels were influenced by the ambient pressure and temperature. Also, soot generation of mixing fuel was decreased than n-heptane fuel due to the oxygen content of n-butanol fuel.

Oxide Layer Growth in High-Pressure Steam Oxidation (고압 수증기 내에서 산화막 형성에 관한 연구)

  • 박경희;안순의;구경완;왕진석
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2000.07a
    • /
    • pp.735-738
    • /
    • 2000
  • This paper shows experimentally that oxide layer on the p-type Si-substrate can grow at low temperature(500$^{\circ}C$∼600$^{\circ}C$) using high pressure water vapor system. As the result of experiment, oxide layer growth rate is about 0.19${\AA}$/min at 500$^{\circ}C$, 0.43${\AA}$/min at 550$^{\circ}C$, 1.2${\AA}$/min at 600$^{\circ}C$ respectively. So, we know oxide layer growth follows reaction-controlled mechanism in given temperature range. Consequently, granting that oxide layer growth rate increases linearly to temperature over 600$^{\circ}C$, we can expect oxide growth rate is 5.2${\AA}$/min at 1000$^{\circ}C$. High pressure oxidation of silicon is particularly attractive for the thick oxidation of power MOSFET, because thermal oxide layers can grow at relatively low temperature in run times comparable to typical high-temperature, 1 atm conditions. For higher-temperature, high-pressure oxidation, the oxidation time is reduced significantly

  • PDF

Fabrication and Characterization of High Temperature Electrostatic Chucks

  • Bang, Jae-Cheol
    • The Korean Journal of Ceramics
    • /
    • v.5 no.1
    • /
    • pp.87-90
    • /
    • 1999
  • It was suggested that tape casting method can be used to fabricate high-temperature electrostatic chucks(HTESC) based on a metal substrate coated with a glass-ceramic insulating layer. The adhesion of the coating was excellent such that it was able to withstand temperature cycling to over $300^{\circ}C$ without spalling. The electrostatic clamping pressure reached a very high value of about 9 torr at 600V and generally followed the theoretical voltage-squared curve. Based on these results, we believe that we successfully developed a viable technique for manufacturing low cost HTESC.

  • PDF

The Influence of Pressure, Temperature, and Addition of CO2 on the Explosion Risk of Propylene used in Industrial Processes

  • Choi, Yu-Jung;Choi, Jae-Wook
    • Korean Chemical Engineering Research
    • /
    • v.58 no.4
    • /
    • pp.610-617
    • /
    • 2020
  • In process installations, chemicals operate at high temperature and high pressure. Propylene is used as a basic raw material for manufacturing synthetic materials in the petrochemical industry; However, it is a flammable substance and explosive in the gaseous state. Thus, caution is needed when handling propylene. To prevent explosions, an inert gas, carbon dioxide, was used and the changes in the extent of explosion due to changes in pressure and oxygen concentration at 25 ℃, 100 ℃, and 200 ℃ were measured. At constant temperature, the increase in explosive pressure and the rates of the explosive pressure were observed to rise as the pressure was augmented. Moreover, as the oxygen concentration decreased, the maximum explosive pressure decreased. At 25 ℃ and oxygen concentration of 21%, as the pressure increased from 1.0 barg to 2.5 bar, the gas deflagration index (Kg) increased significantly from 4.71 barg·m/s to 18.83 barg·m/s.

ANALYSIS OF PRESTRESSED CONCRETE CONTAINMENT VESSEL (PCCV) UNDER SEVERE ACCIDENT LOADING

  • Noh, Sang-Hoon;Moon, Il-Hwan;Lee, Jong-Bo;Kim, Jong-Hak
    • Nuclear Engineering and Technology
    • /
    • v.40 no.1
    • /
    • pp.77-86
    • /
    • 2008
  • This paper describes the nonlinear analyses of a 1:4 scale model of a prestressed concrete containment vessel (PCCV) using an axisymmetric model and a three-dimensional model. These two models are refined by comparison of the analysis results and with testing results. This paper is especially focused on the analysis of behavior under pressure and the temperature effects revealed using an axisymmetric model. The temperature-dependent degradation properties of concrete and steel are considered. Both geometric and material nonlinearities, including thermal effects, are also addressed in the analyses. The Menetrey and Willam (1995) concrete constitutive model with non-associated flow potential is adopted for this study. This study includes the results of the predicted thermal and mechanical behaviors of the PCCV subject to high temperature loading and internal pressure at the same time. To find the effect of high temperature accident conditions on the ultimate capacity of the liner plate, reinforcement, prestressing tendon and concrete, two kinds of analyses are performed: one for pressure only and the other for pressure with temperature. The results from the test on pressurization, analysis for pressure only, and analyses considering pressure with temperatures are compared with one another. The analysis results show that the temperature directly affects the behavior of the liner plate, but has little impact on the ultimate pressure capacity of the PCCV.

Forming Characteristics with Cavity Pressure and Temperature Signal Inside Mold in High-Pressure Resin Transfer Molding Process of Carbon Fiber Reinforced Composite Material (탄소섬유강화복합소재의 고압수지이송성형공정에서 금형 내 캐비티의 압력 및 온도신호에 따른 성형특성)

  • Han, Beom-Jeong;Jeong, Yong-Chai;Kim, Sung-Ryul;Kim, Ro-Won;Kang, Myung Chang
    • Journal of the Korean Society of Manufacturing Process Engineers
    • /
    • v.16 no.6
    • /
    • pp.81-86
    • /
    • 2017
  • The high-pressure resin transfer molding (HP-RTM) process has a very effective for the mass production of carbon fiber reinforced plastic (CFRP) for light weight in the automotive industry. In developing robust equipment, new process and fast cure matrix systems reduces significantly the cycle time less than 5 minutes in recent years. This paper describes the cavity pressure, temperature and molding characteristics of the HP-RTM process. The HP-RTM mold was equipped with two cavity pressure sensors and three temperature sensors. The cavity pressure characteristics of the HP-RTM injection, pressurization, and curing processes were studied. This experiment was conducted with selected process parameters such as mold cap size, maximum press force, and injection volume. Consequently, this monitoring method provides correlations between the selected process parameters and final forming characteristics in this work.

Characteristics of polycrystalline 3C-SiC micro pressure sensors for high temperature applications (초고온용 다결정 3C-SiC 마이크로 압력센서의 특성)

  • Thien, Duong Xuan;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2008.06a
    • /
    • pp.387-388
    • /
    • 2008
  • High temperature micro pressure sensors were fabricated by polycrystalline (poly) 3C-SiC piezoresistors formed by oxidized SOI substrates with APCVD. These have been designed by bulk micromachining below $1{\times}1mm^2$ diaphragm and Si membrane $20{\mu}m$ thick. The pressure sensitivity of fabricated pressure sensor was 0.1 mV/Vbar. The non-linearity of sensor was ${\pm}0.44%$ FS and the hysteresis was 0.61% FS.TCS of pressure sensor was -1867 ppm/$^{\circ}C$, its TCR was -792 ppm/$^{\circ}C$, and TCGF to 5 bar was -1042 ppm/$^{\circ}C$ from 25 to $400^{\circ}C$.

  • PDF

Evaluation on High Temperature Fracture toughness of Pressure Vessel SA516/70 Steel (압력용기용 SA516/70강의 고온파괴인성평가)

  • 박경동;김정호;윤한기;박원조
    • Journal of Ocean Engineering and Technology
    • /
    • v.15 no.2
    • /
    • pp.99-104
    • /
    • 2001
  • Elastic-plastic fracture toughness $J_{lc}$ can be used as an effective design criterion in elastic plastic fracture mechanics. Most of these systems are$J_{lc}$ $J_{lc}$ value at high temperature must be determined for use of integrity evaluation and designing of such systems. Elastic-plastic fracture toughness $J_{lc}$ tests were performed on SA516/70 carbon steel plate and test results were analyzed according to ASTM E 813-87, ASTM E 813-89 and ASTM E 1152-87.safety and integrity are required for reactor pressure vessels because, they are operated in high temperature. There are single specimen method, which used as evaluation of safety and integrity for reactor pressure vessels. In this study, elastic-plastic fracture toughness($J_{lc}$) and J-$\Delta$a of SA 516/70 steel used as reactor pressure vessel steel are measured and evaluated at room temperature, 150$^{\circ}C $, 250$^{\circ}C $ and 370$^{\circ}C $ according to unloading compliance method.

  • PDF

Optimization of Subcritical Water Hydrolysis of Rutin into Isoquercetin and Quercetin

  • Kim, Dong-Shin;Lim, Sang-Bin
    • Preventive Nutrition and Food Science
    • /
    • v.22 no.2
    • /
    • pp.131-137
    • /
    • 2017
  • Maximum production of isoquercetin and quercetin simultaneously from rutin by subcritical water hydrolysis (SWH) was optimized using the response surface methodology. Hydrolysis parameters such as temperature, time, and $CO_2$ pressure were selected as independent variables, and isoquercetin and quercetin yields were selected as dependent variables. The regression models of the yield of isoquercetin and quercetin were valid due to the high F-value and low P-value. Furthermore, the high regression coefficient indicated that the polynomial model equation provides a good approximation of experimental results. In maximum production of isoquercetin from rutin, the hydrolysis temperature was the major factor, and the temperature or time can be lower if the $CO_2$ pressure was increased high enough, thereby preventing the degradation of isoquercetin into quercetin. The yield of quercetin was considerably influenced by temperature instead of time and $CO_2$ pressure. The optimal condition for maximum production of isoquercetin and quercetin simultaneously was temperature of $171.4^{\circ}C$, time of 10.0 min, and $CO_2$ pressure of 11.0 MPa, where the predicted maximum yields of isoquercetin and quercetin were 13.7% and 53.3%, respectively. Hydrolysis temperature, time, and $CO_2$ pressure for maximum production of isoquercetin were lower than those of quercetin. Thermal degradation products such as protocatechuic acid and 2,5-dihydroxyacetophenone were observed due to pyrolysis at high temperature. It was concluded that rutin can be easily converted into isoquercetin and quercetin by SWH under $CO_2$ pressure, and this result can be applied for SWH of rutin-rich foodstuffs.