• Title/Summary/Keyword: heat treatment processing

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CO Sensor Characteristics of ZnO powders by Sol-Gel methods (Sol-Gel법에 의한 ZnO 분말의 CO 센서 특성)

  • Park, Bo-Seok;Park, Jin-Seoung;Noh, Whyo-Sub
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.821-825
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    • 2002
  • ZnO thick films by Sol-Gel processing were investigated electrics, optics and the sensing characteristics of CO gas. Using the znic acetate dihydrate and acetylaceton (AcAc) as a chelating agent, stable ZnO sol was synthesized. ZnO phase was crystallized through the heat-treatment at $70^{\circ}C$ for 4hrs and influenced the sensing characteristics of the electrics and CO gas by uniform particle distributions not related particle size. The samples on the alumina substrate by thick films were investigated the properties of electrics and the effect of sensing. The sensitivity was so excellent in the sample of the heat-treatment at $600^{\circ}C$ for 12hrs and good in the heat-treatment for 1hrs generally. Crystallization and volatilization of organic materials according to the change of heating treatment temperature of thick films were analyzed by TG-DTA, XRD and mirostructure of thick films were observed by SEM.

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Fabrication of Titanium alloy by Electromagnetic Continuous Casting (EMCC) Method for Medical Applications (전자기 연속 주조법을 이용한 의료용 타이타늄 합금 제작에 관한 연구)

  • Choi, Su-Ji;Lee, Hyun-Jae;Baek, Su-Hyun;Hyun, Soong-Keun;Jung, Hyun-Do;Moon, Byung-Moon
    • Journal of Korea Foundry Society
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    • v.38 no.1
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    • pp.9-15
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    • 2018
  • Electromagnetic continuous casting (EMCC) was used to fabricate Ti-6Al-4V alloys with properties suitable for medical applications. Ti-6Al-4V alloy ingots fabricated by EMCC were subjected to heat treatment, such as residual stress removing (RRS), furnace cooling after solution treatment (ST-FC) and water-cooling after solution treatment (ST-WC), in order to obtain characteristics suitable for the standard. After component analysis, the microstructure and mechanical properties (tensile strength and elongation) were evaluated by ICP, gas analysis, OM, SEM, a Rockwell hardness tester and universal testing machine. The Ti-6Al-4V alloy ingot fabricated by EMCC was fabricated without segregation, and the lamellar structure was observed in the RRS and ST-FC specimens. The ST-WC specimen showed only martensite structure. As a result of evaluating the mechanical properties based on the microstructure results, we found that the water-cooled heat treatment condition after the solution treatment was most suitable for the Ti-6Al-4V ELI standard.

A Study on Mechanical Properties of Micro-Alloyed Steel According to Baking Temperature (베이킹 온도에 따른 비조질강 기계적 특성)

  • Lee, S.H.;Lee, K.T.;Kwon, Y.N.;Kim, J.H.
    • Transactions of Materials Processing
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    • v.15 no.8 s.89
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    • pp.621-627
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    • 2006
  • Recently, micro-alloyed steels which could eliminate heat treatments after forging has been developed. These non heat-treated micro-alloyed steels have several advantages over the conventional quenched and tempered steel for cold forging. First of all, long components can be fabricated with a better dimensional accuracy since bending of long forged part after quenching treatment could be avoided. And it is possible to eliminate two energy consuming heat treatment steps, which are a spherodizing before forging and quenching/tempering after forging. Therefore, more cost effective and environment friendly process could be designed. However, there is non-uniform distribution of strain occurred across the forged part, since these non heat-treated micro-alloyed steel use strain hardening mechanism. In the present study, it was investigated how to lessen non-uniformity and increase strength together for cold forging when a baking heat treatment is applied in micro-alloyed steels. For this purpose, micro-alloyed steels developed by Se-A Besteel recently was used for the experiment.

Evolution of Microstructure and Mechanical Properties of Porous Al Alloy Under Various Heat Treatment (열처리에 따른 다공성 알루미늄 합금 재료의 미세구조와 기계적 성질 변화)

  • 류관무;권영재;김준규;조원승;조남희;황진명;유연철
    • Transactions of Materials Processing
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    • v.12 no.6
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    • pp.588-596
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    • 2003
  • The relationships between evolution of microstructure and mechanical properties of porous Al-3Si-2Mg-2Cu alloy after the foaming and various heat treating were investigated. The foamed alloy having various densities were manufactured by powder compact foaming and heat treated. Then compression test was performed with deformation rate of 0.5/s. The ultimate compression strength was not changed after solution heat treatment but the flow curve after ultimate strength showed very smooth and uniform plateau region. This change of flow curve means that the deformation mechanism is altered from brittle fracture to ductile deformation and the energy absorption property of Al foam is dramatically improved. The improvement of energy absorption without any detriment of mechanical properties is due to that the very brittle precipitation like Al-Cu and Al-Mg was uniformly dissolved in Al matrix after solution heat treatment. And various mechanical properties of Al alloy porous material were improved by 40% with aging of $200^{\circ}C$ and 50min. These improvements are ascribe to the various fine precipitates like $\Omega$ and $\theta$'.

The Effect of Isothermal Annealing on Microstructure of Forged Parts (단조품의 등온 어닐링에 따른 미세조직 변화)

  • Kim, D.B.;Lee, J.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.5
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    • pp.303-308
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    • 2000
  • The ring gears of automobile parts are manufactured generally process chart of which is as follows : forging ${\rightarrow}$ annealing or normalizing ${\rightarrow}$ rough machining ${\rightarrow}$ hardening(Quenching-Tempering or carburizing process) ${\rightarrow}$ finish machining. Isothermal annealing process after forging is most effective in the side of improvment of machinability. On this study we selected two kinds of steel;SCM415, SCM435 of most universal and investigated microstructures to find out most suitable condition of heat treatment in proportion continuous cooling and isothermal annealing. As the cooling rate is $5^{\circ}C$ per minute in continuous cooling process, martensite and bainite are coexisted with ferrite and pearlite in SCM435 steel. If the cooling rate is slower than $5^{\circ}C$ per minute, microstructure were only ferrite and pearlite but formation of band structure can't be avoid. On the other hand, microstructure is only ferrite and pearlite regardless of cooling rate because carbon content of SCM415 steel is low. Moreover formation of band structure isn't exposed by faster cooling rate. Most optimal temperature of the isothermal annealing is from $650^{\circ}C$ to $680^{\circ}C$ in SCM435 steel. When holding time is 60 minute with $650^{\circ}C$, the identical ferrite and pearlite microstructures can be obtained.

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Hot Deformation Behavior of AISI 4340 using Constitutive Model and Processing Map (구성 모델과 공정 지도를 이용한 AISI 4340강의 고온 변형 거동)

  • Kim, Keunhak;Jung, Minsu;Lee, Seok-Jae
    • Journal of the Korean Society for Heat Treatment
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    • v.30 no.5
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    • pp.187-196
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    • 2017
  • High temperature flow behaviors of AISI 4340 steel were investigated using isothermal compression tests under the temperature range from 850 to $1100^{\circ}C$ and a strain rate from 0.01 to $10s^{-1}$. The flow stress decreased with increasing compression temperature and decreasing strain rate. The dynamic softening related to the dynamic recrystallization was observed during hot deformation. The constitutive model based on Arrheniustyped equation with the Zener-Hollomon parameter was used to simulate the hot deformation behavior of AISI 4340 steel. The modification of the Zener-Hollomon parameter and lnA parameter resulted in the improvement of the calculation accuracy of the proposed constitutive model compared with the experimental flow curves. In addition, the process map of AISI 4340 steel was proposed. The instable process condition for hot deformation was predicted and its reliability was verified with the experimental observation.

The Effect of Magnetic Property According to Size and Orientation of Crystal for Electroplated Co-Fe-Ni Alloys (전기 도금된 CoFeNi계 박막의 결정크기와 방향성이 자기특성에 미치는 영향)

  • Jeung, Won-Young;Kim, Hyun-Kyung;Park, Chang-Bean
    • Journal of the Korean Magnetics Society
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    • v.16 no.5
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    • pp.249-254
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    • 2006
  • CoFeNi alloys are some of the most studied soft magnetic materials because of their superial properties over FeNi alloys as write head core materials in HDD and MEMS. We studied the effect of magnetic property according to size and orientation of crystal for electroplated Co-Fe-Ni alleys. In case of heat treated ternary alloy, it affect the change of crystal size and structure. In this study, it intends to improve the magnetic properties of CoFeNi thin film by heat treatment. Minimized coercivity and increased magnetization are due to heat treatment from $300^{\circ}C\;to\;400^{\circ}C$. As a bcc phase formation, it grow to amount of magnetization.

A Study on Herbal Processing Terminology (본초(本草) 포제관련(炮製關聯) 용어(用語)에 대(對)한 연구(硏究))

  • Song, Ji-Chung;Shim, Hyun-A;Eom, Dong-Myung
    • Journal of Society of Preventive Korean Medicine
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    • v.16 no.3
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    • pp.107-117
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    • 2012
  • Objective : Processing of medicinals are one of the most important part in medicinal treatment. However, in text books, there are disagreements and several terms with same meanings. Method : We tried to compare the processing of medicinals in text book, Bonchohak especially in exterior-releasing medicinal and heat-clearing medicinal. Results : The terms of processing of medicinals in introductions of text book, Bonchohak are different from those in an itemized discussion of exterior-releasing medicinal and heat-clearing medicinal. Conclusion : The terms of processing of medicinals in text book, Bonchohak should be reorganized and improved to make be clear and sure as a text book.

Comparison of Hardness and Damping Capacities of Mg-Al Alloy Subjected to T6 Heat Treatment and Low Temperature Long Term Isothermal Aging (T6 열처리 및 저온 장시간 등온 시효한 Mg-Al 합금의 경도 및 진동감쇠능 비교)

  • Joong-Hwan Jun
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.5
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    • pp.277-284
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    • 2023
  • Hardness and damping characteristics of fine discontinuous precipitates (DPs) microstructure generated by low temperature long term isothermal aging were investigated in comparison with those of T6 heat-treated microstructure composed of DPs and continuous precipitates (CPs) in Mg-9%Al alloy. In this study, T6 and fine DPs microstructures were obtained by isothermal aging at 453 K for 24 h and at 413 K for 336 h, respectively, after solution treatment at 693 K for 24 h. The DPs microstructure exhibited higher hardness than the T6 microstructure, which is related to the lower (α + β) interlamellar spacing of the DPs. The DPs microstructure possessed better damping capacity than the T6 microstructure in the strain-amplitude independent region, whereas in the strain-amplitude dependent region, the reverse behavior was observed. The damping tendencies depending on strain-amplitude were discussed based on the microstructural features of the T6 and DPs microstructures.