• Title/Summary/Keyword: heat cured

Search Result 180, Processing Time 0.023 seconds

A Study on the Heat-Curing of Acrylic Resin using Ring Furnace (Ring Furnace를 이용한 Acrylic Resin의 온성에 관한 연구)

  • Choi, Seog-Soon
    • Journal of Technologic Dentistry
    • /
    • v.13 no.1
    • /
    • pp.27-31
    • /
    • 1991
  • The purpose of this study was to evaluate the effect of curing time and curing temperature on the hear - Curing of acrylic resin using ring furnace. Specimens were fabricated from 2 kinds(Laboron, Bertex) heat-cured resin. Total 200 samples were divided into 4 groups(70$^{\circ}C$, 100$^{\circ}C$, 13$^{\circ}C$, 150$^{\circ}C$) and each group was divided into 5 small groups(30 min., 45min., 60min., 75min., 90min.). A microscope(Olympus Coll Co. Japan) was used to examine a randomly selected central zone, midzone and surface for each complete specimen. The results of the experiment were as follows : 1. To obtain non-polymerzation, cure the resin for 30 minutes at 70$^{\circ}C$ and 100$^{\circ}C$ in a ring furnace. 2. To obtain with porosity, cure the resin for 45 minutes, 60 minutes and 75 mintes at 70$^{\circ}C$ and for 90 minutes at 150$^{\circ}C$ in ring furnace. Porosity appears in Laboron for 30 minutes, 45 minutes at 150$^{\circ}C$ in a ring furnace. 3. Every other specimens connot get a sight of special problem with makes eye in the made surface.

  • PDF

Physical Properties of High-Solid Coatings with Acrylic Resins Containing Acetoacetoxy Group and HDI-Trimer (Acetoacetoxy기 함유 아크릴수지와 HDI-Trimer에 의한 하이솔리드 도료의 도막물성)

  • You, Hyuk-Jae;Chung, Dong-Jin;Hahm, Hyun-Sik;Park, Hong-Soo;Kim, Seong-Kil
    • Journal of the Korean Applied Science and Technology
    • /
    • v.20 no.3
    • /
    • pp.237-242
    • /
    • 2003
  • The high-solid coatings were prepared by blending the synthesized acrylic resin in the previous paper and hexamethylene diisocyanate-trimer and curing it at room temperature. The characterization of the films of the prepared coatings was performed. The impact resistance, $60^{\circ}C$ specular gloss, cross-hatch adhension, and heat resistance of the films proved to be good, and the pencil hardness and drying time proved to be slightly poor. Especially, there was a remarkable improvement in the heat resistance. This improvement may stem from the regular arrangement of ethyl groups introduced into the acrylic resin. From a viscoelastic measurement using a rigid-body pendulum, curing was accelerated with the $T_g$ value. With the increase in $T_g$, log damp value was lowered and dynamic viscoelasic $T_g$ of a cured film was increased.

Mechanical properties and adiabatic temperature rise of low heat concrete using ternary blended cement

  • Kim, Si-Jun;Yang, Keun-Hyeok;Lee, Kyung-Ho;Yi, Seong-Tae
    • Computers and Concrete
    • /
    • v.17 no.2
    • /
    • pp.271-280
    • /
    • 2016
  • This study examined the mechanical properties and adiabatic temperature rise of low-heat concrete developed based on ternary blended cement using ASTM type IV (LHC) cement, ground fly ash (GFA) and limestone powder (LSP). To enhance reactivity of fly ash, especially at an early age, the grassy membrane was scratched through the additional vibrator milling process. The targeted 28-day strength of concrete was selected to be 42 MPa for application to high-strength mass concrete including nuclear plant structures. The concrete mixes prepared were cured under the isothermal conditions of $5^{\circ}C$, $20^{\circ}C$, and $40^{\circ}C$. Most concrete specimens gained a relatively high strength exceeding 10 MPa at an early age, achieving the targeted 28-day strength. All concrete specimens had higher moduli of elasticity and rupture than the predictions using ACI 318-11 equations, regardless of the curing temperature. The peak temperature rise and the ascending rate of the adiabatic temperature curve measured from the prepared concrete mixes were lower by 12% and 32%, respectively, in average than those of the control specimen made using 80% ordinary Portland cement and 20% conventional fly ash.

Temperature History of the Concrete Corresponding to Various Curing Sheets in the Low Temperature (저온환경에서의 양생시트 변화에 따른 콘크리트의 온도이력 특성)

  • Baek, Dae-Hyun;Hong, Seak-Min;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 2008.11a
    • /
    • pp.781-784
    • /
    • 2008
  • In this paper, insulating effect and strength development of concrete under low temperature are reported varying curing sheets. According to test results, in temperature -5$^{\circ}$C concrete subject to exposure and air cap condition, result in a frost damage at early age by a fall of below zero temperature. Mean while, the combination of PE film and non-woven fabric maintained around 3 $^{\circ}$C within first 24 hours since placement. For double bubble sheets, concrete temperature maintained above 7$^{\circ}$C due to its excellent heat insulating capability. As a result of core strength test, strength of specimens cured with viny + non-woven fabric and double bubble sheets had higher strength than strength of other specimens due to good heat insulation effect at early age.

  • PDF

Thermal cracking assessment for nuclear containment buildings using high-strength concrete

  • Yang, Keun-Hyeok;Mun, Jae-Sung;Kim, Do-Gyeum;Chang, Chun-Ho;Mun, Ju-Hyun
    • Computers and Concrete
    • /
    • v.26 no.5
    • /
    • pp.429-438
    • /
    • 2020
  • To shorten the construction times of nuclear facility structures, three high-strength concrete mixtures were developed with specific consideration given to their curing temperatures, their economic efficiency, and the practicality of their quality control. This study was conducted to examine the temperature rise profiles of these three concrete mixtures and the potential for early-age thermal cracking in the primary containment vessel of a nuclear reactor with a wall thickness of 1200 mm. The one-layer placement height of the concrete for the primary containment vessel was increased from the conventional 3 m to 3.5 m. A nonlinear finite element analysis (FEA) was conducted using the thermal properties of concrete determined from the isothermal hydration and adiabatic hydration tests, and tuned through comparisons made with temperature rise profiles obtained for 1200-mm-thick mock-up wall specimens cured at temperatures of 5, 20, and 35℃. The hydration heat performance of the three concrete mixtures and their potential to produce thermal cracking in nuclear facilities indicate that the mixtures have considerable potential for practical application to the primary containment vessel of a nuclear reactor at various curing temperatures, fulfilling the minimum requirements of the ACI 301 and minimizing the likelihood of the occurrence of thermal cracks.

Optimum Curing and Full-out Velocity in the Rubber Extrusion Process for Electric Cable Manufacture (전선피복용 고무압출가공 공정의 최적 경화 및 선출 속도)

  • Kim, Duk-Joon;Choi, Sang-Soon;Kim, Tae-Ho
    • Elastomers and Composites
    • /
    • v.33 no.2
    • /
    • pp.93-102
    • /
    • 1998
  • In electric cable industries, the curing extent of the rubber materials covering the electric cores gives an significant effect on their final performance. The curing extent of rubber is controlled mostly by pull-out velocity of cable in the extrusion process. The final curing extent may be different for different radial positions inside the rubber because of the non-uniform temperature distributions during the curing process. In this contribution, the prediction of curing extent distribution throughout the radial direction of rubber is represented when the cable is passing through the steam curing zone with a fixed pull-out velocity. The prediction of the optimum pull-out velocity for the desired curing extent distribution is also reported. The steady-state heat balance was developed for the curing and cooling processes in which the pull-out rubber was cured by high temperature steam and then cooled by ambient water. A few essential material properties such as density, specific heat, and thermal conductivity were measured to analyze the temperature distribution during the curing and cooling processes. The times to reach 90% curing extent at varying temperatures were measured and used to determine the final cure extent distribution inside the rubber.

  • PDF

Physical Properties of High-Solid Coatings with Acrylic Resins Containing Caprolactone Group and HDI-Trimer (Caprolactone기 함유 아크릴수지와 HDI-Trimer에 의한 하이솔리드 도료의 도막물성)

  • Jo, Hye-Jin;Shim, Il-Woo;You, Hyuk-Jae;Wu, Jong-Pyo;Kim, Myung-Soo;Hahm, Hyun-Sik;Park, Hong-Soo;Baik, Woon-Phil
    • Journal of the Korean Applied Science and Technology
    • /
    • v.21 no.4
    • /
    • pp.300-305
    • /
    • 2004
  • High-solid coatings were prepared by blending of previosly synthesized acrylic resins and hexamethylene diisocyanate-trimer and curing it at room temperature. The characterization of the films of the prepared coatings was performed. The impact resistance, cross-hatch adhesion, $60^{\circ}$specular gloss, and heat resistance of the films proved to be good, and the pencil hardness and drying time proved to be slightly poor. Especially, there was a remarkable improvement in the heat resistance. This improvement may stem from the regular arrangement of ethyl groups introduced into the acrylic resin. As a result of Rigid-body pendulum visco-elasticity measurement, dynamic $T_g$ values of cured films increased with dynamic $T_g$ values.

Literatural study on the Causal Pathogenesis and Pathology of Kyeolhyung (결흉(結胸)의 병인병리에 대한 문헌적 고찰)

  • Jeon, Sang-Yun;Kim, Sung-Jin;Hong, Seok;Chung, Su-Mi;Han, Hong-Jun;Chung, Jong-An
    • Journal of Physiology & Pathology in Korean Medicine
    • /
    • v.20 no.6
    • /
    • pp.1442-1446
    • /
    • 2006
  • This study was wrriten in order to to help understanding of Kyeolhyung(結洶). Kyeolhyung is a syndrome of epigastric pain and fullness due to accumulation of pathogen in the chest mostly caused by too early purgation of Taiyang(太陽) channel syndrome which leads to the exterior syndrome of heat from the exterior into the interior or combines with the original excessive fluid of the chest. The knotted chest can be divided into large, small, heat and substantice, cold and substantice, water and blood Kyeolhyung. Kyeolhyung is basically treated by purgation but practically it is treated by according to its own symptom and syndromes. And we were cured of the Kyeolhyung discriminating from Zanggyul(藏結) and Bijeung(비증).

A multi Step Cure Process to Prevent Residual Bubbles in LED Encapsulation Silicone Resin (LED Encapsulation 실리콘의 기포잔류방지를 위한 Step 경화공정 연구)

  • Song, M.J.;Kim, H.K.;Yoon, G.S.;Kim, K.H.
    • Transactions of Materials Processing
    • /
    • v.21 no.2
    • /
    • pp.101-106
    • /
    • 2012
  • Generally, rapid cure reaction of LED encapsulation silicone resin causes serious defects in cured resin products such as warpage, residual bubbles, and reduced wettablility. In order to prevent residual bubbles in silicone resin, the step cure process was examined in the present paper. Three kinds of step cure processes were applied, and bubble-free phenomenon was observed. Most of the bubbles were removed under $70^{\circ}C$, the minimum temperature for activating cure reaction. In addition, degree of cure(DOC) and temperature distribution were predicted by using FEM analysis of heat transfer. It was concluded that maintaining cure temperature which provide a DOC under 0.5~0.6 effectively reduces residual bubbles.

Temperature History of Wall Concrete with Heat Insulating Curing Method Subjected to Severly Cold Climate (혹한온도 조건에서의 양생방법 변화에 따른 벽체 콘크리트의 온도이력 특성)

  • Son, Ho-Jung;Han, Sang-Yoon;Cheong, Sang-Hyeon;Ahn, Samg-Ku;Han, Cheon-Goo;Han, Min-Cheol
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2011.11a
    • /
    • pp.51-52
    • /
    • 2011
  • This study is to propose a curing method for a concrete wall structure under severe cold climate. The curing methods of using heated cable, heated panel and insulated form were applied. Results showed that the concrete cured by the heated cable resulted in the highest temperature history and the highest strength development at 28 days. Further, it is believed that the curing methods of the heated panel and insulated form are also recommendable for the resistance of the early frost damage on the concrete in practice.

  • PDF