• Title/Summary/Keyword: hard phase

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Structure of Ni and NiO Nanoparticles Observed by X-ray Coherent Diffraction Imaging

  • Kim, Chan;Kim, Yoon-Hee;Hamh, Sun-Young;Son, Jun-Gon;Khakurel, Krishna Prasad;Iqbal, Mazhar;Noh, Do-Young
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.542-543
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    • 2012
  • Coherent diffraction imaging (CDI) method using hard x-ray at 5.46 keV was applied to study assembly of Ni and Ni oxide nano structures formed on a Si3N4 membrane. Density distribution of Ni nano-particles was obtained quantitatively with about 15 nm lateral resolution by reconstructing images from the speckle diffraction pattern. In addition, reconstructed images of nickel oxide particles indicated that Ni atoms diffuse out during the oxidation process leaving pores inside the nickel oxide crust. Furthermore, we recognize that really weak phase object, less than 5 nm thickness of Ni residues, can be reconstructed due to the reference particles. We achieved quantitative information of nanometer sized materials and demonstrate the effect of reference particles by using hard x-ray coherent diffractive imaging method.

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Three-Phase Soft Switching Sinewave Inverter with Bridge Power Module Package Configurated Auxiliary Resonant AC Link Snubber

  • Iyomori Hisashi;Nagai Shin-ichiro;Shiraishi Kazuhiro;Ahmed Tarek;Eiji Hiraki;Mutsuo Nakaoka
    • Proceedings of the KIPE Conference
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    • 2003.07b
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    • pp.507-510
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    • 2003
  • This paper presents a novel prototype of tile three-phase bridge power block module type a auxiliary resonant AC link snubber circuit, which is effectively used for the three-phase voltage source type sinewave soft switching PWM inverter using IGBTs. Its operating principle Is described for current source load model, along with its practical design approach based on the simulation data. The performance evaluation of the three-phase voltage source type snewave soft switching PWM inverter incorporating a single three-phase bridge mo여le of active auxiliary resonant AC link snubber treated here Is illustrated, which is concerned with power duality efficiency power loss analysis. This inverter is discussed as compared with those of tile three-phase voltage source type sinewave hard switching PWM inverter. The power loss analysis of this soft switching PWM Inverter using IGBT power modules is evaluated on the basis of the measured v-i characteristics and switching power losses of IGBT, and antiparaliel diodes. The practical effectiveness of this inverter is proven by the power loss analysis for distributed power supply.

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Dispersity of CNT and GNF on the Polyurethane Matrix: Effect of Polyurethane Chemical Structure (폴리우레탄 분자구조 변화에 따른 CNT와 GNF의 분산특성 연구)

  • Im, Hyun-Gu;Kim, Hyo-Mi;Kim, Joo-Heon
    • Polymer(Korea)
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    • v.32 no.4
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    • pp.340-346
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    • 2008
  • The aim of this study is to understand the effect of structure on the dispersion of both CNT and GNF in the phase of synthesized polyurethanes matrix. Various CNT/PU and GNF/PU composite films were prepared. Polyurethane having a different hard segment was blended with both CNT and GNF. PU having HDI as hard segment showed good dispersion with both CNT and GNF because of their linear structural character and molecular kinesis while PU having aromatic ring showed poor dispersion with those due to their structural complexity. Structural effect also induced the increase of its electro conductivity. The PU/CNT composite showed a bad dispersion (because of phase separation between PU matrix and CNT) but good electro conductivity at its surface (because CNT was collected on the surface of composite film due to low density of CNT). PU/CNT and PU/GNF composite films have quite low normalized sheet resistance value compared with silver/PU nanocomposite film because the fiber type filler could have much more contact points than that of sphere shaped silver particles have.

Sliding Wear Mechanism of Ultra-Fine Grained Low Carbon Dual Phase Steel as n Function of Applied Load (결정립 미세화에 따른 이상조직 탄소강의 하중에 따른 마멸 기구)

  • Yu, H.S.;Yi, S.K.;Shin, D.H.;Kim, Y.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.421-424
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    • 2007
  • Dry sliding wear behavior of ultra-fine grained (UFG) plain low carbon dual phase steel, of which microstructure consists of hard martensite in a ductile ferrite matrix, has been investigated. The wear characteristics of the UFG dual phase steel was compared with that of a coarse grained dual phase steel under various applied load conditions. Dry sliding wear test were carried out using a pin-on-disk type tester at various loads of 1N to 100N under a constant sliding speed condition of 0.20m/s against an AISI 52100 bearing steel ball at room temperature. The sliding distance was fixed as 1000m for all wear tests. The wear rate was calculated by dividing the weight loss, measured to the accuracy of 10-5g by the specific gravity and sliding distance. The worn surfaces and wear debris were analyzed by SEM, EDS and profilometer. Micro-vickers hardness of the cross section of worn surfaces were conducted to analyze strain hardening underneath the contact surfaces. The wear mechanism of the UFG dual phase steel was investigated with emphasis on the unstable nature of the grain boundaries of the UFG microstructure.

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Carrier phase recovery algorithm for LDPC coded system (LDPC 코드를 이용한 위상 동기 알고리즘)

  • Lee Juhyung;Kim Namshik;Park Hyuncheol;Kim Pansu;Oh Dukgil;Lee Hojin
    • Proceedings of the IEEK Conference
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    • 2004.06a
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    • pp.43-46
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    • 2004
  • In this paper, we present a carrier phase estimation algorithm for LDPC coded systems. LDPC coded system can not achieve the ideal performance if phase offset is introduced by channel. However, the estimation of phase offset is very hard since the operating point of LDPC is very low SNR. To solve this problem, the algorithm using the tentative soft decision value and based on Maximum Likelihood (ML), was proposed in [2]. But this algorithm has problem which works only under constant phase offset. If phase offset is time variant, it has a severe degradation in performance. To solve this problem. we propose two types of estimators. symbol by symbol estimator: Unidirectional estimator (UDE) and hi-directional estimator (BDE), and sub-block estimator (SBE).

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Dry sliding wear behavior of plain low carbon dual phase steel by strain hardening and oxidation (가공경화와 산화층 형성에 의한 이상조직 저탄소강의 건식 미끄럼 마멸 거동)

  • Yu, H.S.;Kim, Y.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.149-152
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    • 2006
  • Dry sliding wear behavior of low carbon dual phase steel, of which microstructure consists of hard martensite in a ductile ferrite matrix, has been investigated. The wear characteristics of the dual phase steel was compared with that of a plain carbon steel which was normalized at $950^{\circ}C$ for 30min and then air-cooled. Dry sliding wear tests were carried out using a pin-on-disk type tester at various loads of 1N to 10N under a constant sliding speed condition of 0.2m/sec against an AISI 52100 bearing steel ball at room temperature. The sliding distance was fixed as 1000m for all wear tests. The wear rate was calculated by dividing the weight loss measured to the accuracy of $10^{-5}g$ by the specific gravity and sliding distance. The worn surfaces and wear debris were analyzed by SEM, EDS and a profilomter. Micro vickers hardness values of the cross section of worn surface were measured to analyze strain hardening behavior underneath the wearing surfaces. The were rate of the dual phase steel was lower than the plain carbon steel. Oxidation on the sliding surface and strain hardening were attributed for the higher wear resistance of the dual phase steel.

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Sliding Wear Mechanism of Ultra-Fine Grained Low Carbon Dual Phase Steel as a Function of Applied Load (경정립 미세화에 따른 이상조직 탄소강의 하중에 따른 마멸기구)

  • Yu, H.S.;Yi, S.K.;Shin, D.H.;Kim, Y.S.
    • Transactions of Materials Processing
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    • v.16 no.4 s.94
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    • pp.299-303
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    • 2007
  • Dry sliding wear behavior of ultra-fine grained(UFG) plain low carbon dual phase steel, of which microstructure consists of hard martensite in a ductile ferrite matrix, has been investigated. The wear characteristics of the UFG dual phase steel was compared with that of a coarse grained dual phase steel under various applied load conditions. Dry sliding wear test were carried out using a pin-on-disk type tester at various loads of 1N to 100N under a constant sliding speed condition of 0.20m/s against an AISI 52100 bearing steel ball at room temperature. The sliding distance was fixed as 1000m for all wear tests. The wear rate was calculated by dividing the weight loss, measured to the accuracy of 10-5g by the specific gravity and sliding distance. The worn surfaces and wear debris were analyzed by SEM, EDS and profilometer. Micro-vickers hardness of the cross section of worn surfaces were conducted to analyze strain hardening underneath the contact surfaces. The wear mechanism of the UFG dual phase steel was investigated with emphasis on the unstable nature of the grain boundaries of the UFG microstructure.

Carbon and Cobalt Diffusion in Liquid Phase Sintering of WC-Co with Gradient Composition

  • Park, Dong-Kyu;Kim, Ki-Won;Jung, Woo-Hyun
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.635-636
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    • 2006
  • In this study, the diffusion behaviors of C and Co in liquid phase sintering of WC-Co system were investigated whether these two components diffused in the same direction in case of having opposite gradient each other with not being $\eta$ phase. The green compacts with controlled compositions in not being of $\eta$ phase and gradient composition which one is WC-5Co-1.2%C, the other is WC-XCo-0.2%C (where X = 5, 10, 15, 20, 25) were sintered at $1350^{\circ}C$ and $1400^{\circ}C$ and then the diffusion behaviors of C and Co were investigated by analyses of compositional change, also determined for microstructure and microhardness. Also, same testing was carried out on the specimens with dual layers sintered in upright and reverse positions to evaluate the effect of gravity on the diffusion in liquid Co. From the results of this study, we can find the fact that the direction of diffusion for C and Co in WC-Co system during liquid phase sintering was different and the effect of gravity for the liquid was insignificant. Also other physical properties were changed on the diffusion of elements.

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New Resonant AC Link Snubber-Assisted Three-Phase Soft-Switching PWM Inverter and Its Comparative Characteristics Evaluations

  • Yoshida, Masanobu;Hiraki, Eiji;Nakaoka, Mutsuo
    • Journal of Power Electronics
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    • v.3 no.4
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    • pp.239-248
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    • 2003
  • This paper presents a novel prototype of three-phase voltage source type zero voltage soft-switching inverter with the auxiliary resonant snubbers suitable for high-power applications with IGBT power module packages in order to reduce their switching power losses as well as electromagnetic conductive and radiative noises. A proposed single inductor-assisted resonant AC link snubber circuit topology as one of some auxiliary resonant commutation snubbers developed previously to achieve the zero voltage soft-switching (ZVS) for the three-phase voltage source type sinewave PWM inverter operating under the instantaneous space voltage vector modulation is originally demonstrated as compared with the other types of resonant AC link snubber circuit topologies. In addition to this, its operation principle and unique features are described in this paper. Furthermore, the practical basic operating performances of the new conceptual instantaneous space voltage vector modulation resonant AC link snubber-assisted three-phase voltage source type soft-switching PWM inverter using IGBT power module packages are evaluated and discussed on the basis of switching voltage and current waveforms, output line to line voltage quality, power loss analysis, actual power conversion efficiency and electromagnetic conductive and radiative noises from an experimental point of view, comparing with those of conventional three-phase voltage source hard-switching PWM inverter using IGBT power modules.

Auxiliary resonant DC Link and power loss analysis of three phase voltage type inverter (보조 공진 DC 링크 스너버형 컨버터와 3상 전압형 인버터의 전력손실분석)

  • Kim, J.Y.;Mun, S.P.;Kim, Y.M.;Lee, H.W.;Suh, K.Y.
    • Proceedings of the KIEE Conference
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    • 2002.07b
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    • pp.1064-1066
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    • 2002
  • This paper proposes a new prototype auxiliary resonant DC link(ARDCL)snubber circuit and deals with its power loss on the basis of actually measured conduction loss characteristic of switching device module. Voltage type soft switching three phase inverter using proposed ARDCL snubber circuit is presented along with its performance evaluations. And, the power loss analysis of three phase hard and soft switching inverter are carried out from the point of simulation and experimental results.

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