• Title/Summary/Keyword: granule powder

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Synthesis and Characterization of Zeolite 4A on Activated Carbon Supports (활성탄 지지체상에서 제올라이트 4A 합성 및 특성)

  • Park, Jeong-Hwan;Suh, Jeong-Kwon;Jeong, Soon-Yong;Lee, Jung-Min;Doh, Myung-Ki
    • Applied Chemistry for Engineering
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    • v.8 no.2
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    • pp.204-210
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    • 1997
  • Zeolite 4A-impregnated complex molecular sieve was prepared by hydrothermal reaction after aluminosilicate gel was penetrated into the pore of activated carbon granule. The crystals of zeolite 4A mainly were formed in the macropore of activated carbon, and their average diameter is $0.8{\mu}m$. The pore volume of activated carbon granule is $0.67m{\ell}/g$, and the pore volume of the sample including 21.6wt% of zeolite 4A crystal is $0.41m{\ell}/g$ decreasing the pore volume by 40% due to the crystallization of zeolite 4A crystals on the internal surface of activated carbon. The calcium ion exchange capacity of zeolite 4A-impregnated sample is 320mg $CaCO_3/g$ zeolite, and this value is almost the same as that of zeolite 4A powder. The crystal of zeolite 4A was not separated from the support of activated carbon granule in the course of ultrasonic dispersion. The adsorption isotherm of water on zeolite 4A-impregnated sample shows the intermediate shape between types, I and III. In addition, zeolite 4A-impregnated sample shows the hydrophilic and hydrophobic properties simultaneously.

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Fabrication of Calcined Clay Granule Comprising Zeolite (제올라이트를 함유하는 소성점토의 제조)

  • Kim, Byoung-Gon;Lee, Gye-Seung;Park, Chong-Lyuck;Jeon, Ho-Seok;Jeong, Soo-Bok
    • Korean Journal of Soil Science and Fertilizer
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    • v.41 no.4
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    • pp.239-246
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    • 2008
  • This research tried to find out the optimum fabrication method of calcined clay granules comprising zeolite. Kaolin clay and natural zeolite powder were used as raw materials of calcined clay, and silica stone powder was used for controlling the porosity of the granules. The granulation was performed with two kinds of granulators: a pan granulator and a high-shear mixer granulator. Various granules were fabricated by the mixing ratios and the rotation speeds of the granulators, and were heated from 400 to $700^{\circ}C$ at $100^{\circ}C$ interval. The crushing strength, pore size distribution, and CEC of the granules were measured. The evaluation method for the resistance of granules to human treading was created and the tests were conducted at dry and wet conditions. The resistance and crushing strength improved in proportion to the rotation speed of the granulator and the heating temperature, but the CEC decreased. The pellet made by the pan granulator did not have the strength against treading upon heating to below $700^{\circ}C$, but the pellet made by the high-shear mixer granulator endured the treading test upon heating to over $500^{\circ}C$

Granulation of Fine Zeolite Powder by Adding Polyvinyl Alcohol (Polyvinyl Alcohol첨가(添加)에 의한 Zeolite미분(微粉)의 입상화(粒狀化))

  • Choi, Jyung;Choi, Choong Ryeol;Lee, Dong Hoon
    • Korean Journal of Soil Science and Fertilizer
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    • v.28 no.2
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    • pp.123-129
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    • 1995
  • For the propose of increasing the value added, zeolite powder was granulated by adding Polyvinyl Alcohol (PVA) as cementing material. The optimal concentration of PVA for granulation and the physical properties of the prepared granule were investigated. Four percent PVA stock solution was made by adding distilled water at $90^{\circ}C$ water bath and incorporated with zeolite. The contents of water stable granule above 2.0mm in diameter was 98.0% in the case of 0.3% PVA addition and almost 100% in the case of 0.6% PVA addition. Increasing PVA concentration of granules increased the hardness and decreased the infiltration rate and the maximum water holding capacity of granules, However, the drying method hardly affected the physical properties of granules. With the increase in the mixing ratios of kaolinite or bentonite to zeolite, the hardness of granules increased but high water contents of granules resulted in rapid decrease in the hardness of granules. However, when smectite or perlite was mixed with zeolite, the increase in mixing ratios to zeolite resulted in the decrease in hardness, the increase in the infilteration rate and maximum water holding capacity of granules.

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Enhancement of Biological Control of Botrytis cinerea on Cucumber by Foliar Sprays and Bed Potting Mixes of Trichoderma harzianum YC459 and Its Application on Tomato in the Greenhouse

  • Lee Sun-Kug;Sohn Hwang-Bae;Kim Geun-Gon;Chung Young-Ryun
    • The Plant Pathology Journal
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    • v.22 no.3
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    • pp.283-288
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    • 2006
  • Trichoderma harzianum YC459 (Th 459), isolated from sawdust compost, was effective in controlling cucumber and tomato gray mold caused by Botrytis cinerea under controlled and plastic film tunnel conditions. A water suspension of the wettable powder formulation of Th 459 significantly $(P\leq0.05)$ reduced the severity of cucumber gray mold by foliar spraying at all tested concentrations from $10^5\;to\;10^8$ colony forming unit (cfu)/ml in repeated experiments. The control efficacy was maintained at least seven days with the average control value of 70% in cucumber pot tests. Mixing one to eight grams of the granular formulation ($10^8cfu/g$ dry weight) of Th 459 into one liter nursery potting mix at seeding also significantly $(P\leq0.05)$ reduced the severity of cucumber gray mold by suppression of lesion formation three weeks after treatment. Application of mixing granular formulation at seeding in combination with foliar spraying during cultivation provided a more significant reduction $(P\leq0.05)$ of cucumber gray mold than granule mixing or leaf spray alone. The foliar spraying of the formulated wettable powder of Th 459 significantly $(P\leq0.05)$ reduced the infection of tomato fruits by B. cinerea as effective as the chemical fungicide, dichlofluanid, in three plastic film tunnel experiment trials. It is suggested that effective control of gray mold of cucumber and tomato can be provided by both treatment of Th 459 into potting mix and foliar spray through induction of systemic resistance and direct inhibition of the pathogen.

Effect of Potash Feldspar on the Growth of Organic Radish and Beet (카리장석의 유기농 무와 비트 생육촉진효과)

  • Shim, Chang-Ki;Kim, Min-Jeong;Kim, Yong-Ki;Hong, Sung-Jun;Park, Jong-Ho;Han, Eun-Jung;Kim, Seuk-Chul;Lee, Sung-Buk
    • Korean Journal of Organic Agriculture
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    • v.24 no.3
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    • pp.413-425
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    • 2016
  • Potassium (K) is an element essential for plant growth. This study was aimed to examine the effects of three formulations of potash feldspar, powder, sand, and granule type on the growth of radish and beet in organic farming. 0.1% three formulations of potash feldspar were treated on the soil before transplanting 15 days-old seedlings of radish and beet in greenhouse. The results showed that all kinds of potash feldspar significantly increased shoot and root growth, and soluble solid contents excepted for root hardness in radish and beet. Among them, the powder type of potash feldspar was the most effective on foliage and root growth of radish and beet. Based on the results, it was confirmed that 0.1% potash feldspar treated in the rhizosphere of radish and beet can promote the growth of them.

Bone Healing Capacity of Demineralized Dentin Matrix Materials in a Mini-pig Cranium Defect

  • Kim, Jong-Yub;Kim, Kyung-Wook;Um, In-Woong;Kim, Young-Kyun;Lee, Jeong-Keun
    • Journal of Korean Dental Science
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    • v.5 no.1
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    • pp.21-28
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    • 2012
  • Purpose: In this study the bone healing ability of autogenous tooth bone graft material as a substitute material was evaluated in a mini-pig cranial defect model through histologic examinations and osteonectin reverse transcription polymerase chain reaction (RT-PCR) quantitative analysis. Materials and Methods: A defect was generated in the cranium of mini-pigs and those without a defect were used as controls. In the experimental group, teeth extracted from the mini-pig were manufactured into autogenous tooth bone graft material and grafted to the defect. The mini-pigs were sacrificed at 4, 8, and 12 weeks to histologically evaluate bone healing ability and observe the osteonectin gene expression pattern with RT-PCR. Result: At 4 weeks, the inside of the bur hole showed fibrosis and there was no sign of bone formation in the control group. On the other hand, bone formation surrounding the tooth powder granule was observed at 4 weeks in the experimental group where the bur hole was filled with tooth powder. Osteonectin gene expression; there was nearly no osteonectin expression in the control group while active osteonectin expression was observed from 4 to 12 weeks in the experimental group. Conclusion: We believe this material will show better results when applied in a clinical setting.

Facile Preparation of Nanoporous Silica Aerogel Granules (나노다공성 실리카 에어로겔 과립의 간단 제조)

  • Kim, Nam Hyun;Hwang, Ha Soo;Park, In
    • Applied Chemistry for Engineering
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    • v.22 no.2
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    • pp.209-213
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    • 2011
  • Hydrophobic silica aerogel beads with low thermal conductivity and high porosity were prepared using a cost-effective sodium silicate as a silica source via an ambient-pressure drying process. Monolithic wet gels were first prepared by adjusting pH (~5) of a diluted sodium silicate solution. The silica aerogel beads (0.5~20 mm) were manufactured by breaking the wet gel monoliths under a simultaneous solvent exchange/surface modification process and an ambient-pressure drying process without using co-precursors or templates. Dried silica aerogel beads exhibit a comparable porosity ($593m^2/g$ of surface area, 34.9 nm of pore size, and $4.4cm^3/g$ of pore volume) to that of the aerogel powder prepared in the same conditions. Thermal conductivity of the silica aerogel beads (19.8 mW/mK at $20^{\circ}C$) is also identical to the aerogel powder.

A study on Titanium Hydride Formation of Used Titanium Aircraft Scrap for Metal Foaming Agents

  • Hur, Bo-Yong;Ahn, Duck-Kyu;Kim, Sang-Youl;Jeon, Sung-Hwan;Park, Su-Han;Ahn, Hyo-Jun;Park, Chan-Ho;Yoon, Ik-Sub
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.209-212
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    • 2001
  • Aircraft industry is developed very fast so titanium scrap was generated to manufacture. Titanium scrap was wasted and used to deoxidize cast iron so we are study recycling of it. In this research were studied that metal hydride of reacted in hydrogen chamber of AMS4900, 4901, return scrap titanium alloy and sponge titanium granule. The temperature of hydrogenation was 40$0^{\circ}C$ in the case of pure sponge titanium but return scrap titanium alloy were step reaction temperature at 40$0^{\circ}C$ and 50$0^{\circ}C$, and after the hydride of titanium alloy were crushed by ball mill for 5h. Titanium hydride contains to 4wt.% of hydrogen theoretically as theory. It was determined by heating and cooling curve in reaction chamber. The result of XRD was titanium hydride peak only that it was similar to pure titanium. Titanium hydride Powder particle size was about 45${\mu}{\textrm}{m}$, and recovery ratio was 95w% compared with scrap weight for a aluminum foam agent.

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A Study on the Establishing the Preparation Conditions for Pine Mushroom(Tricholoma matsutake Sing.) Granular Tea (송이버섯을 이용한 과립차 제조 조건 확립에 관한 연구)

  • Park, Mi-Lan;Choi, Soo-Keun;Byun, Gwang-In
    • Journal of the East Asian Society of Dietary Life
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    • v.17 no.5
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    • pp.689-695
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    • 2007
  • The pine mushroom is recognized as being a valuable functional food and is considered a prized mushroom. One of the product development plans for this mushroom is a granular tea. Thus, for this study, the physical properties and sensory qualities evaluation of such a this product were measured. First, we extracted pine mushrooms at various temperatures(50, 60, 70, 80 and $90^{\circ}C$) to make a pine mushroom granular tea. The extraction yield and free amino acid content were greatest in the $50^{\circ}C$ extraction. This extract that was acquired at $50^{\circ}C$ was lyophilized and pulverized to make the granule tea. According to the results, the granular tea made from 4% pine mushroom powder had the best taste, with a Brix value of 1.9% and a pH of 4.12. The L-value of chromaticity was 49.00, the a-value -0.85, and the b-value was 1.28.

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The Study on Fabrication and Sound Absorption Properties of Al-Zn-Mg-Cu Alloy Foams (Al-Zn-Mg-Cu 발포합금 제조 및 흡음특성에 관한 연구)

  • Jeong, Seung-Reung;Hur, Bo-Young
    • Journal of Korea Foundry Society
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    • v.31 no.3
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    • pp.145-151
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    • 2011
  • Metallic foam has been known as a functional material which can be used for absorption properties of energy and sound. The unique characteristics of Al foam of mechanical, acoustic, thermal properties depend on density, cell size distribution and cell size, and these characteristics expected to apply industry field. Al-Zn-Mg-Cu alloy foams was fabricated by following process; firstly melting the Al alloy, thickening process of addition of Ca granule to increased of viscosity, foaming process of addition of titanium hydride powder to make the pores, holding in the furnace to form of cooling down to the room temperature. Metal foams with various porosity level were manufactured by change the foaming temperature. Compressive strength of the Al alloy foams was 2 times higher at 88% porosity and 1.2 times higher at 92% porosity than pure Al foams. It's sound and vibration absorption coefficient were higher than pure Al foams and with increasing porosity.