• 제목/요약/키워드: grain-size distribution

검색결과 657건 처리시간 0.027초

Effect of dopants(Tri-valent, Penta-valent) on the electrical and optical properties of SnO2 based transparent electrodes

  • Kim, G.W.;Sung, C.H.;Seo, Y.J.;Park, K.Y.;Heo, S.N.;Lee, S.H.;Koo, B.H.
    • Journal of Ceramic Processing Research
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    • 제13권spc2호
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    • pp.394-397
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    • 2012
  • In this work, we studied the influence of the dopant elements concentration on the properties of SnO2 thin films deposited by pulsed laser deposition. X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), Hall effect measurement and UV-Vis studies were performed to characterize the deposited films. XRD results showed that the films had polycrystalline nature with tetragonal rutile structure. FE-SEM micrographs revealed that the as deposited films composed of dense microstructures with uniform grain size distribution. All the films show n-type conduction and the best transparent conductive oxide (TCO) performance was obtained on 6 wt% Sb2O5 doped SnO2 film prepared at pO2 of 60mtorr and Ts of 500 ℃. Its resitivity, optical transmittance, figure of merit are 7.8 × 10-4 Ω cm, 85% and 1.2 × 10-2 Ω-1, respectively.

Factors affecting hydraulic anisotropy of soil

  • Nurly Gofar;Alfrendo Satyanaga;Gerarldo D. Aventian;Gulnur Pernebekova;Zhanat Argimbayeva;Sung-Woo Moon;Jong Kim
    • Geomechanics and Engineering
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    • 제36권4호
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    • pp.343-353
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    • 2024
  • The hydraulic anisotropic behavior of unsaturated soil has not been fully explored in relation to the grain-size distribution. The present study conducted laboratory assessments to examine the hydraulic anisotropy condition of statically compacted specimens in various initial states. The investigation incorporated the concept of hydraulic anisotropy by employing two discrete forms of soil stratification: horizontal-layering (HL) and vertical-layering (VL). The examined soils comprised sandy silt and silty sand, exhibiting either unimodal or bimodal soil-water characteristic curve (SWCC). This study aimed to investigate the potential correlation between the hydraulic anisotropy ratio and soil properties. The present study established a correlation between the hydraulic anisotropy ratio and several soil parameters, including fine content, dry density, plastic limit, and liquid limit. The study results indicate a non-linear relationship between the percentage of fine and dry density in soils with unimodal and bimodal soil-water characteristic curve (SWCC) and hydraulic anisotropy ratio.

EFFECT OF PROCESS CONTROL AGENT ON THE MICROSTRUCTURE OF Ni-BASED ODS SUPERALLOY PRODUCED BY MECHANICAL ALLOYING AND SINTERING

  • JU-YEON HAN;HYUNJI KANG;SUNG-TAG OH
    • Archives of Metallurgy and Materials
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    • 제64권3호
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    • pp.949-952
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    • 2019
  • The effects of different types of process control agents (PCA) on the microstructure evolution of Ni-based oxide dispersion-strengthened superalloy have been investigated. Alloy synthesis was performed on elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % using high energy ball milling for 5 h. The prepared powders are consolidated by spark plasma sintering at 1000℃. Results indicated that the powder ball-milled with ethanol as PCA showed large particle size, low carbon content and homogeneous distribution of elemental powders compared with the powder by stearic acid. The sintered alloy prepared by ethanol as PCA exhibited a homogeneous microstructure with fine precipitates at the grain boundaries. The microstructural characteristics have been discussed on the basis of function of the PCA.

충청남도 금산군 일대 제4기 지질 및 골재자원 분포 특성 (Distribution Characteristics of Quaternary Geology and Aggregate Resources in Geumsan-gun, Chungcheongnam-do)

  • 김진철;김주용;이진영
    • 자원환경지질
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    • 제54권5호
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    • pp.595-603
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    • 2021
  • 하천 및 육상 골재 자원의 주 대상인 모래층의 분포는 제4기 퇴적 환경 중 충적 및 하천 퇴적환경에 주로 속한다. 충청남도 금산군 일대의 골재 자원 분포는 특징적으로 감입곡류 하천이 우세한 퇴적 환경 중심으로 발달하고 있는 반면, 붕적이나 선상지성 퇴적환경에서 형성된 퇴적층은 육상 및 하천 골재 분포 비율이 상대적으로 낮다. 봉황천 주변과 소하천들이 합류하는 부근 일대는 소규모이지만 하천의 범람원이 발달하며 골재 분포 지역에 해당된다. 금산군 제4기 퇴적층의 수직 분포는 약 5~12m 범위와 평균 8m의 제4기 퇴적층 두께를 갖는다. 골재 부존 구간은 평균 3.6m 두께이며 평균 입도는 점토-실트 약 21%, 모래 67%, 그리고 자갈 12%이다. 골재 부존 구간의 주요 특징은 조립질 모래가 우세하고 자갈은 아각형 또는 아원형, 분급은 일반적으로 불량하고 괴상의 형태를 띠며 암회색~황갈색 범위의 토색을 보인다. 금산군 내에서 골재 개발 가능성이 큰 분포 지역은 금강본류, 봉황천과 소하천 지류의 현 하상과 구하상을 따라 분포하는 충적 퇴적층 및 하천 퇴적층이다.

Effect of Magnetic Field Annealing on Microstructure and Magnetic Properties of FeCuNbSiB Nanocrystalline Magnetic Core with High Inductance

  • Fan, Xingdu;Zhu, Fangliang;Wang, Qianqian;Jiang, Mufeng;Shen, Baolong
    • Applied Microscopy
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    • 제47권1호
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    • pp.29-35
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    • 2017
  • Transverse magnetic field annealing (TFA) was carried out on $Fe_{73.5}Cu_1Nb_3Si_{15.5}B_7$ nano-crystalline magnetic core with the aim at decreasing coercivity ($H_c$) while keeping high inductance ($L_s$). The magnetic field generated by direct current (DC) was applied on the magnetic core during different selected annealing stages and it was proved that the nanocrystalline magnetic core achieved lowest $H_c$ when applying transverse field during the whole annealing process (TFA1). Although the microstructure and crystallization degree of the nanocrystalline magnetic core exhibited no obvious difference after TFA1 compared to no field annealing, the TFA1 sample showed a more uniform nanostructure with a smaller mean square deviation of grain size distribution. $H_c$ of the nanocrystalline magnetic core annealed under TFA1 decreased along with the increasing magnetic field. As a result, the certain size nanocrystalline magnetic core with low $H_c$ of 0.6 A/m, low core loss (W at 20 kHz) of 1.6 W/kg under flux density of 0.2 T and high $L_s$ of $13.8{\mu}H$ were obtained after TFA1 with the DC intensity of 140 A. The combination of high $L_s$ with excellent magnetic properties promised this nanocrystalline alloy an outstanding economical application in high frequency transformers.

Enhancement of Porosity and Strength of Porous Al2O3 Ceramics by Al(H2PO4)3 Addition

  • Bai, Jiahai;Piao, Jiasi;Gao, Jie;He, Jing;Du, Qingyang;Li, Chengfeng
    • 한국세라믹학회지
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    • 제56권4호
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    • pp.350-353
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    • 2019
  • Porous alumina ceramics with addition of 0, 5, 10, 15, and 20 wt% Al(H2PO4)3 were sintered at 1300, 1350, and 1400℃. The effects of the Al(H2PO4)3 addition on crystal phases, water absorption, open porosity, pore size distribution, microstructures, and flexural strength were studied extensively. The experimental results revealed that only characteristic peaks of corundum were indexed in the XRD patterns of the as-prepared porous ceramics. The water absorption and open porosity of the porous Al2O3 ceramics increased remarkably with an increase in Al(H2PO4)3 addition. The flexural strength first increased to a maximum value when 5 wt% Al(H2PO4)3 was added and then decreased as additional Al(H2PO4)3 was further added. SEM images showed that the average Al2O3 grain size in the porous ceramics changed in an opposite way as the flexural strength. The porous Al2O3 ceramics with 10 wt% Al(H2PO4)3 addition exhibited comparable flexural strength to the ceramics without Al(H2PO4)3 addition, although the latter had much higher porosity.

레디믹스트 숏크리트 개발 I : 기초 연구 (Development of Ready-mixed Shotcrete I : Basic Study)

  • 김동민;마상준
    • 대한토목학회논문집
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    • 제31권5C호
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    • pp.171-185
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    • 2011
  • 레디믹스트(Ready-mixed) 숏크리트는 전문공장에서 원재료를 건조배합 형태로 생산하여 시공현장으로 운반 및 타설되는 재료로서, 확실한 골재 품질관리가 가능하며 규격화된 재료 사용으로 시공 품질 개선이 가능하다. 특히, 현장 배치플랜트의 축소 혹은 생략이 가능하기 때문에, 설치비용 절감 및 부지확보로 인한 민원과 환경문제를 해결할 수 있는 추가적인 장점이 있다. 본 연구에서는 숏크리트 성능 향상을 위한 방법으로 혼화재 및 급결제에만 국한되어 있던 기존 연구방향을 벗어나, 골재 자체의 품질 개선을 통해 숏크리트 성능을 향상시키고자 하였다. 기초 연구에서는 국내 숏크리트 시공실태 및 공급골재의 품질파악을 실시하였고, 현장실험을 통해 레디믹스트 숏크리트의 굵은 골재 최대치수를 8mm로 결정하였다. 또한, Pilot Plant Test를 실시하여 공장생산 공정의 재료분리 현상을 최소화 하고자 하였고, 현장실험을 통해 강섬유와 동일 수준의 휨인성을 발휘할 수 있는 합성섬유의 최적 혼입량과 고로슬래그 미분말의 최적 치환율을 도출하였다.

Controlled Synthesis of Single-Walled Carbon Nanotubes

  • Park, Chong-Yun
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제40회 동계학술대회 초록집
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    • pp.2-2
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    • 2011
  • Single-walled carbon nanotubes (SWNTs) have been considered as a promising candidate for nextgeneration electronics due to its extraordinary electrical properties associated with one-dimensional structure. Since diversity in electronic structure depends on geometrical features, the major concern has been focused on obtaining the diameter, chirality, and density controlled SWNTs. Despite huge efforts, the controlled synthesis of SWNTs has not been achieved. There have been various approaches to synthesize controlled SWNTs by preparation of homogeneously sized catalyst because the SWNTs diameter highly depends on catalyst nanoparticles size. In this study, geometrically controlled SWNTs were synthesized using designed catalytic layers: (a) morphologically modified Al2O3 supporting layer (Fe/Al2O3/Si), (b) Mo capping layer (Mo/Fe/Al/Si), and (c) heat-driven diffusion and subsequent evaporation process of Fe catalytic nanoparticles (Al2O3/Fe/Al2O3/Si). These results clearly revealed that (a) the grain diameter and RMS roughness of Al2O3 supporting layer play a key role as a diffusion barrier for obtaining Fe nanoparticles with a uniform and small size, (b) a density and diameter of SWNTs can be simultaneously controlled by adjusting a thickness of Mo capping layer on Fe catalytic layer, and (c) SWNTs diameter was successfully controlled within a few A scale even with its fine distribution. This precise control results in bandgap manipulation of the semiconducting SWNTs, determined by direct comparison of Raman spectra and theory of extended tight binding Kataura plot. We suggest that these results provide a simple and possible way for the direct growth of diameter, density, and bandgap controlled SWNTs by precise controlling the formation of catalytic films, which will be in demand for future electronic applications.

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독도 인근 해저퇴적물과 유기 퇴적물 분포 특성 (Characterization of Clastic and Organic Sediments Near Dokdo, Korea)

  • 전창표;김창환;이성주
    • 한국광물학회지
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    • 제26권2호
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    • pp.65-80
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    • 2013
  • 독도로부터의 거리 및 수심에 따라 채취된 표층 퇴적물에 대하여 입도분석, 광물분석, 유기물 분석 및 미화석 분석 결과를 이용하여 독도 인근 해저의 퇴적 기작 및 유기 퇴적물의 분포를 규명하였다. 독도 인근 해저 퇴적물은 자갈 및 사질이 우세하며, 끌림에 의한 퇴적 작용이 주를 이루는 반면에 독도와 거리가 멀어짐에 따라 실트와 머드의 비율이 증가하며 점토광물과 장석 등의 광물 성분의 변화를 보이고 뜬짐에 의한 퇴적이 우세해지는 경향을 보인다. 퇴적물에 포함된 유기 퇴적물의 군집 조성 또한 큰 변화를 보이는데, 연안 퇴적물에서는 해양 기원의 유기 퇴적물이, 심해 퇴적물에서는 육상 기원의 유기 퇴적물이 우점한다. 이러한 유기 퇴적물의 군집 변화는 퇴적물의 입도에 큰 영향을 받는 것으로 밝혀졌으며 유기 퇴적물중 높은 화분 농집도는 심해 퇴적물의 유기탄소 함량을 증가시키는데 중요한 역할을 하는 것으로 판단된다.

An interpretation of potential catastrophic collision at P/2010 A2

  • Kim, Yoonyoung;Ishiguro, Masateru;Michikami, Tatsuhiro;Nakamura, Akiko M.
    • 천문학회보
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    • 제41권1호
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    • pp.49.1-49.1
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    • 2016
  • Solar System has evolved with numerous collisions among asteroids. Ancient catastrophic collisions of large parent bodies led the formation of asteroid families and relevant dustband structures up to the present day, and it would be interesting to address a question - "what happens if an asteroid collides with another asteroid?" Recent discoveries of "active asteroids" in the main-belt have attracted interest for their potential to witness a catastrophic collision in the current Solar System. So far, however, there is no direct evidence for catastrophic collision on active asteroids while several objects have been confirmed for other mechanisms (e.g., 596 Scheila for impact cratering, P/2013 R3 and P/2013 P5 for rotational breakup). The most potential candidate for catastrophic collision could be a sub-km active asteroid P/2010 A2, which is still controversial on its driving mechanism, but if confirmed, would have made P/2010 A2 the unique example of catastrophic collision on the current main asteroid belt. In this presentation, we revisit all of archival data of P/2010 A2 in a combination with our own observation using Subaru/Suprime-Cam on 2011 June, where we have a great benefit of a large orbital coverage. We found a grain size dependence of dust ejection velocity from P/2010 A2 (a power-law size distribution with an index of k~ -1/10), which is favorable to a catastrophic disruption scenario in agreement with laboratory impact experiments. At this conference, we plan to provide our understanding of the morphology of P/2010 A2 through a perspective of catastrophic collision.

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