• Proceedings of the Korean Society of Machine Tool Engineers Conference
• /
• 2003.10a
• /
• pp.59-65
• /
• 2003

Four kinds of $Si_3N_4$-based ceramic cutting tools with different sintering time were fabricated to investigante the effect of sintering time on the microstructure, mechanical properties, grain sizes and the cutting performance. An endeavor was also made to determine the relation among mechanical property, Brain size and tool life. $Si_3N_4$ home made cutting tool sintered for 1 hour under $1760^{\circ}$ temperature and 25MPa pressure showed the best cutting performance among selected ceramic tools during machining both Bray cast iron and heat treated SCM440. Multiple linear regression model was used to estimate the tool lift from mechanical property, grain size and showed good result. It was also shown that hardness imposed the biggest offect on tool life.

• Tribology and Lubricants
• /
• v.11 no.5
• /
• pp.26-30
• /
• 1995

Sliding experiments have been conducted on alumina and silicon carbide ceramics. Wear and friction data of both materials indicate that wear proceeds in two distinct stages. The wear occurs by a relatively mild plastic-grooving process in the initial stage, but eventually gives way to a severe grain pull-out process after a defined period of sliding test. The datails of the transition mechanism are presented. The effects of grain size and second phase particle on the wear transition are also presented.

• Transactions of Materials Processing
• /
• v.33 no.3
• /
• pp.193-199
• /
• 2024

The friction welding characteristics of stainless steels, mainly used in energy and chemical plant industries due to its excellent corrosion resistance and high strength, was evaluated in this study. Friction welding was introduced and conducted at a rotation speed of 2,000 RPM, friction pressure of 30 MPa, burn-off length of 5 mm and upset pressure of 110 ~ 200 MPa on rod typed specimens. The grain boundary characteristics distributions such a grain size, shape, misorientation angle and kernel average misorientation of the welds were clarified by electron backscattering diffraction method. The application of friction welding on SUS304 alloy resulted in a significant refinement of the grain size in the weld zone (5.11 mm) compared to that of the base material (48.09 mm). The mechanical properties of the welds, on the other hand, appeared to be relatively low or similar to those of the base material, which were mainly caused by dislocation density in the initial material and grain refinement in the welds.

• Korean Journal of Materials Research
• /
• v.19 no.6
• /
• pp.330-336
• /
• 2009

The size of crystallites in mono-dispersed cubic silver bromide grains was measured by applying a powder X-ray diffraction method and Scherrer's equation to grains that were suspended in swollen gelatin layers. In order to evaluate the existence of defects, the measured crystallite size was compared to those measured by using a scanning electron microscope. In the case of the grains prepared by the controlled double jet method, the size of crystallites was equal to the edge length of the grains that had edge lengths smaller than 400 nm. This result proved the usefulness of the above-stated method for measuring the size of crystallites and also evaluating the presence of any crystal defect in each grain. In the case of the grains, which were precipitated in the presence of a sensitizing dye and potassium iodide, the size of crystallites was smaller than the edge's length, indicating the discontinuities in the grains introduced during the precipitation process.

• Journal of the Korean Ceramic Society
• /
• v.40 no.4
• /
• pp.354-359
• /
• 2003

The microwave dielectric characteristics of (1-x)(Al$\_$$\frac{1}{2}$/Ta$\_$$\frac{1}{2}$/)O$_2$-x(Mg$\_$1/3/Ta$\_$2/3/)O$_2$ (0$\leq$x$\leq$1.0) ceramics were investigated by crystalstructure, variations of ionic polarizability, and microstructures. As x increased, (1-x)(Al$\_$$\frac{1}{2}$/Ta$\_$$\frac{1}{2}$/)O$_2$-x(Mg$\_$1/3/Ta$\_$2/3/)O$_2$ transformed to tetragonal structure. Because the ionic radius of (Mg$\_$1/3/Ta$\_$2/3/)$\^$4+/was slightly bigger than one of (Al$\_$$\frac{1}{2}$/Ta$\_$$\frac{1}{2}$/)$\^$4+/, the cell parameters increased with increase of (Mg$\_$1/3/Ta$\_$2/3/)O$_2$concentration and coincided with prediction of the molecular additivity rule. As x increased, the compositions revealed ordered phase and were of single phase above 60 mol%. The increase of the ordered phase and grain size enhanced the Q and when ordering was completed at x over 0.6, the grain size was major factor for the increase in the a. Though the grain size increased, however, the porosity deteriorated the q. Therefore, the a depended on the order/disorder, the porosity, and the grain size in regular order.

• Korean Journal of Fisheries and Aquatic Sciences
• /
• v.44 no.6
• /
• pp.772-784
• /
• 2011

We measured grain size, organic matter, and metallic elements (Fe, Cu, Pb, Zn, Cd, Cr, Mn, Hg, and As) in intertidal sediments collected from six islands in the western part of Jellanam Province in order to evaluate heavy metal contamination in the tidal flat sediments of coastal islands. The evaluation of metal contamination was carried out using geochemical assessment techniques such as sediment quality guidelines (SQGs), enrichment factor (EF), and geoaccumulation index ($I_{geo}$). Surface sediments were classified into four sedimentary facies: sand, gravelly muddy sand, slightly gravelly mud, and silt. The concentrations of heavy metals in intertidal sediments from Jaeun, Amtae, Biguem, and Docho islands showed good positive correlations with mean grain size and ignition loss, indicating that the concentrations of metallic elements in these sediments were dependent on grain size and the organic matter content. The concentrations of heavy metals in sediments from almost all of the stations were lower than two criterion values proposed by the National Oceanic and Atmospheric Administration (NOAA) in the United States. Based on the EF and $I_{geo}$ results, surface sediments were a little polluted for Cr and were moderately polluted for As. Our results suggest that more intensive studies are necessary in the future in order to determine the major source of As in intertidal sediment and to evaluate the As pollution level in macrobenthos.

• KOREAN JOURNAL OF CROP SCIENCE
• /
• v.33 no.s01
• /
• pp.1-17
• /
• 1988

Rice Quality is considered to the five catagories ; the nutritional value: the characteristics of cooking. eating and processing: grain size, shape and appearance : milling yields: and storage characteristics. Because most rice is processed and consumed in whole-kernel form. the cooking and eating quality is of important and the physical properties of the intact kernel such as size, shape and general appearance are of particular significance in determining marketing quality. Eating Quality which can be directly evaluated by consumer's panel test is so complicate and variable, and thus the objective and simplified method of evaluation is required of using appropriate instruments. Even though many researches have been done to evaluate the eating quality in various aspects such as the texture of cooked rice kernels, amylogram analysis of rice powder, amylose content. gelatinization temperature. moisture absorption of rice kernel, and cooking characteristics, none of them is satisfied for the evaluation of eating quality. The improving eating quality should be also considered to many cultural factors. such as varieties, climatic and soil conditions, cultural method, handling after harvest. milling and storage conditions. In Korea, many researches in grain size. shape and appearance, and eating quality have been done with the varietal improvement mainly by rice breeders, but no effective method of evaluation was established. A few research have been done in the relationship between rice quality and cultural factors. In the future, research in rice quality should emphasize to establish the standard evaluation method in the physicochemical properties of rice kernels for application of varietal selection. and to develop cultural practices for the preserving quality characteristics of the varieties.

• Journal of the Mineralogical Society of Korea
• /
• v.22 no.4
• /
• pp.371-383
• /
• 2009

Crystallinity and textural relations, which are crucial in terms of the quality concept of high-purity limestone, have not been effectively applicable to the limestone evaluation as crude ore due to the difficulties in precise measurements. To overcome the above, as a new method of ore characterization, a measurement of shape factor and grain boundary frequency utilizing the image analysing system was adopted in this study. Some domestic limestones used for lime manufacturing were investigated by such a quality evaluation method, and its results are discussed and correlated each other samples. As the result, even though calcite contents of crude ore, i.e., limestone grade and its crystal size are similar, quality of manufactured lime is remarkably different depending on the degree of shape factor and grain boundary frequency. In other words, as the more irregular in crystal shape and the higher the grain boundary frequency, the manufactured quick lime became more superior in all terms of lime quality such as rate of calcination, porosity, reactivity, sintering and decrepitation effect. However, because the quick lime become easily overheated in case of relatively higher degree in shape factor and grain boundary effect, a technology minimizing heating time is necessary for the manufacturing of high quality lime. In limestone industry, such a ore characterization method will be much more reasonable than the conventional method by measurement of mean size, because the method may collectively comprise crystal shape and other textural factors which can not be numerically evaluated in the past.

• Proceedings of the KIEE Conference
• /
• 1999.07d
• /
• pp.1864-1866
• /
• 1999

The magnetic nondestructive test can be applied to evaluate the magnetic material characteristics and the fracture properties through the internal defects of SA-508 used in the pressure vessels of the nuclear power plants as the direct and accurate in-situ testing methods. The fracture toughness, yield strength and the stress distribution around the defects in the surface and sub-surface of magnetic materials can be directly estimated by Bark-hausen noise(BN) methods as NDT. The testing process of SA-508 by Barkhausen noise method was advanced by controlling the austenizing peak temperature and the time of maintenance at a constant austenizing peak temperature, therefore causing the variation of fracture toughness. Through above process. we can evaluate the variations of effective grain size and the correlation of effective grain size and FATT at each situation. And the stress distribution around the defects can be quantified nondestructively through Barkhausen method.

• Analytical Science and Technology
• /
• v.11 no.4
• /
• pp.316-320
• /
• 1998

An image analysis was used for the interpretation of microstructures of ferrous metal artifacts. For the purposes, various microstructural features such as average grain size, phase area, shape factor, and composition of the inclusions, were parameterized for the information about manufacturing techniques such as casting, heating and tempering. The carbon content was determined through the evaluation of the amount of pearlite phase. As the amount of pearlite phase increased the shape factor also increased. Grain size was relatively smaller in trans-section than in cross-section. The manufacturing direction was trans-sectional because the orientation of inclusions was elongated lengthwise. All inclusions was of silicate groups and the manufacturing temperature was estimated up to $1450^{\circ}C$.