• 한국분말재료학회지
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• 제4권4호
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• pp.283-290
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• 1997

$Ti_5Si_3$ intermetallics containing 0-6 wt% of Cu were made by reactive sintering (RS) under vacuum using elemental powder mixtures (Process 1), electro-pressure sintering (EPS) using RS'ed materials (Process2), and EPS using elemental powder mixtures (Process 3). Relatively low dense titanium silicides were gained by process 1, in which porosity decreased with increasing Cu content. For example, porosity changed from 42 to 19.4% with the increase in Cu content from 0 to 6 wt%, indicating that Cu is a useful sintering aid. The titanium silicides fabricated by Process 2 had a higher density than those by Process 1 at given composition, and porosity decreased with increasing Cu content. For example, porosity decreased from 38 to 6.8% with the change in Cu content from 0 to 6 wt%. A high dense titanium silicides were obtained by Process 3. In this Process, porosity decreased a little by Cu addition, and was almost insensitive to Cu content. Namely, about 9 or 7% of porosity was shown in 0 or 1-6 wt% Cu containing silicides, respectively. The hardeness increased by Cu addition, and was not changed markedly with Cu content for the silicides fabricated by Process 3. This tendency was considered to be resulted from porosity, hardening of grain interior by Cu addition, and softening of grain boundary by Cu-base segregates. All these results suggested that EPS using elemental powder mixtures (Process 3) is an effective processing method to achieve satisfactorily dense titanium silicides.

• 한국해양공학회지
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• 제22권4호
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• pp.20-26
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• 2008

The primary purpose of this study was to quantitatively examine whether there was a difference in the settling velocities of cohesive sediments in the Saemankeum artificial lake before and after the closure of the Saemankeum seadike. Through in situ sediment sampling and laboratory experiments, the settling velocities were estimated as a function of the suspension concentration and their physico-chemical properties, such as grain size distribution, the percentage of organic contents, mineralogical composition, etc. were also examined. In this study, their inter-relation with settling velocities were also analyzed qualitatively. The result of the settling tests for Saemankeum sediments showed that there was a big difference in the settling velocities before and after the closure of the Saemankeum seadike. Its settling velocities in a flocculated settling region became remarkably larger after the closure compared to those before the closure, while they were similar but relatively smaller in a hindered settling region. This was found to be mainly due to the difference in their grain size.

• 대한치과기공학회지
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• 제29권1호
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• pp.49-57
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• 2007

This study was to add crushed frit with different grain sizes to 3Y-TZP so that it could determine the mechanical properties depending on sintering temperature. In this study, 3 types specimens were prepared in powder with respective additions of 20wt.% frit, which was sized through 24-, 48- and 72-hour ball milling with zirconia. Then, sintered pellets were tested in experiments under the temperature variations for different compositions. As a result, this study came to the following findings: 1. It was found that the higher sintering temperature and the longer ball milling time of frit led to the higher sintered density. 2. Bending strength tended to increase with higher sintering temperature and longer ball milling time of frit. 3. Hardness tended to increase with higher sintering temperature and longer ball milling time of frit. 4. However, it was found that fracture toughness didn't vary significantly depending on sintering temperature. From these findings, it was concluded that the smaller frit grain size and the narrower particle size distribution of frit lead to the better mechanical properties.

• 한국세라믹학회지
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• 제39권6호
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• pp.528-534
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• 2002

CaO ceramics were prepared by conventional sintering process and their hydration behaviors were evaluated by measuring weight increment on saturated water vapor pressure at ambient temperature. CaCO$_3$ and limestone were used as CaO source materials and $Al_2$O$_3$, MgO and SiO$_2$ were added as sintering agents. $Al_2$O$_3$ was a liquid phase sintering agent to increase densification and grain growth rates, whereas MgO and SiO$_2$, densification and grain growth inhibitors. Regardless of composition, all of the prepared CaO ceramics showed the improved hydration resistance as bulk density increased. Especially, when bulk density was more than 3.0 g/㎤, there was no weight increment after 120 h of hydration. Therefore, to decrease contact area between CaO and water vapor by increasing bulk density with the $Al_2$O$_3$ sintering additive was effective for the improvement of CaO hydration resistance.

• 한국세라믹학회지
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• 제26권1호
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• pp.13-20
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• 1989

After sintering Si3N4 containing 20wt% of variable composition ratio of Y2O3 and Al2O3 at 1$600^{\circ}C$, the specimens were annealed at 125$0^{\circ}C$ and 135$0^{\circ}C$ for 5, 10, 15 hours in order to crystallize the remanining oxynitride glass phases. The main grain-boundary crystalline phases in the Si3N4-Y2O3-Al2O3 system were melilite and YAG. By annealing 15hrs. at 125$0^{\circ}C$, almost all of the glasses were crystallized. During the growth of melilite, lattice volyume of $\beta$-Si3N4 was increased as Al3+ and O2- ions in the oxynitride glass diffuse into $\beta$-Si3N4 lattice, but during the growth of YAG, lattice volume of $\beta$-Si3N4 was decreased by reverse diffusion of Al3+ and O2- ions. In case of crystallization of glass phase to melilite, thermal expansion of sample was decreased, but in case of crystallization to YAG, inverse phenomen on was observed.

• 한국가구학회지
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• 제23권3호
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• pp.298-304
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• 2012

Since 1990's, a flooring based on plywood has gotten customers' demand. Costs of raw material and production increased because of changed environment of industry. Tropical timber such as Red Meranti (Shorea acuminate) used for raw material of the floor has been depleting beside countries in South Eastern Asia changed species of afforestation. As a result, it gets hard to secure good quality of raw material for plywood. Moreover plywood price is increased suddenly after earthquake in Japan. Eucalyptus (Eucalyptus globulus) in china has been using for raw material as a countermeasure of changed environment of industry. In this study, possibility of using flooring consisted of Eucalyptus veneer as a core layer was checked by heat transfer experiments. Flooring consisted of Red Meranti was used for comparison. Two factors which impact on heat transfer are a type of density gradient and density difference between Long-grain veneer and Short-grain veneer. Red Meranti samples are 'M' type of density gradient on the other hand Eucalyptus samples are 'W' type of density gradient.

• 한국전기전자재료학회논문지
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• 제16권6호
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• pp.538-548
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• 2003

We studied effects by Re$_2$O$_3$(R=Dy, Gd, Ho) addition on the properties of Mn-Zn ferrite. The doping concentration range from 0.05 wt% to 0.25 wt%. All samples were prepared by standard fabrication of ceramics. With increasing the rare earth oxides, specific density and initial permeability increased on the whole. But, the tendencies such as upper result had the measured value on limitation and characteristics saturated or decreased properties after that. In case of excessive addition of additive beyond some level, initial permeability properties of ferrite have gone down in spite of anomalous grain. With increasing the content of additive, both the real and imaginary component of complex permeability and the magnetic loss (tan$\delta$) increased. Because the increased rate of real component had higher than imaginary component, magnetic loss increased none the less for increasing the real component related with magnetic permeability. But, the magnetic loss of ferrite doped with the rare earth oxides was lower than that of Mn-Zn ferrite at any rate. The small amount of present rare earth oxides in Mn-Zn ferrite composition led to enhancement of resistivity in bulk, and more so in the grain boundary. It was seem to be due to the formation of mutual reaction such as between iron ions and rare earth element ions.

• 한국주조공학회지
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• 제32권1호
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• pp.32-37
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• 2012

In this study, microstructural evaluation was carried out on secondary hardening type ultrahigh strength steel, Fe-Co-Ni composition. This paper as a first part of whole research presented the microstructural behavior by cyclic heat treatment. The cyclic heat treatment method includes normalizing, stress relieving, solution treatment and aging. Especially, solution treatments performed triple times to get maximized solution hardening. Phase transformation and microstructure were observed by using optical microscope (OM), Electron back-scattered diffraction (EBSD) and X-ray stress analyzer. During the triple solution treatment, size of grain boundary was dramatically decreased by generating a packet from the martensite transformation of residual austenite in the inner part of grain, whereas the hardness increase was not significant.

• Journal of Biosystems Engineering
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• 제25권1호
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• pp.33-38
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• 2000

This study was performed to investigate airtight storage characteristics of rough rice using airtight flexible pve container. A storage test of rough rice of 4 tonnes was carried out to determine the changes of gas composition of air in the container, grain moisture content, air temperature and relative humidity , the presence of insects ,germination rate, crack ratio , fat acidity , 1000-kernel weight, and brown rice recovery over storage period of 5 months in Suwon. Concentration of oxygen was decreased from 20% to 16% and carbon dioxide was increased of from 0.03% to 1.6%. The grain moisture content was decreased from 14.4%(w.b) to 14.1%(w.b) for 5 months storage period . Insect population levels were low but these increased after 5 months storage. Most of insects were dead, Fat acidity increased from 7.5(mg KOH/100g) to 10.2(mg KOH/100g). Other storage factors such as germination rate, brown rice recovery and 1000-kernel , and 1000-kernel weight slightly decreased and crack ratio was slightly increased. Qualities of rough rice during 5 months storage period under hemetic air conditions were maintained fairly good considering the above changes of quality factors during storage.

• Journal of the korean society of oceanography
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• 제32권3호
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• pp.112-119
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• 1997

Coastal sediments collected near the Youngkwang Nuclear Power Plant were analysed for major(Al$_2$O$^_3$, Fe$^_2$O$^_3$, MgO, CaO, Na$^_2$O, K$^_2$O, TiO$^_2$, MnO), trace (Ba, Sr, V, Co, Cr, Cu, Ni, Zn, Pb) metal, and P$^_2$O$^_5$ contents. The composition of bulk metals from most stations fits within the range as those in the average crustal and sedimentary rocks, suggesting that the anthropogenic perturbation of these components is insignificant. The abundance and distribution of total contents for the majority of metals in the surface sediment could be explained by the grain size and were associated with mud (<63 ${\mu}$m) contents. However, distributions of Ca, K, Sr and Ba did not have any significant association with the sediment grain size. This may be due to the geochemical coherence among these metals in certain minerals abundant in coarse grained fractions. The distribution of Pb appears to be partly affected by the contribution from aerosol fallout. Using the R'-mode factor analysis, we show that the variance of the metal contents could be explained by four factors which account for 93.7% of the total variance. It appears that texturally controlled and/or sorting factors influenced by fine fraction are the most dominant factors which determine the relative abundance and distribution of metals in the study area.