• Journal of Dental Rehabilitation and Applied Science
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• v.22 no.2
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• pp.111-123
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• 2006

A Study on the Fracture Strength of All-Ceramic Crown according to the Zirconia Coping Design using CAD/CAM System L. Bulgan, In-Ho Cho, Soo-Yeon Shin Department of Prosthodontics, Graduate School, Dankook University The fracture strength of prosthesis is important, because it affects the function, and long term success of prosthesis and teeth. The purpose of this study was to compare the fracture strength of zirconia coping designs. Experimental test group were classified into three designs according to coping design, Modified design: Zirconia coping margin was located at 1mm above the axiogingival line angle. Collarless design: The coping margin terminated at the axiogingival line angle Butt design: The coping margin was extended to the finishing line of prepared margin. A $Cercon^{(R)}$(Degussa, Germany) CAD/CAM system was used to make the zirconia coping. Fracture strength was measured using loading machine at a cross head speed of 1mm/min. The results were statistically analyzed using the one-way ANOVA and multiple comparison test. Statistical significance was set in advance at the probability level of less than 0.05. The result : I. Collarless($738N{\pm}155N$) and Modified($755N{\pm}185N$) groups showed significantly a lower fracture strength than Butt($1057N{\pm}262N$) group(p<0.05). II. There were no statistical differences of the fracture strength between Modified($755N{\pm}185N$) and Collarless($738N{\pm}155N$) groups. III. When comparing the fractured surface, all the group showed porcelain fracture, which were fractured at the labial surface of baked porcelain The butt design of the zirconia coping has higher fracture strength than modified and collarless design.

• The Journal of Advanced Prosthodontics
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• v.2 no.4
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• pp.117-121
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• 2010

PURPOSE. The present study was intended to evaluate the effect of soldering techniques with infrared ray and gas torch under different gap distances (0.3 mm and 0.5 mm) on the tensile strength and surface porosity formation in Ni-Cr base metal alloy. MATERIALS AND METHODS. Thirty five dumbbell shaped Ni-Cr alloy specimens were prepared and assigned to 5 groups according to the soldering method and the gap distance. For the soldering methods, gas torch (G group) and infrared ray (IR group) were compared and each group was subdivided by corresponding gap distance (0.3 mm: G3 and IR3, 0.5 mm: G5, IR5). Specimens of the experimental groups were sectioned in the middle with a diamond disk and embedded in solder blocks according to the predetermined distance. As a control group, 7 specimens were prepared without sectioning or soldering. After the soldering procedure, a tensile strength test was performed using universal testing machine at a crosshead speed 1 mm/min. The proportions of porosity on the fractured surface were calculated on the images acquired through the scanning electronic microscope. RESULTS. Every specimen of G3, G5, IR3 and IR5 was fractured on the solder joint area. However, there was no significant difference between the test groups (P > .05). There was a negative correlation between porosity formation and tensile strength in all the specimens in the test groups (P < .05). CONCLUSION. There was no significant difference in ultimate tensile strength of joints and porosity formations between the gas-oxygen torch soldering and infrared ray soldering technique or between the gap distance of 0.3 mm and 0.5 mm.

• Advances in aircraft and spacecraft science
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• v.1 no.1
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• pp.1-14
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• 2014

Physico-chemical changes of the plasma modified titanium alloy [Ti-6Al-4V] surface were studied with respect to their crystallographic changes by X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM).The plasma-treatment of surface was carried out to enhance adhesion of high performance nano reinforced epoxy adhesive, a phenomenon that was manifested in subsequent experimental results. The enhancement of adhesion as a consequence of improved spreading and wetting on metal surface was studied by contact angle (sessile drop method) and surface energy determination, which shows a distinct increase in polar component of surface energy. The synergism in bond strength was established by analyzing the lap-shear strength of titanium laminate. The extent of enhancement in thermal stability of the dispersed nanosilica particles reinforced epoxy adhesive was studied by Thermo Gravimetric Analysis (TGA), which shows an increase in onset of degradation and high amount of residuals at the high temperature range under study. The fractured surfaces of the joint were examined by Scanning electron microscope (SEM).

• The Journal of Advanced Prosthodontics
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• v.8 no.4
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• pp.267-274
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• 2016

PURPOSE. This study aimed to evaluate the effect of surface treatments on bond strength of indirect composite material (Tescera Indirect Composite System) to monolithic zirconia (inCoris TZI). MATERIALS AND METHODS. Partially stabilized monolithic zirconia blocks were cut into with 2.0 mm thickness. Sintered zirconia specimens were divided into different surface treatment groups: no treatment (control), sandblasting, glaze layer & hydrofluoric acid application, and sandblasting + glaze layer & hydrofluoric acid application. The indirect composite material was applied to the surface of the monolithic zirconia specimens. Shear bond strength value of each specimen was evaluated after thermocycling. The fractured surface of each specimen was examined with a stereomicroscope and a scanning electron microscope to assess the failure types. The data were analyzed using one-way analysis of variance (ANOVA) and Tukey LSD tests (${\alpha}$=.05). RESULTS. Bond strength was significantly lower in untreated specimens than in sandblasted specimens (P<.05). No difference between the glaze layer and hydrofluoric acid application treated groups were observed. However, bond strength for these groups were significantly higher as compared with the other two groups (P<.05). CONCLUSION. Combined use of glaze layer & hydrofluoric acid application and silanization are reliable for strong and durable bonding between indirect composite material and monolithic zirconia.

• Korean Journal of Materials Research
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• v.30 no.3
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• pp.105-110
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• 2020

Cu/PET composite films are widely used in a variety of wearable electronics. Lifetime of the electronics is determined by adhesion between the Cu film and the PET substrate. The formation of an anisotropic nanostructure on the PET surface by surface modification can enhance Cu/PET interfacial adhesion. The shape and size of the anisotropic nanostructures of the PET surface can be controlled by varying the surface modification conditions. In this work, the effect of Cu/PET interface nanostructures on the failure mechanism of a Cu/PET flexible composite film is studied. From observation of the morphologies of the anisotropic nanostructures on plasma-treated PET surfaces, and cross-sections and surfaces of the fractured specimens, the Cu/PET interface area and nanostructure width are analyzed and the failure mechanism of the Cu/PET film is investigated. It is found that the failure mechanism of the Cu/PET flexible composite film depends on the shape and size of the plasmatreated PET surface nanostructures. Cu/PET interface nanostructures with maximal peel strength exhibit multiple craze-crack propagation behavior, while smaller or larger interface nanostructures exhibit single-path craze-crack propagation behavior.

• Geomechanics and Engineering
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• v.12 no.4
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• pp.657-673
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• 2017

Preventing water seepage and inrush into mines where close multiple-seam longwall mining is practiced is a challenging issue in the coal-rich Ordos region, China. To better protect surface (or ground) water and safely extract coal from seams beneath an aquifer, it is necessary to determine the height of the mining-induced fractured zone in the overburden strata. In situ investigations were carried out in panels 20107 (seam No. $2-2^{upper}$) and 20307 (seam No. $2-2^{middle}$) in the Gaojialiang colliery, Shendong Coalfield, China. Longwall mining-induced strata movement and overburden failure were monitored in boreholes using digital panoramic imaging and a deep hole multi-position extensometer. Our results indicate that after mining of the 20107 working face, the overburden of the failure zone can be divided into seven rock groups. The first group lies above the immediate roof (12.9 m above the top of the coal seam), and falls into the gob after the mining. The strata of the second group to the fifth group form the fractured zone (12.9-102.04 m above the coal seam) and the continuous deformation zone extends from the fifth group to the ground surface. After mining Panel 20307, a gap forms between the fifth rock group and the continuous deformation zone, widening rapidly. Then, the lower portion of the continuous deformation zone cracks and collapses into the fractured zone, extending the height of the failure zone to 87.1 m. Based on field data, a statistical formula for predicting the maximum height of overburden failure induced by close multiple seam mining is presented.

• Journal of Korean Society of Environmental Engineers
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• v.37 no.8
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• pp.465-471
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• 2015

Adsorption experiments for radionuclides such as $^3H$, $^{90}Sr$ and $^{99}Tc$ were conducted using fractured rock collected in unsaturated zone. The released radionuclide through artificial barrier from the near surface repository can be transported by the flow of rainfall or pore water through fractures in unsaturated zone and reach to groundwater flow. Therefore, it is important to investigate transport behavior (retardation) of radionuclides through fractured rock for the safety assessment and long-term performance of repository. Fractured rock samples were collected and characterized by X-ray microtomography (XMT) analysis, which can be used to develop a more robust unsaturated fracture transport model. When fracture-filling materials are exist, distribution coefficient of $^{90}Sr$ is higher than without fracture-filling materials. In this study, batch sorption distribution coefficient ($K_d$) of radionuclide was determined and used to increase our understanding of radionuclide retardtion through fracture-filling materials.

• Journal of Ocean Engineering and Technology
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• v.20 no.1 s.68
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• pp.16-19
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• 2006

With the fast growth of the shipbuilding industry, the number of lifting lugs used every year has reached onehundred. This paper is aimed at examining the cause of cracking in the hopper top plate, due to block lifting. First of all, we have investigated the fracture surface in the occurrence position of the crack of the hopper top plate, using the scanning electron microscope. In this study, we have evaluated the structural strength for COT super block under present lifting conditions. For this purpose, the equivalent stresses have been calculated by linear elastic analysis, using the finite element program ABAQUS.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.1
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• pp.91-98
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• 2008

One of the two spindles in the X-lift fractured suddenly during normal operation. The fracture occurred at the notch where the bending moment might be the maximum. Macrofractographic features associated with rotating-bending fatigue are evident on the fracture surface. The 3-D finite element analysis of the X-lift reveals that the spindle rotated under bending. The measured surface strain of the spindle varies cyclically as the spindle rotates. It supports that the spindle rotated under bending. The X-lift is not perfectly symmetrical with respect to both the horizontal and the vertical plane. The slightly unsymmetrical deformation can cause the bending of the spindle.

• Economic and Environmental Geology
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• v.33 no.4
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• pp.309-320
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• 2000

Aperture is an important parameter for determining the hydraulic characteristics of fractured media. In this study the topography of artificial rock joint surface was measured using 3D laser profilometer to analyze the aperture distribution. The initial aperture distribution was determined when the contact area became one percent of total joint surface. The initial aperture distribution of granite joint, with the mean value of 0.78 mm and the standard deviation of 0.34 mm was much different from that of the marble joint, with the mean value of 0.57 mm and the standard deviation of 0.26 mm. Apertures of both granite and marble showed normal distributions. Aperture distribution with the contact area of 25% was also analyzed. Mean value was decreased to one third compared to the initial aperture, but the standard deviation was decreased slightly. To determine the spatial correlation of the aperture distribution variogram analysis was carried out on the initial aperture data. Most experimental variograms were fitted well with exponential model. It is expected that the measured aperture characteristics can be used for stochastic analysis of fluid flow through rock joints.