• Tribology and Lubricants
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• v.33 no.6
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• pp.275-281
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• 2017

In this work, we have fabricated anodic aluminum oxide (AAO) with ordered nanoscale porosity through an anodization process. We deposited gold and nano-organic thin films on the porous AAO surface to protect its structure and reduce friction. We investigated the tribological characteristics of the porous AAO with respect to the protective surface coatings using tribometers. While investigating the frictional characteristics of the samples by applying normal forces of the order of micro-Newton, we observed that AAO without a protective coating exhibits the highest friction coefficient. In the presence of protective surface coatings, the friction coefficient decreases significantly. We applied normal forces of the order of milli-Newton during the tribotests to investigate the wear characteristics of AAO, and observed that AAO without protective surface coatings experiences severe damage due to the brittle nature of the oxide layer. We observed the presence of several pieces of fractured particles in the wear track; these fractured particles lead to an increase in the friction. However, by using surface coatings such as gold thin films and nano-organic thin films, we confirmed that the thin films with nanoscale thickness protect the AAO surface without exhibiting significant wear tracks and maintain a stable friction coefficient for the duration of the tribotests.

• Journal of Welding and Joining
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• v.21 no.7
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• pp.4-8
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• 2003

• Journal of Welding and Joining
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• v.22 no.1
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• pp.10-13
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• 2004

• Journal of the Korean institute of surface engineering
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• v.49 no.3
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• pp.260-264
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• 2016

In this study, fractured surface morphology and mechanical properties of Ni-Cr-Mo alloys with various contents of Mo for dental material use have been evaluated by mechanical test. The alloys used were Ni-13Cr-xMo alloys with Mo contents of 4, 6, 8, and 10 wt.%, prepared by using a vacuum arc-melting furnace. Ni-13Cr-xMo alloys were used for mechanical test without heat treatment. The phase and microstructure of alloys using an X-ray diffraction (XRD) and optical microscopy (OM) were evaluated. To examine the mechanical properties of alloys according to microstructure changes, the tensile test and the hardness test were carried out using tensile tester. To understand the mechanism of Mo addition to Ni-Cr alloy on mechanical property, the morphology and fractured surfaces of alloys were investigated by field-emission scanning electron microscope (FE-SEM). As a result, 79Ni-13Cr-8Mo alloy was verified that the tensile strength and the hardness were better than others. Varying Mo content, the changes of microstructures of alloys were identified by OM and SEM and that of 79Ni-13Cr-8Mo alloy was proved fabricated well. Microstructures of alloys were changed depending on Mo content ratio. It has been observed that 8% alloy had the most suitable mechanical property for dental alloy.

• Proceedings of the Korean Geotechical Society Conference
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• 2008.10a
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• pp.1571-1580
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• 2008

Subsea tunnels that link land to island and among nations for transportation, efficient development of limited surface and pursuit of economic development should be designed to support pore water pressure on the lining. It is generally constructed in the bed rock of the sea bottom. When the tunnel excavation face meets fractured-zones below sea bottom, collapse may occur due to an increase of pore water pressure and large inflow. Such an example can be found in the Norwegian subsea tunnel experiences in 1980's. In this study hydraulic behavior of tunnel heading is investigated using numerical method based on the collapse of Norwegian subsea tunnel. The effect of pore water pressure and inflow rate were mainly concerned. Horse-shoe shaped model tunnel which has 50 m depth from the sea bottom is considered. To evaluate hydraulic performance, parametric study was carried out for varying relative permeability. It is revealed that pore water pressure has increased with an increase of sea depth. Especially, at the fractured-zone, pore water pressure on the lining has increased significantly. Inflow rate into tunnel has also increased correspondingly with an increase in sea depth. S-shaped characteristic relation between relative permeability and normalized pore water pressure was obtained.

• Journal of the Korean Society for Heat Treatment
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• v.18 no.2
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• pp.83-90
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• 2005

Failure cause of the fractured engine parts was analyzed by microstructural observation. These parts were failed far earlier than the expected service life. By the stereoscope and SEM examinations of the fractured surface, the fracture modes have been identified as wear and fatigue failure. From the observation of microstructure and microhardness measurements of the failed gears, the probable cause for failures are internal oxidation during using and retained austenite and carbide networks due to heat-treatment, respectively. These defected structures at near surface contributed to the wear and fatigue failure.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1998.06b
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• pp.43-53
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• 1998

Heat - affected zones degenerated in cold forging die have been investigated to improve the tool life. There are many cases of heat-affected zone which are degenerated in manufacturing die and using the cold forging process. In order to define amounts of grinding inmanufacturing the toolfor cold forging, we have investigated the hardness and microstructure of surface layer after EDM. Considering the results of T.R.S. and compression test, it is likely that mechanical properties of tool have been decreased sharply if the heat-affected zones degenerated by EDM were not machined properly. also analyzed the tool surfac which is fractured during the cold forging. According to the microstructures and hardness distribution, surface of many tools have been degenerated in cold forging and fractured due to the heat-affected zone.

• Journal of Ocean Engineering and Technology
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• v.8 no.1
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• pp.114-122
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• 1994

X-ray stress constant, K, was determined for the diffraction line of (211)plane by using Cr-K$\alpha$ radiation. K was -340.87 MPa/deg. Fatigue crack propagation tests of SS41 steel were conducted under stress ratios of 0.1, 0.3 and 0.5. The half-value breadth of X-ray diffraction profile was measured at and beneath the fracture surface. The half-value breadth, B, on the fracture surface was found to increase with increasing $K_max$. The value of B was influenced by stress ratio in SS41 steel. The half-value breadth took the maximum value at the borden of reversed plastic zone, while it approached to the initial (pre-fatigue) value near the boundary of monotonic plastic zone. The maximum depth of the plasticzone was evaluated on the basis of the half-value breadth distribution. The depth $\omega$$_y$ is related to $K_max$by the following equation : $\omega$$_y$ = $\alpha$($K_max$/$\sigma$$_y$$)^2$ where .sigma.$\sigma$$_y$ is the yield strength obtength obtained in tension test .alpha.is 0.136 for SS41 steel.

• Transactions of the Korean Society of Automotive Engineers
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• v.7 no.8
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• pp.248-261
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• 1999

The fatigue life of mechanical components and structures has been influenced by mechanical, material and environmental conditions. It is important to search out the load type and size for accurate cause of fracture at the damaged surface of material. The fractographic method by x-ray diffraction can utilize residual stress $\sigma$_r and half-value breadth B and find out the types and the mechanical conditions of fracture. This study showed the relationship between fracture mechanical parameters $\Delta$K, $K_{max}$ and X-ray residual stress $\sigma$_r for normalized SS41 steel with homogeneous crystal structure and M.E.F. dual phase steel(martensite encapsulated islands of ferrite). The fatigue crack propagation tests were carried out under stress ratios 0.1 and 0.5. The x-ray diffraction technique according to crack propatation direction was applied to fatigue fractured surface. Residual stress $\sigma$_r was independent on stress ratios by arrangement of $\Delta$K. The equation of $\sigma$_r$\Delta$K was established by the experimental data. Therefore, fracture mechanical parameters can be estimated can be estimated by the measurement of X-ray parameters.

• Journal of Biomedical Engineering Research
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• v.16 no.4
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• pp.533-542
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• 1995

The present study investigated the effectiveness of pretreatment on dentin bonding. The adhesive resin was 5% 4-methacryloyloxyethyl trimellitate anhydride (4-META) in methyl methacrylate (MMA) combined with poly-MMA powder. Polymerization of this resin was initiated by tri-n-butyl borage (TBB). Ground bovine dentin samples were etched with either an aqueous solution of 10% citric (10-0 solution) (Group I) or aqueous solution of 10% citric acid and 3% ferric chloride(10-3 solution) (Group ll ). After etching, the primer (an aqueous solution of 35% hydroxyethyl methacrylate (HEM- A) and 5% glutaraldehyde was applied on the differently etched surfaces (Group III , Group IV). The 10-0 treatment showed the lowest tensile bond strength, followed by the 10-3 treatment, primer application after the 10-0 treatment and primer application after the 10-3 treatment. The relationship among the surface morphology after pretreatment, fractured surface morphology and tensile bond strength was examined. It revealed that the surface morphology change by different pretreatment influenced the bond strength and the resulting fractured surface morphology. The correlation of tensile bond strength with the fracture morphology was explained.