• Applied Microscopy
• /
• v.26 no.4
• /
• pp.447-456
• /
• 1996

Fracture surfaces of materials contain useful information ranging from crack path to the mechanism of fracture. Since limitation of electron transparency requires a sample in the form of thin foil for TEM observations, it is impossible to extract such information directly from the fracture surfaces. In this study, the method of surface replication from the ceramic fracture surface is employed to characterize the process of crack propagation in ceramic matrix composites using TEM analysis. The surface replica from the fracture surface in ceramic materials provides detailed surface morphology and more importantly, loosened particles on the fracture surface are collected. Electron diffraction and chemical composition analyses of these particles reveal crack path in the specimen. Furthermore, one can determine the mode of fracture by observing the fracture surface morphology from the image of replica. Two examples are given to illustrate the potential of the surface replication technique. In the first example, apparent toughness increase in $B_{4}C-Al$ composites at high strain rate is investigated by surface replication to elucidate the mechanism of fracture at different strain rates. The polytypes of SiC formed during the sintering of SiC-AlN composite and their effect on the fracture behavior of SiC-AlN composite are analyzed in the second example.

• Journal of Biomedical Engineering Research
• /
• v.19 no.5
• /
• pp.433-441
• /
• 1998

This study was performed to evaluate the effects of surface flaw on the fracture of all-ceramic materials. A feldspathic porce lain of VMK68, a cashable ceramic of IPS-Empress, and an alumina-glass composite of In-Ceram were used. Specimens were prepared as 12$\times$3$\times$1mm in dimensions, and a Vickers-produced indentation crack was made at the center of the tensile surface. Test specimens were immersed in dlstilled water and In oil, which were broken under a crosshead speed of 0.05 mm/min by 3-point bend test at 37$^{\circ}C$. The characteristic patterns of Vickers indentation and fracture surfaces were examined by an optical microscope and a scanning electron microscope. The fracture surfaces of the VMK68 and the IPS-Empress showed a median crack pattern at the fracture origin and indicated a tendency to cleavage hackle. The fracture surface of the alumina-glass composite, In-Ceram, showed a Palmqvist crack pattern at the fracture origin and indicated a tendency of toughening by the frictional Interlocking between the microstructurally rough fracture surfaces.

• Analytical Science and Technology
• /
• v.5 no.2
• /
• pp.203-211
• /
• 1992

Fracture behavior and martensite substructure of Ni-36.5at.%Al alloy were investigated with the addition of vanadium which is known as scavenging element of grain boundary. The fracture surfaces were examined by scanning electron microscopy and the EDX spectrometer was applied for composition analysis of fracture surfaces. The substructure of martensite was studied by transmission electron microscopy. By addition of vanadium, fracture surfaces show mixed modes of intergranular and transgranular fracture and more Al content is found on the grain boundaries. For Ni-36.5at.%Al alloy, the planar faults observed in the martensite plates are the internal twins. By increasing the vanadium content, the modulated structure with stacking faults and dislocations dominates while the twinned martensite disappears. The stacking fault is determined to be extrinsic due to the substitution of V for Al. It is concluded that the segregation of sulfur on the high-energy state stacking fault area suppresses the intergranular fracture.

• The Journal of Advanced Prosthodontics
• /
• v.9 no.1
• /
• pp.22-30
• /
• 2017

PURPOSE. The aim of this study was to investigate the effect of reinforcing materials on the fracture resistances of glass fiber mesh- and Cr-Co metal mesh-reinforced maxillary complete dentures under fatigue loading. MATERIALS AND METHODS. Glass fiber mesh- and Cr-Co mesh-reinforced maxillary complete dentures were fabricated using silicone molds and acrylic resin. A control group was prepared with no reinforcement (n = 15 per group). After fatigue loading was applied using a chewing simulator, fracture resistance was measured by a universal testing machine. The fracture patterns were analyzed and the fractured surfaces were observed by scanning electron microscopy. RESULTS. After cyclic loading, none of the dentures showed cracks or fractures. During fracture resistance testing, all unreinforced dentures experienced complete fracture. The mesh-reinforced dentures primarily showed posterior framework fracture. Deformation of the all-metal framework caused the metal mesh-reinforced denture to exhibit the highest fracture resistance, followed by the glass fiber mesh-reinforced denture (P<.05) and the control group (P<.05). The glass fiber mesh-reinforced denture primarily maintained its original shape with unbroken fibers. River line pattern of the control group, dimples and interdendritic fractures of the metal mesh group, and radial fracture lines of the glass fiber group were observed on the fractured surfaces. CONCLUSION. The glass fiber mesh-reinforced denture exhibits a fracture resistance higher than that of the unreinforced denture, but lower than that of the metal mesh-reinforced denture because of the deformation of the metal mesh. The glass fiber mesh-reinforced denture maintains its shape even after fracture, indicating the possibility of easier repair.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.35 no.1
• /
• pp.58-65
• /
• 2007

Mixed mode interlaminar fracture behaviors of carbon fabric/epoxy composites were investigated through MMF (Mixed Mode Flexural) test by varying mixed mode ratio ranging from 20% to 90%. Mixed mode interlaminar fracture criteria based on NL point and 5% offset point were also suggested in order to predict mixed mode interlaminar fracture behaviors. Fracture surfaces and crack propagating behaviors were examined through a travelling scope and a scanning electron microscope. According to the results, mixed mode interlaminar fracture behaviors can be predicted by mixed mode interlaminar fracture criterion with m=1.5 and n=0.5 on the basis of NL point or mixed mode interlaminar fracture criterion with m=2 and n=3 on the basis of 5% offset point. Fracture surfaces and crack propagating behaviors are sensitive to mixed mode ratios. MMF test can be successfully applicable in evaluating mixed mode interlaminar fracture toughness of carbon fabric/epoxy composites.

• Journal of the Korean Ceramic Society
• /
• v.26 no.5
• /
• pp.645-654
• /
• 1989

Specimens of WC-Co were indented to measure the resulting crack size and unindented samples were fractured in 3-point flexure to obtain the strength and to measure characteristic features on the fracture surface. Fracture toughness was determined using fractography and compared to those determined using identation techniques. We show that principles of fracture mechanics can be applied WC-Co composites and can be used to analyze the fracture process. The fracture surfaces were examined by scanning electron microscopy and optical microscopy. Characteristic feature observed in glasses, single crystals and polycrystalline materials known as mirror, mist, hackle, and crack branching were identified for these composites. We discuss the importance of fracture surface analysis in determining the failure-initiating sources and the failure behaviorof WC-Co composites.

• Journal of Dental Rehabilitation and Applied Science
• /
• v.26 no.4
• /
• pp.373-388
• /
• 2010

Fracture causes serious problems in many instance of prosthetic failures. But it is hard to find the definite causes when fractures occur. Fractography encompasses the examination of fracture surfaces that contain features resulting from the interaction of the advancing crack with the microstructure of the material and the stress fields. All fractured specimens(implant retaining screw) retrieved from Gangneung-Wonju national university dental hospital for 3 years(from 2007 to 2009). After pretreatment of samples, the scanning electon microscope were used for surface examination and fracture analysis. In case of most of the fractured specimens, fracture took place by fatigue fracture and fractured surface represents fatigue striation. Fatigue striation indicate the progression of the crack front under cyclic loading, are characteristic of stage 2 crack growth. The site of crack initiation and stage 1 crack growth were not easily identified in any of the failure, presumably because of the complex microstructural features of the polycrystalline sample. In case of fractured by overload, dimpled or cleavage surface were observed. Using the interpretation of characteristic markings(ratchet mark, fatigue striation, dimple, cleavage et al) in fracture surfaces, failure events containing the crack origin, crack propagation, material deficiency could be understand. Using the interpretation of characteristic markings in fracture surfaces, cause and mechanism of fractures could be analyzed.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.26 no.5
• /
• pp.835-842
• /
• 2002

In this paper, static and fatigue bending strengths and failure mechanisms of CFRP (carbon fiber reinforced plastics) laminates having impact damages have been evaluated. Composite laminates used for this experiment are CF/EPOXY orthotropy laminated plates, which have two-interfaces $[0^0_ 4/90^0_4]_{ sym}$. A steel ball launched by the air gun collides against CFRP laminates to generate impact damages. The damage growth during bending fatigue test is observed by the scanning acoustic microscope (SAM) and also, the fracture surfaces were observed by using the SEM (scanning electron microscope). In the case of impacted-side compression, fracture is propagated from the transverse crack generated near impact point. On the other hand, fracture is developed toward the impact point from the edge of interface-B delamination in the case of impacted-side tension. Eventually, failure mechanisms have been confirmed based on the observed delamination areas and fracture surfaces.

• Explosives and Blasting
• /
• v.26 no.1
• /
• pp.57-66
• /
• 2008

It has been proven that the pre-cracking notches in a blasting hole are applicable to control crack growth along specific direction. This study compared the roughnesses of the fracture plane resulting from test blasts using a regular charge hole and notched charge hole to investigate the effect of the notches of charge hole on the formation of fracture plane. A notch bit system was used to drill the notched hole in the rock specimens. The surfaces of the fracture planes were reconstructed as Digital Elevation Model (DEM) using digital photogrammetric method and the roughnesses of the surfaces were estimated with Surface Roughness Profile Index (SRp).

• Proceedings of the KSME Conference
• /
• 2001.11a
• /
• pp.9-15
• /
• 2001

In the case of a crack propagation, a portion of the work of inelastic deformation near the crack tip is dissipated as heat. In order to understand the thermal effect on fracture toughness, tensile test was carried out using thermocouples to monitor the variation of temperature with SA516 Gr70. The experimental results show that the temperature of specimen was increased $3.6^{\circ}C$ at static load condition. And the thermal effect was investigated connected with the steady-state stress in the vicinity of a crack propagation in the elastic-plastic C-T specimen theoretically. And fracture toughness, the energy to make crack surfaces, presented correctively. The fracture toughness with considering heat at the blunting of the crack tip ws lower about 19.3% than that of ignoring heat. So, it is resonable to apply the fracture toughness with considering thermal energy and it would be good explanation for constraint effect depending on the configuration in the presence of excessive plasticity.