• Title/Summary/Keyword: fracture characteristic

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Effects of Aging on Properties of MgO-Partially Stabilized Zirconia (마그네시아 부분안정화 지르코니아 소결체의 특성에 미치는 열처리 효과)

  • 정형진;오영제;이홍림
    • Journal of the Korean Ceramic Society
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    • v.24 no.3
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    • pp.243-250
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    • 1987
  • The effects aging on some properties and thermal-shock behavior of zirconia partially stabilized with 9 mol% MgO (9MZ) were studied. 9MZ specimens were aged over $1200^{\circ}$-$1400^{\circ}C$ for 12hours subsequently, after sintering at $1650^{\circ}C$ for 4 hours. Fracture strength(both before and after thermal-shock test), linear thermal expansion, monoclinic fraction and phase transition by XRD, density, galvanic potential and microstructure were measured. Quantitative chemical analysis around the grain-boundary of the specimen aged at $1350^{\circ}C$ was also conducted by EDX. The aging of 9MZ specimen causes a thermal decomposition of cubic-$ZrO^{2}$ into the formation metastable tetragonal-$ZrO^{2}$ and MgO. The former increases the residual strength after thermal-shock test and the latter improves the thermal-shock resistance due to thermal conduction through the continuous magnesia phase and the formation of monoclinic phase content in matrix were increased with decreasing the aging temperature from $1400^{\circ}C$ to $1200^{\circ}C$. Galvanic potential of the aged specimen exhibited a proper emf characteristic.

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Relationships between Gas Hydrate Occurrence Types and Sediment Characteristics in the Ulleung Basin, East Sea (동해 울릉분지의 가스 하이드레이트 산출형태와 퇴적물 특성의 관계)

  • Kim, Dae-Ha;Bahk, Jang-Jun;Lee, Jin-Heuck;Ryu, Byong-Jae;Kim, Ji-Hoon;Chun, Jong-Hwa;Torres, Marta E.;Chang, Chan-Dong
    • Economic and Environmental Geology
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    • v.45 no.4
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    • pp.397-406
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    • 2012
  • During the 2nd Ulleung Basin Gas Hydrate Drilling Expedition (UBGH2) in 2010, gas-hydrate-bearing sediment cores were recovered at 10 drill sites. Base, on Infrared (IR) thermal image and grain-size analysis of the cores, three distinct types of gas hydrate are classified: Type I (fracture-filling in mud layers), Type II (disseminated in mud layers), and Type III (pore-filling in sand layers). Types I and II gas hydrates occur in mud as discrete veins, nodules or disseminated particles. Type III fills the pore spaces of the sand layers encased in mud layers. In this case, the sand content of hosting sediments shows a general linear relationship with gas hydrate saturation. The degrees of temperature anomalies (${\Delta}T$) from IR images generally increase with gas hydrate saturation regardless of gas hydrate occurrence types. Type I is dominantly found in the sites where seismic profiles delineate chimney structures, whereas Type II where the drill cores are composed almost of mud layers. Type III was mainly recovered from the sites where hemipelagic muds are frequently intercalated with turbidite sand layers. Our results indicate that gas hydrate occurrence is closely related to sedimentological characteristic of gas hydrate-bearing sediments, that is, grain size distribution.

A Study on Mineralogical Characteristic and Accelerated Weather Test of Red and Yellow Color Natural Inorganic Pigments (적색 및 황색 계열의 천연 무기안료의 광물학적 특성 및 촉진내후성 평가 연구)

  • Park, Ju Hyun;Jeong, Hye Yeong
    • Journal of the Mineralogical Society of Korea
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    • v.32 no.4
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    • pp.259-271
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    • 2019
  • We evaluated mineralogical, physical property and accelerated weather resistance of cinnabar, realgar and orpiment used as cultural heritages and traditional paintings. JB and JS are sample names of cinnabar and JH and UH are sample names of orpiment and Realgar, respectively. As a result of mineralogical property evaluation, Jinsa was identified cinnabar (HgS) and there was no difference in chemical composition according to the grade. UH and JH were confirmed realgar (AsS) and orpiment (As2S3), respectively. The polarization characteristics such as shape and color indicate that pigments using our test were natural mineral pigment observed by polarization microscope. Especially, in the case of cinnabar, it is not easy to distinguish between natural mineral pigment and synthetic pigment. But the results of polarization microscope said that cinnabar is natural occurring mineral which have authentic mineral particle and unevenly fracture. As a result of thermal analysis, JH has a higher glass transition temperature and heat stability than UH. After accelerated weather test, cinnabar, realgar and orpiment were striking result in color change because of light degradation. Red color of cinnabar turn into black and the color of realgar and orpiment became brighter than before. JB (meta-cinnabar) is more photosensitivity and faster becoming dark than JB (cinnabar). Finally light transforms realgar (red, As4S4) in arsenolite (As2O3).

Studies on Transport Mechanisms of Turtle Bladder I . Epithelium of Urinary Bladder (Turtle bladder의 수송기작(輸送機作)에 관한 연구 : I. 방광(膀胱)의 상피조직(上皮組織))

  • Jeon, Jin-Seok
    • Applied Microscopy
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    • v.19 no.2
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    • pp.119-137
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    • 1989
  • It has been shown in this and earlier investigation that the turtle bladder mucosa has three main cell types on their mucosal surface. They are the granular cells, ${\alpha}$ CA cells, and ${\beta}$ CA cells. The three major transport mechanisms that occurs in the turtle bladder are sodium reabsorption, proton secretion, and bicarbonate secretion. In the present work the trans-port mechanisms by bladder epithelial cells of freshwater turtle, Pseudemys scripta, are summarized as follows. 1. The granular cells play an important role in sodium transport, while the ${\alpha}$ and ${\beta}$ CA cells do not appear to play a determining role in sodium transport. 2. It appears that the active sodium transport in the granular cells occurs in two-step process, implying that first, sodium diffuses into the cells, followed by an energy-dependent efflux step, which is catalyzed by the ouabain-sensitive Na-K ATPase. 3. The ${\alpha}$ type of CA cells are responsible for the proton secretion using the proton pump on the apical plasma membrane, while the ${\beta}$ type of CA cells are believed to be responsible for bicarbonate secretion. 4. When looked at under freeze-fracture electron microscopy, the apical plasma membrane of ${\alpha}$ cells have a characteristic population of rod-shaped intramembranous particles which are believed to be components of the proton pumps. Conversely, ${\beta}$ type of CA cells show rod-shaped particles in their basolateral plasma membranes, which is consistent with the proton absorptive, bicarbonate secretory mechanism. 5. In the turtle bladder, the ${\alpha}$ and ${\beta}$ type of cells are believed to be both responsible for proton transport, but in opposite directions.

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Electrochemical Properties of Needle Coke through a Simple Carbon Coating Process for Lithium Ion Battery (침상 코크스의 피치 코팅에 따른 리튬 이차전지 탄소계 음극소재의 전기화학적 특성)

  • Hwang, Jin Ung;Lee, Jong Dae;Im, Ji Sun
    • Applied Chemistry for Engineering
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    • v.31 no.5
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    • pp.514-519
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    • 2020
  • Graphite materials for lithium ion battery anode materials are the most commercially available due to their structural stability and low price. Recently, research efforts have been conducted on carbon coatings by improving side reactions at the edge site of carbon materials. The carbon coating process has classified into a CVD by chemical reaction, wet coating process with solvent and dry coating by mechanical impact. In this paper, the rapid crush/coating process was used to solve the problem of which only few parts of the carbon precursor (pitch) can be used and also environmental problems caused by solvent removal in the wet coating process. When the ratio of needle coke to pitch was 8 : 2 wt%, and the rapid crush/coating process was carried out, it was confirmed that the fracture surface was coated by pitch. The pitch-coated sample was treated at 2400 ℃ and 41.8% improvement in 10C/0.1C rate characteristic was observed. It is considered that the material simply manufactured through the simple crush/coating process can be used as an anode electrode material for a lithium ion battery.

Characteristic of Intermetallic Compounds for Aging of Lead Free Solders Applied to 48 $\mu$BGA (48 $\mu$BGA에 적용한 무연솔더의 시효처리에 대한 금속간화합물의 특성)

  • Shin, Young-Eui;Lee, Suk;Fujimoto, Kozo;Kim, Jong-Min
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.3
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    • pp.37-42
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    • 2001
  • The concerns of the toxicity and health hazard of lead in solders have demanded the research to find suitable lead-free solder alloys. It was discussed that effect of the intermetallic formation and structure on the reliability of solder joints. In this study, lead-free solder alloys with compositions of Sn/3.5Ag/0.75Cu, Sn/2.0Ag/0.5Cu/2.0Bi were applied to the 48 $\mu$BGA packages. Also, the lead-free solder alloys compared with eutectic Sn/37Pb solder using shear test under various aging temperature. Common $\mu$BGA with solder components was aged at $130^{\circ}C$, $150^{\circ}C$ and $170^{\circ}C$. And the each temperature applied to 300, 600 and 900 hours. The thickness of the intermetallics was measured for each condition and the activation energy for their growth was computed. The fracture surfaces were analyzed using SEM (Scanning Electron Microscope) with EDS (Energy Dispersive Spectroscopy). These results for reliability of lead-free interconnections are discussed.

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Evaluation of mechanical Characteristic according to the Filler Metal by GTA welding Process using 7075 Aluminum Alloy (알루미늄 합금 7075의 용가재에 따른 GTA용접공정의 기계적 특성 평가)

  • Son, Yeong-San;Lim, Byung-Chul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.4
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    • pp.521-526
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    • 2017
  • In the GTA welding process of Al 7075 alloy using different types of filler metals, the tensile test and micro-hardness test were conducted to evaluate the mechanical characteristics. Also, the radiographic test result showed that the weld met the criterion of level 1 in accordance with KS D 0242 for verifying the welding integrity and there were no welding defects. The tensile test result obtained using Al 7075 as a filler metal showed that the material was fractured in the weld zone. The tensile strengths of the materials using Al 7075 and ER 4043 as the filler metal were about 240MPa and 253MPa, their yield strengths were about 132MPa and 120MPa and their elongation percentages were 6.6% and 13%, respectively. The micro-hardness value of the deposited metal zone when using Al 7075 as the filler metal was Hv 132. However, the micro-hardness of the material using ER4043 as the filler metal was about 24% lower than that using Al 7075. When the chemical composition of the filler metal is the same as that of the material itself, fracture can occur in the deposited metal zone. Therefore, it is not desirable to use the same material as the filler metal for the welding of Al 7075 alloy. Moreover, the use of Al-Si based ER 4043 as a filler metal is more desirable than using the same material as a filler metal for welding Al 7075.

Numerical Analysis for Dynamic Behavioral Characteristics of Submerged Floating Tunnel according to Shore Connection Designs (지반 접속부 설계에 따른 수중터널의 동적 거동 특성에 대한 수치해석적 연구)

  • Seok-Jun, Kang;Joohyun, Park;Gye-Chun, Cho
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.25 no.1
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    • pp.27-41
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    • 2023
  • Submerged floating tunnels must be connected to the ground to connect continents. The displacement imbalance at the shore connection between the underground bored tunnel and submerged floating tunnel can cause stress concentration, accompanying a fracture at the shore connection. The elastic joint has been proposed as a method to relive the stress concentration, however, the effect of the elastic joints on the dynamic behavior should be evaluated. In this study, the submerged floating tunnel and shore connection under dynamic load conditions were simulated through numerical analysis using a numerical model verified through a small-scaled physical model test. The resonant frequency was considered as a dynamic behavioral characteristic of the tunnel under the impact load, and it was confirmed that the stiffness of the elastic joint and the resonant frequency exhibit a power function relationship. When the shore connection is designed with a soft joint, the resonant frequency of the tunnel is reduced, which not only increases the risk of resonance in the marine environment where a dynamic load of low frequency is applied, but also greatly increases the maximum velocity of tunnel when resonance occurs.

Domestic Disabled People's Use of Dental Service Institutes and Their Oral Health Related Quality of Life (재가 장애인의 구강진료기관 이용실태와 구강건강관련 삶의 질)

  • Lee, Hyun-Ok;Yang, Chun-Ho;Kim Jin;Kim, Young-Im
    • Journal of dental hygiene science
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    • v.9 no.5
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    • pp.593-600
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    • 2009
  • In this study, disabled people's life quality according to their use of dental healthcare services were examined, and the factors that influence their life quality were examined. The subjects in this study were 198 domestic disabled people in Jeollabuk-do, on whom a survey was conducted from May 1 to June 1, 2008. After the collected data were analyzed with SPSS WIN 12.0 program, the following findings were acquired: 1. 68.2% of the subjects had an experience of using dental service institutes. Over 80.0% of the physically disabled, the mentally handicapped, and the sensory-disturbance sufferers each used dental service institutes in their locations. Regarding the reason for visiting dental service institutes, 43.4% of the physically disabled visited for regular examination (the largest group for that reason), followed by the mentally handicapped with 37.9%. 43.5% of the sensory-disturbance sufferers visited for pain and fracture. 2. The subjects' life quality level relating to oral health was found to be an average 3.39 point score. There was a statistically significant difference in their life quality levels in terms of demographic features, such as age, religion, marriage/non-marriage, education, and subjective health status variables. Those experienced in using dental service institutes enjoyed higher levels of life quality (p=.011). And, with regard to disability characteristics, the degree of disability and the period of disability influenced the quality of life with a statistical significance. 3. Regarding variables influencing the life quality of subjects, in terms of general characteristic variables, subjective health status were influential variables, and in terms of characteristic variables relating to the use of dental clinics and disability, the experience of using dental service institutes influenced the quality of life. In conclusion, nationwide efforts to nurture separate dental personnels responsible for the disabled, to expand relevant facilities and to improve the health care insurance are required to promote the oral health of domestic disabled people's.

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A preliminary numerical analysis on the behaviour of tunnel under construction in fracture zone considering seismic load (지진 하중을 고려한 단층파쇄대에서의 시공 중 터널 거동 분석에 관한 수치해석적 연구)

  • Oh, Dong-Wook;Hong, Soon-Kyo;Kim, Dae-Kon;Lee, Yong-Joo
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.21 no.2
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    • pp.279-299
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    • 2019
  • Recently occurred earthquake Gyeongju and Pohang served as a momentum to remind that Korean peninsular is not a safety zone from earthquake anymore. The importance of seismic design, therefore, have been realized and researches regarding design response spectrum have been actively carried out by many researchers and engineers. Current tunnel seismic design method is conducted to check safety of tunnel structure by dynamic numerical analysis with condition of completed lining installation, so, it is impossible to consider safety of tunnel behavior under construction. In this study, therefore, dynamic numerical analysis considering seismic wave propagations has been performed after back analysis using results from field monitoring of tunnel under construction in fractured zone and 1st reinforcement (shotcrete, rockbolt) behaviour are analyzed. Waves are classified by period characteristic (short and long). As a result, the difference depending on period characteristic is minor, and increasements of displacement are obtained at crown displacement due to seismic wave is 28~31%, 14~16% at left side of tunnel in the fractured zone, 13~27% at right side of tunnel in the bed rock, respectively. In case of shotcrete axial force is increased 113~115% at tunnel crown, 102% at left side, 106~110% at right side, respectively. Displacement and axial force of rockbolts which are selected by type of anchored grounds (only fractured zone, fractured zone and bed rock, only bedrock) are analyzed, as a result, rockbolt which is anchored to fractured zone and bed rock at the same time are weaker than any other case.