• Steel and Composite Structures
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• 제20권5호
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• pp.999-1022
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• 2016

The use of Carbon Fiber Reinforced Polymer (CFRP) to strengthen steel structures has attracted the attention of researchers greatly. Previous studies demonstrated bonding of CFRP plates to the steel sections has been a successful method to increase the mechanical properties. However, the main limitation to popular use of steel/CFRP strengthening system is the concern on durability of bonding between steel and CFRP in various environmental conditions. The paper evaluates the performance of I-section steel beams strengthened with pultruded CFRP plate on the bottom flange after exposure to diverse conditions including natural tropical climate, wet/dry cycles, plain water, salt water and acidic solution. Four-point bending tests were performed at specific intervals and the mechanical properties were compared to the control beam. Besides, the ductility of the strengthened beams and distribution of shear stress in adhesive layer were investigated thoroughly. The study found the adhesive layer was the critical part and the performance of the system related directly to its behavior. The highest strength degradation was observed for the beams immersed in salt water around 18% after 8 months exposure. Besides, the ductility of all strengthened beams increased after exposure. A theoretical procedure was employed to model the degradation of epoxy adhesive.

• 마이크로전자및패키징학회지
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• 제11권2호
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• pp.23-28
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• 2004

본 실험에서는 Ag 층을 이용한 무 플럭스 접합 공정을 개발하였으며 Ag의 유무에 따른 효과를 관찰하기 위해 In ($10{\mu}m$)과 Sn ($10{\mu}m$)솔더 및 Ag (100 nm)/In과 Ag/Sn 솔더를 thermal evaporation 방법으로 하부 금속층 위에 형성하였다. 접합부의 접촉저항과 전단 하중을 측정하기 위해 쿠폰시편을 제조하였으며 이리한 쿠폰시편은 $130^{\circ}C$에서 0.8, 1.6, 3.2 MPa의 접합압력을 가하여 30초간 접합을 실시하였다. 전단하중과 4단자 저항측정법을 이용하여 접합부의 특성을 분석하였으며 주사전자현미경(Scanning Electron Microscope), EDS (Energy Dispersive Spectrometry)과 X-ray mapping을 통해 접합부를 관찰하였다. 전단하중 측정 결과 0.8 MPa에서는 In-Sn 솔더의 접합이 이루어지지 않았으며 접합압력이 증가해도 Ag/In-Ag/Sn 시편의 전단하중 측정값이 In-Sn 시편에 비해 높게 나타났다. 접합부의 저항감은 $2-4\;m{\Omega}$을 나타내었으며 접합압력이 증가할수록 In-Sn 혼합층이 더 많이 관찰되었다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1996년도 춘계학술대회 논문집
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• pp.220-223
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• 1996

Mechanical properties of Plasma-Enhanced Chemical Vapor Deposited (PECVD) silicon nitride thin film was studied to determine the feasibility of the film as a passivation layer over the aluminum bonding areas of integrated circuit chips. Ultimate strain of the films in thicknesses of about 5 k${\AA}$ was measured using four-point bending method. The ultimate strain of these films was constant at about 0.2% regardless of residual stress. Intrinsic and residual stresses of these films were measured and compared with thermal shock and cycling test results. Comparison of the results showed that more tensile films were more susceptible to crack- induced failure.

• 한국철도학회:학술대회논문집
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• 한국철도학회 2009년도 춘계학술대회 논문집
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• pp.574-580
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• 2009

This study is investigate the bending behavior of real size RC beams strengthened with carbon fiber sheets. For experimental study, 1 control beam and 8 strengthened beams of real size(4 NU-beams and 4 U-beams) are tested and compared. NU-beam has not a V-shaped band and V-beam has a V-shaped band. The variables of experiment are composed of the number of carbon fiber sheets, the existence of U-shaped band, and four point loading, etc. The experimental results showed that the strengthening system with U-shaped band controls the premature debonding and provides a more ductile failure mode than the strengthening system without V-shaped band. It can be found from the load-deflection curves that as the number of fiber sheets is increased, the maximum strength and the flexural rigidity is increased. For the strengthening method with carbon fiber sheets of the real size RC beams, it is required the finding a solution to the bonding problem.

• Restorative Dentistry and Endodontics
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• 제13권1호
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• pp.103-111
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• 1988

The purpose of this study was to, examine the sealing ability of the denting bonding agent, when used with gutta percha cone, as a root canal sealer. Seventy two upper and lower extracted human teeth with single root were randomly selected and instrumented in a conventional method with K-file. After instrumentation and dry the canal with paper point, there were divided into three groups and twenty four teeth in each group were filled with the following material; In group I: Scotchbond in combination with gutta percha cone. In group II: AH 26 in combination with gutta percha cone. In group III: Tubli-Seal in combination with gutta percha cone. All specimens were immersed in Indian Ink, decalcified, and cleared. The depth of dye penetration into the canals were evaluated by caliper at the intervals of 1 day, 1 week, 2 weeks. The results were as follows; 1. Depth of dye penetration for all groups increased with time. 2. As to difference in mean dye penetration at time interval of 1 day and 14 days, Scotchbond group exhibited the smallest value as 0.53mm and Tubli-Seal group exhibited the largest value as 0.70mm. 3. There was the difference of dye penetration between each group, but its difference was not significant, statistically.

• 한국가시화정보학회지
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• 제18권3호
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• pp.61-68
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• 2020

Thermographic phosphor (TP) thermometry is a noncontact optical measurement method and has been applied in many fields such as combustion and heat transfer. However, due to the limitation of bonding technology and measurement method, most TP thermometry studies were conducted only on the air environment with water-soluble binders. In this paper, a temperature measurement technology in water using TP is proposed by coatings of manganese activated magnesium fluorogermanate (Mg4FGeO6:Mn4+, MFG) with Polydimethylsiloxane (PDMS). Four MFG-PDMS coatings with different thicknesses were prepared. The lifetime of MFG was not affected by the thickness of the coating as a result of the experiment and analysis of phosphor intensity using a photomultiplier tube. To measure the surface temperature field of an immerged body in water, a cylinder-type cartridge heater was coated with MFG doped PDMS. Transient surface temperature field was successfully measured even the initial temperature is higher than the boiling point of water.

• Smart Structures and Systems
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• 제16권1호
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• pp.67-79
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• 2015

Acoustic emission analysis is an effective technique for monitoring the evolution of damage in a structure. An experimental analysis on a set of reinforced concrete beams under flexural loading was carried out. A mixed AE analysis method which used both parameter-based and signal-based techniques was presented to characterize and identify different failure mechanisms of damage, where the signal-based analysis was performed by using the Hilbert-Huang transform. The maximum instantaneous energy of typical damage events and the corresponding frequency characteristics were established, which provided a quantitative assessment of reinforced concrete beam using AE technique. In the bending tests, a "pitch-catch" system was mounted on a steel bar to assess bonding state of the steel bar in concrete. To better understand the AE behavior of bond-slip damage between steel bar and concrete, a special bond-slip test called pullout test was also performed. The results provided the basis of quantitative AE to identify both failure mechanisms and level of damages of civil engineering structures.

• 한국산학기술학회논문지
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• 제21권11호
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• pp.86-93
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• 2020

국내 사회기반 시설물의 경우 70년대 이후로 건설되어 향후 신규건설에 대한 수요보다 유지보수에 대한 수요가 크게 증가할 것으로 전망된다. 더욱이 경주지진과 포항지진 이후로 과거 시공된 시설물의 내진성능에 대한 평가 및 보수 보강 사업이 이루어지고 있다. 본 연구에서는 보강공법 중 L형 GFRP 외부부착공법을 대상으로 하여 시험체를 설계하고, 에폭시와 화약식 타정 총으로 압력 핀을 시공하는 방법으로 외부부착된 L형 GFRP Plate의 보강효과를 확인하기 위하여 4점 휨 시험을 수행하였다. 실험결과를 바탕으로 L형 GFRP Plate의 보강효과를 확인하고, 국내의 "복합신소재시스템에 의한 철근콘크리트구조물의 보강설계 및 시공 지침서"에 따라 L형 GFRP 외부부착공법이 적용된 보의 거동에 대하여 평가하고 에폭시와 압력 핀을 조합하여 시공하는 부착방법의 효용성을 평가하였다. 실험 결과를 분석한 결과 지침에 따른 설계는 부재의 강도를 잘 예측하는 것으로 나타났으나, GFRP Plate 보강재의 손상을 동반하는 고정법의 사용으로 인하여 설계가정의 조건을 만족하는 파괴가 일어나지 않는 것으로 분석하였다.

• Computers and Concrete
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• 제29권 6호
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• pp.393-405
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• 2022

Lightweight concrete is a superior material due to its light weight and high strength. There however remain significant lacunae in engineering knowledge with regards to shear failure of lightweight fiber reinforced concrete beams. The main aim of the present study is to investigate the optimum usage of steel fibers in lightweight fiber reinforced concrete (LWFRC). Multi-scale finite element model calibrated with experimental results is developed to study the effect of steel fibers on the mechanical properties of LWFRC beams. To decrease the amount of steel fibers, it is preferred to reinforce only the middle section of the LWFRC beams, where the flexural stresses are higher. For numerical simulation, a multi-scale finite element model was developed. The cement matrix was modeled as homogeneous and uniform material and both steel fibers and lightweight coarse aggregates were randomly distributed within the matrix. Considering more realistic assumptions, the bonding between fibers and cement matrix was considered with the Cohesive Zone Model (CZM) and its parameters were determined using the model update method. Furthermore, conformity of Load-Crack Mouth Opening Displacement (CMOD) curves obtained from numerical modeling and experimental test results of notched beams under center-point loading tests were investigated. Validating the finite element model results with experimental tests, the effects of fibers' volume fraction, and the length of the reinforced middle section, on flexural and residual strengths of LWFRC, were studied. Results indicate that using steel fibers in a specified length of the concrete beam with high flexural stresses, and considerable savings can be achieved in using steel fibers. Reducing the length of the reinforced middle section from 50 to 30 cm in specimens containing 10 kg/m3 of steel fibers, resulting in a considerable decrease of the used steel fibers by four times, whereas only a 7% reduction in bearing capacity was observed. Therefore, determining an appropriate length of the reinforced middle section is an essential parameter in reducing fibers, usage leading to more affordable construction costs.

• Bulletin of the Korean Chemical Society
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• 제35권12호
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• pp.3495-3501
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• 2014

A novel crystal, the mono-protonated metformin acetate (1), was obtained and characterized by elemental analysis, IR spectroscopy and X-ray crystallography. It was found that one of the imino group in the metformin cation was protonated along with the proton transfer from the secondary amino group to the other imino group. Its crystal structure was then compared with the previously reported diprotonated metformin oxalate (2). The difference between them is that the mono-protonated metformin cations can be linked by hydrogen bonding to form dimers while the diprotonated metformin cations cannot. Both of them are stabilized by intermolecular hydrogen bonds to assemble a 3-D supermolecular structure. The four potential tautomer of the mono-protonated metformin cation (tautomers 1a, 1b, 1c and 1d) were optimized and their single point energies were calculated by Density Functional Theory (DFT) B3LYP method based on the Polarized Continuum Model (PCM) in water, which shows that the most likely existed tautomer in human cells is the same in the crystal structure. Based on the optimized structure, their Wiberg bond orders, Natural Population Analysis (NPA) atomic charges, molecular electrostatic potential (MEP) maps were calculated to analyze their electronic structures, which were then compared with the corresponding values of the diprotonated metformin cation (cation 2) and the neutral metformin (compound 3). Finally, the possible tautomeric mechanism of the mono-protonated metformin cation was discussed based on the observed phenomena.