• 제목/요약/키워드: flushing time

검색결과 139건 처리시간 0.022초

탄소섬유 정밀여과막 및 광촉매 혼성 수처리 공정에서 물 역세척 조건의 영향 (Effect of Water Back-flushing Condition in Hybrid Water Treatment Process of Carbon Fiber Microfiltration Membrane and Photocatalyst)

  • 박진용;조광희
    • 멤브레인
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    • 제22권3호
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    • pp.216-223
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    • 2012
  • 본 연구에서는 정수처리용 탄소섬유 정밀여과막 및 광촉매의 혼성공정에서 물 역세척 주기(FT) 변화의 영향을 알아보고, 알루미나 한외여과막을 사용한 기존의 결과와 비교하였다. 물 역세척 시간(BT)는 10초로 고정한 채, FT를 2~10분으로 변화시키면서, 그 영향을 180분 운전 후 막오염에 의한 저항($R_f$), 투과선속(J)과 총여과부피($V_T$) 측면에서 고찰하였다. FT가 감소할수록, $R_f$는 감소하고 J는 증가하여 알루미나 한외여과막을 사용한 기존의 결과와 동일하였다. 탁도의 처리효율은 99.2% 이상으로 높게 나타났으며, FT 변화에 의한 영향이 보이지 않아 기존의 결과와는 달랐다. 한편, 유기물의 처리효율은 NBF 조건에서 65.6%로 가장 낮았으며 FT가 감소할수록 증가하여 기존의 결과와 역시 다른 현상을 보였다. 이런 차이를 보인 것은 세라믹 분리막의 재질의 차이로 인한 막오염 현상이 다른 기작을 보이기 때문인 것으로 판단된다.

실리카 기반 컬럼의 세척, 재생 및 보관 가이드 (Column cleaning, regeneration and storage of silica-based columns)

  • Matt James;Mark Fever
    • FOCUS: LIFE SCIENCE
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    • 제1호
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    • pp.1.1-1.4
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    • 2024
  • This article provides comprehensive guidance on the maintenance, cleaning, regeneration, and storage of silica-based HPLC (High-Performance Liquid Chromatography) columns. The general considerations emphasize the importance of using in-line filters and guard cartridges to protect columns from blockage and irreversible sample adsorption. While these measures help, contamination by strongly adsorbed sample components can still occur over time, leading to an increase in back pressure, loss of efficiency, and other issues. To maximize column lifetime, especially with UHPLC (Ultra-High Performance Liquid Chromatography) columns, it is advisable to use ultra-pure solvents, freshly prepared aqueous mobile phases, and to filter all samples, standards, and mobile phases. Additionally, an in-line filter system and sample clean-up on dirty samples are recommended. However, in cases of irreversible compound adsorption or column voiding, regeneration may not be possible. The document also provides specific recommendations for column cleaning procedures, including the flushing procedures for various types of columns such as reversed phase, unbonded silica, bonded normal phase, anion exchange, cation exchange, and size exclusion columns for proteins. The flushing procedures involve using specific solvents in a series to clean and regenerate the columns. It is emphasized that the flow rate during flushing should not exceed the specified limit for the particular column, and the last solvent used should be compatible with the mobile phase. Furthermore, the article outlines the storage conditions for silica based HPLC columns, highlighting the impact of storage conditions on the column's lifetime. It is recommended to flush all buffers, salts, and ion-pairing reagents from the column before storage. The storage solvent should ideally match the one used in the initial column test chromatogram provided by the manufacturer, and column end plugs should be fitted to prevent solvent evaporation and drying out of the packing bed.

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하천에 순간적으로 유입된 오염물질의 플러싱 효과 분석 (An Analysis of Flushing Effects for Instantaneous Contaminants Input into River)

  • 정재욱;김수열;김진영;윤세의
    • 한국방재학회 논문집
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    • 제4권3호
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    • pp.43-50
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    • 2004
  • 본 연구에서는 갈수시 하천에 순간적으로 유입되는 오염물질에 대해 댐방류량 변화에 따른 플러싱 효과를 분석하였다. 한강하류부(잠실수중보${\sim}$신곡수중보)에 RMA-2 및 RMA-4 모형을 적용하였으며, 유로특성을 반영할 수 있도록 종확산계수는 $50m^2/s$을 사용하였다. 댐방류량은 1시간동안 $500m^3/s,\;1000m^3/s,\;1500m^3/s,\;2000m^3/s$로 변화시켰으며, 갈수시 유량은 $200m^3/s$로 고정하였다. 정체되어 있는 경우와 순간적으로 유입되는 경우, 성산대교 부근에서 농도가 1ppm 이하로 떨어지는 시간을 각 유량별로 분석하였다. 댐방류량이 증가할수록 희석시간이 단축되는 것을 알 수 있었고, 댐방류량과 희석시간이 선형관계가 있는 것으로 나타났다. 순간적으로 유입된 오염물질이 정체된 오염물질의 경우보다 댐방류량에 민감하게 영향을 받으며, 댐방류량에 의한 플러싱을 시도할 경우에는 본류의 오염물질이 지류로 역류하는 범위를 파악할 수 있었다.

Hydro-hypsographic 분석을 이용한 근소만 해수 교환 특성 연구 (A study on the flushing characteristics in Geunso bay using hydro-hypsographic analysis)

  • 최종국;유주형;우한준;엄진아
    • 한국습지학회지
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    • 제13권1호
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    • pp.45-52
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    • 2011
  • 만과 외해와의 해수유통은 저서환경에 영양염과 산소 공급, 오염물질 정화 등 생태계를 건강하게 만드는 중요한 요인이며, 만 내 저서환경의 건강성은 해수 교환 특성과 밀접한 관련을 갖는다. 이 연구에서는 서해안 근소만 저서환경의 해수 분포 및 유동 특성을 파악하기 위한 hydro-hypsographic 분석을 통해 수리적 교환시간을 계산함으로써 근소만의 해수유통 특성을 정량적으로 분석하였다. 위성영상 자료를 이용한 수륙경계선 추출방법과 음향측심기에 의해 획득한 조하대 수심자료를 이용하여, 연구지역의 지형고도모델을 작성하였으며, 지리정보시스템의 공간분석 기능을 이용하여 hydro-hypsographic 분석을 실시하였다. 분석결과, 근소만 전체 면적의 95%가 갯벌인 것으로 나타났으며, 수리적 교환시간은 1.03 tidal cycle로서 만의 해수 유통 특성이 우수한 것으로 나타났다. 국내외 타 지역과 비교하였을 때도, 근소만이 상대적으로 저서환경이 차지하는 면적이 넓고 조차도 국외 지역에 비해 커서 해수의 교환이 상대적으로 잘 이루어지고 있는 것으로 분석되었다. 이 연구의 결과는 국내 만들의 해수유통 특성 분석에 의해 각 만들의 건강성을 정량화 할 수 있는 체계 마련 및 만의 저서환경, 생태 등 관리를 위한 기초자료로 활용 가능할 것이다.

Permeability-increasing effects of hydraulic flushing based on flow-solid coupling

  • Zhang, Jiao;Wang, Xiaodong
    • Geomechanics and Engineering
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    • 제13권2호
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    • pp.285-300
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    • 2017
  • Shallow coal resources are increasingly depleted, the mining has entered the deep stage. Due to "High stress, high gas, strong adsorption and low permeability" of coal seam, the gas drainage has become more difficult and the probability of coal and gas outburst accident increases. Based on the flow solid coupling theory of coal seam gas, the coupling model about stress and gas seepage of coal seam was set up by solid module and Darcy module in Comsol Multiphysics. The gas extraction effects were researched after applying hydraulic technology to increase permeability. The results showed that the effective influence radius increases with the expanded borehole radius and drainage time, decreases with initial gas pressure. The relationship between the effective influence radius and various factors presents in the form: $y=a+{\frac{b}{\left(1+{(\frac{x}{x_0})^p}\right)}}$. The effective influence radius with multiple boreholes is obviously larger than that of the single hole. According to the actual coal seam and gas geological conditions, appropriate layout way was selected to achieve the best effect. The field application results are consistent with the simulation results. It is found that the horizontal stress plays a very important role in coal seam drainage effect. The stress distribution change around the drilling hole will lead to the changes in porosity of coal seam, further resulting in permeability evolution and finally gas pressure distribution varies.

클라우드 컴퓨팅에서 사용자 작업환경의 끊김 없는 연계를 위한 웹 서비스 연결 관리 기법 (Web Service Connection Management Scheme for Seamless Migration of User Workspace in Cloud Computing)

  • 최민
    • 한국IT서비스학회지
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    • 제8권1호
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    • pp.193-202
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    • 2009
  • Cloud computing emerges as a new computing paradigm which targets reliable and customizable services. The term builds on decades of research in virtual machine, distributed and parallel computing, utility computing, and more recently networking, web service, and software as a service. In this paper, we provide a seamless connection migration of web services. This is useful for cloud computing environment in which many client terminals have mobility. With the wireless internet facility, those mobile users can move place to place during internet communication. Therefore, we provide solutions to the two major problems in current virtualization based migration: communication failure problems and connection re-establishment. Communication channel flushing by zero window notification helps to resolve the communication failure problems and TCP port inheritance prevents connection re-establishment errors during socket reconstruction. Thus, our web service migration facility is now able to preserve open network connections, and even for server sockets. This is a highly transparent approach, in that we did not Introduce additional messages for channel flushing and did not make any modification to the TCP protocol stack. Experimental results show that the overhead due to connection migration of web services is almost negligible when compared with time to take the conventional web service migration.

Si 입자를 함유한 반도체 세정폐수의 한외여과 특성[I] -Polysulfone 평판막에 의한 투과분리- (Permeation Behavior of Semiconductor Rinsing Wastewater Containing Si Particles in Ultrafiltration System -I. Permeation Characteristics of Polysulfone Flat Plate Membrane-)

  • 곽순철;이석기;전재홍;남석태;최호상
    • 멤브레인
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    • 제8권2호
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    • pp.102-108
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    • 1998
  • 본 연구는 Si 미립자를 함유한 반도체 세정폐수의 평판막을 이용한 한외여과특성을 검토하였다. 평판막의 투과유속은 시간이 경과함에 따라 점차 감소하는 경향을 나타냈으며, 이현상은 막표면에 형성된 케익층의 증가 및 기공막힘에 기인한다. 흐름형태에 따른 투과유속은 cross flow가 dead-end flow의 약 1.4배 높았다. Si 미립자에 의한 막오염을 제거하는데는 역세법이 sweeping법 보다 우수하였다. 막오염으로 인한 투과유속의 감소는 질소가스로 역세척하여 초기투과유속의 약 85% 정도 회복되었다. 평판막을 이용한 cross flow 공정의 용질배제율은 약 90%였으며, 투과수증의 Si 미립자의 크기는 평균 70 nm였다.

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김치용기에서의 이산화탄소 농도 제어를 위한 주입 프로그램 조건 설정 (Programmed Conditions of Supplying Carbon Dioxide to Keep its Desired Concentration in Kimchi Container)

  • 안덕순;조민경;박수연;이동선
    • 한국포장학회지
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    • 제25권2호
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    • pp.31-35
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    • 2019
  • Kimchi is a refreshing sour food which gives sour and carbonic acid taste of carbon dioxide produced during the fermentation process. So, carbon dioxide injection was tried to raise carbonic acid taste of kimchi stored in the airtight container. First, carbon dioxide injection times of a given gas supply system were determined experimentally to attain initial concentration of 80% for different solid/liquid ratios. Since carbon dioxide is dissolved in kimchi to decrease its concentration during storage, periodical carbon dioxide injection conditions were needed and determined to keep the $CO_2$ concentration above 70%. For the initial flushing to 80% $CO_2$ concentration in model system filled with water, the injection time ranged from 40 to 89 seconds for free volumes of 2-8 L. $CO_2$ injection conditions for the under-ripened storage at $10^{\circ}C$ consisted of longer time at more frequent cycles for watery kimchi than for Chinese cabbage kimchi. At $0^{\circ}C$ of subsequent ripened stage storage of watery kimchi, the periodical injection at 3 hour interval was required because of continuous dissolution of carbon dioxide. However, Chinese cabbage kimchi did not require subsequent $CO_2$ injection during the ripened state storage and needed only flushing to 80% $CO_2$ at time of the container opening and closing. These results can be used as basic information for the programmed control of $CO_2$ injection in the kimchi container system.

득량만의 해수 교환 및 물질 순환에 관한 연구 1 . 해수의 수송량 및 교환 시간 (Study on the Water and Material Exchange in Deukryang Bay 1. Volume Transport and Turnover Time of Sea Water)

  • 조규대;이충일
    • 한국환경과학회지
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    • 제7권3호
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    • pp.311-320
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    • 1998
  • The volume transport and turnover time of the Deukryang Bay. located at the southern area of Korea, were calculated based on the current meter(RCM-7,ACM 16M) data observed at the three gateways of the tegrating observed data and then averaging on time. dangdo and Kogumdo. The total water volume transports through three entrances of the bay in May and October were $3.9{\times}10-2Sv, 3.4{\times}10^{-2}Sv(1Sv=10^6m^3s^{-1}$) and turnover time were 0.97day, 1.12day, respectively. Semidiurnal tides were predominant (70~85%). The water volume transports by residual currents were 2~4% of total water volume transports . The average fraction of fresh water calculated by tidal prism method using salinity difference between inflow current and outflow current through three entrances In Deukryang Bay was about 0.06% of total volume and the flushing time of fresh water was estimated as 0.97day.

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Direct Embryo Collection(DEC)에 의한 한우의 수정란 채란 (Embryo Recovery by Direct Embryo Collection (DEC) in Korean Native Cattle (Hanwoo))

  • 유한준;이용승;박정준;김기원;박춘근
    • 한국수정란이식학회지
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    • 제26권3호
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    • pp.153-158
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    • 2011
  • This study was performed in order to simplify the operation and minimize stress of donor and be readily available in the field with low cost and high quality embryos using the Direct Embryo Collection (DEC). Donors, at random stages of the estrous cycle, received a CIDR. 7 days later, 200 mg FSH was treated with 40, 30, 20, 10 mg FSH levels in declining doses twice daily by intramuscular injection for 4 days. On the 3rd day administration of FSH, 25 mg $PGF_2{\alpha}$ was administered and CIDR was withdrawn. After FSH injections were complete, donors were artificially inseminated twice at 12 hr intervals. The donor cattle received 250 ${\mu}g$ GnRH at time of 1 st insemination and embryos were recovered 8 days after the 1st insemination. Embryo collection from superovulated donors was performed to flushing by non-surgical methods of 3-way, 2-way and DEC (l-way). The average number of recovered embryos were 11.25${\pm}$0.63, 12.5${\pm}$0.65 and 11.75${\pm}$0.48 from operations of 3-way, 2-way and DEC methods, respectively. There were no significant differences among the embryo collection methods. Also, The average number of transferable embryos were 6.25${\pm}$0.48, 7.25${\pm}$0.48 and 7.25${\pm}$0.63 from each embryo collection procedures. The number of transferable embryos was no differences among the 3-way, 2-way and DEC methods, respectively. Meanwhile, the ratio of transferable embryos for all recovered embryos from DEC methods was higher as 61.7 % than 55.6 %, 58 % from methods of 3-way, 2-way. And the flushing solution required for recovering embryos by DEC method was significantly lower as 0.28${\pm}$0.32 1 than 1.8${\pm}$0.12 1, 1.75${\pm}$0.10 1 from 3-way, 2-way methods (p<0.05). Also, the time required for recovering embryos by DEC methods was significantly lower as 27${\pm}$2 min than 51${\pm}$3, 45${\pm}$2 min, respectively (p<0.05). In conclusion, these results suggest that DEC method for embryo collection may be effectively used for production of in vivo embryos using less flushing solution and, it might be effectively available in the field compared to conventional embryo recovery methods using 3-way or 2-way balloon catheter.