• Analytical Science and Technology
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• v.20 no.6
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• pp.508-515
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• 2007

Age determination was carried out with the bricks relating to Muryong Royal Tomb of the Baekje Kingdom, for which there is no information on the external gamma dose rate, by using the subtraction method of luminescence dating. In the subtraction method, each paleodose for fine grain and for quartz inclusion is required for the sample to be dated. In this study, the paleodose for the fine grain was estimated by thermoluminescence measurement and the paleodose for the quartz inclusion was determined using optically stimulated luminescence. The resultant ages among the bricks showed good agreement with standard deviation of 6 % error. Finally the bricks relating to Muryong Royal Tomb were evaluated as AD $530{\pm}50yrs$($1{\sigma}$ SD).

• Journal of the Korean Society for Heat Treatment
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• v.16 no.2
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• pp.83-89
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• 2003

As a research for developing fine-grained high strength low carbon steels, the effects of austenitization temperature and hot deformation on microstructure was investigated in 0.15 wt.% carbon steels with microalloying elements such as Nb and Ti. When the steels were reheated at $1250^{\circ}C$, Nb containing steel showed very coarse austenite grain size of $200{\mu}m$ whereas Nb-Ti steel did fine one of $70{\mu}m$ because Ti carbonitrides could suppress the austenite grain growth. In case of 50% reduction at $850^{\circ}C$, the austenite grains in the Nb steel partially recrystallized while those in the Nb-Ti steel fully recrystallized probably due to finer prior austenite grains.For the Nb-Ti steel, ferrite grain size was not sensitively changed with austenitization temperature and compression strain and, severe deformation of 80% reduction was not essentially necessary to refine ferrite grains to about $3{\mu}m$ which could be obtained through lighter deformation of 40% reduction.

• International Journal of Korean Welding Society
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• v.2 no.1
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• pp.25-28
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• 2002

In the coarse grain HAZ adjacent to the fusion line, most of the TiN particles in conventional Ti added steel are dissolved and austenite grain growth is easily occurred during welding process. To avoid this difficulty, thermal stability of TiN particle is improved by increasing the nitrogen content in steel. In this study, the effect of hlgh nitrogen TiN particle on preventing austenite grain growth in HAZ was investigated. Increased thermal stability of TiN particle is helpful for preventing the austenite grain growth by pinning effect. High nitrogen TiN particle in simulated HAZ were not dissolved even at high temperature such as 1400'E and prevented the austenite grain growth in simulated HAZ. Owing to small austenite grain size in HAZ the width of coarse grain HAZ in high nitrogen TiN steel was decreased to 1/10 of conventional TiN steel. Even high heat input welding, the microstructure of coarse grain HAZ consisted of fine polygonal ferrite and pearlite and toughness of coarse grain HAZ was significantly improved.

• KIEAE Journal
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• v.7 no.5
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• pp.135-142
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• 2007

This is an experimental study on the structural characteristics of reinforced concrete beams using of the oyster shells as a substitute fine aggregate of concrete. In this study, the main factors consist of the grain sizes and the percentage of substitution of oyster shells to fine aggregate in the equal water cement ratio. The results of the study showed as followed. The initial load value of them represented similar constant within 10% of the maximum load value in each test beam. But the maximum load value and the ultimate load value decreased with increased grain size and the rate of substitution. As the grain size of oyster shells became smaller, the load values of them were somewhat higher. The deflection among deformation properties of reinforced concrete beams with oyster shells represented typical curves like that of normal reinforced concrete. In the deformation of steel and concrete, the deformation was proportionated to the load till yield point and from yield point until approaching the ultimate load point. One type was typical curve of the load and the deformation and the other type irregularly was changed to very small deformation for the load increase centering around load axis. After the analyzing structural behaviors and the properties of reinforced concrete test beams with oyster shells, the most excellent grain size of oyster shells represented 1.0mm and less or 5.0mm and less with taking uniformly, and the percentage of practicable substitution of them to fine aggregate was about 30%.

• Journal of Welding and Joining
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• v.18 no.2
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• pp.49-56
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• 2000

Recently developed Austenite stainless steel, 309L was used to overlay on 3Cr-1Mo-V-Ti-B steels, using Electroslag welding process, which wide electrodes were adopted. Transition region in welding interlayer relating to disbonding crack was investigated. Also, the effect of welding condition on the width of transition region and coarsening grains of the austenite were studied. 1) With increasing welding speed the width of martensite at transient region was increased, but the amount of delta ferrite in weld metal was reduced, being fine grained. 2) The form of martensite at the transition region was occurred by reversible transformation during cooling since the interdiffusion of Cr and Ni from weld metal and Fe and C from base metals at the transition region, causes to lowering the concentration of Cr and Ni at the transition region, leading to increasing Ms point. 3) With increasing welding speed, the grain of austenite formed at the welding interface was finer. With increasing welding current under the same welding speed, the grain size of the austenite was finer. At high current, original grain size of the austenite is coarse, but the austenite has fine grains because the austenite was transformed to martensite during cooling. 4) In the case of high welding speed, the width of martensite at the welding interface was increased, but the grain size of austenite at the welding interface was finer. This indicates that the inhibition of disbonding crack may be achieved through dispersening fine carbides in the gain boundary.

• Journal of Powder Materials
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• v.3 no.4
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• pp.271-278
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• 1996

In this study, the effect of the transition elements on the microstructure and mechanical properties of rapidly solidified Al-Mg-X alloys was investigated. As a result of the rapid solidification processing, fine equiaxed grains with a mean diameter of 2 $\mu$m were observed in these alloys. Many fine particles were found to be distributed rather homogeneously throughout the matrix with relatively large particles occasionally at grain boundaries. The ultimate tensile strengths of Al-Mg-X alloys were found to decrease rather remarkably at 150 $^{\circ}C$ without the gain of the ductility at 150 $^{\circ}C$, which may result from segregation of $\beta$ ($Al_{3}Mg_{2}$) precipitates. Fine dimples were observed on the fracture surfaces for all alloy systems and the variation of the size and shape of dimples was not observed upon alloy systems. The ductility at 530 $^{\circ}C$ was found to be ~100%, suggesting that grain boundary sliding did not contribute to ductiliy despite he grain size stabilization. The absence of superplastic behavior may be associated with low boundary misorientation in rapidly solidified Al-Mg-X alloys.

• Journal of the Korean Ceramic Society
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• v.20 no.4
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• pp.324-332
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• 1983

In this studies resistivity thermal expansion and microstructure of the Forsterite Porcelain as a high frequency insulator were investigated. The body containing Zn-glass shows higher resistivity than any other body. The bodies containing K, Ba, Cd-glass respectively consist of fine crystals of mosaic type. The bodies containing Bi, Zn, Zr-glass repectively included more large crystals because of the grain growth and coherence of fine particles In the 4 series Forsterite containing excess MgO 0-6% the thermal coefficients of the bodies increased with the increasing of excess MgO and the bodies have conspicuously high thermal expansion coefficients when 15% excess $BaCO_3$ was added to. The resistivities of additive bodies of $BaCO_3$ 0, 5, 10% in Forsterite containg excess MgO 2% are higher than any other that of composition. Bacause the growing of Forsterite crystals was restrained with the increasing of excess MgO $BaCO_3$ their grain size became fine and their grain boundaries were decomposed and also the glass phase having high refractive inder was increased. The higher the firing temperature increased the more the process of crystal growing was progressed.

• Geomechanics and Engineering
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• v.13 no.6
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• pp.947-961
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• 2017

An innovative spiral variable-section capillary model is established for piping critical hydraulic gradient of cohesion-less soils causing water/mud inrush in tunnels. The relationship between the actual winding seepage channel and grain-size distribution, porosity, and permeability is established in the model. Soils are classified into coarse particles and fine particles according to the grain-size distribution. The piping critical hydraulic gradient is obtained by analyzing starting modes of fine particles and solving corresponding moment equilibrium equations. Gravities, drag forces, uplift forces and frictions are analyzed in moment equilibrium equations. The influence of drag force and uplift force on incipient motion is generally expounded based on the mechanical analysis. Two cases are studied with the innovative capillary model. The critical hydraulic gradient of each kind of sandy gravels with a bimodal grain-size-distribution is obtained in case one, and results have a good agreement with previous experimental observations. The relationships between the content of fine particles and the critical hydraulic gradient of seepage failure are analyzed in case two, and the changing tendency of the critical hydraulic gradient is accordant with results of experiments.

• Korean Journal of Metals and Materials
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• v.48 no.10
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• pp.936-941
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• 2010

Al-Zn based alloys are the most common types of wrought Al alloys. Although Al-Zn alloys have high strength, they cannot be applied to a conventional casting process. In this study, Al-Zn-based alloys applicable to a die casting process were developed successfully. The developed Al-45 wt% Zn-based alloys showed a fine equiaxed grain structure and high strength. A fine equiaxed grain having an average size of $25{\mu}m$ was obtained by the die casting process. The UTS and elongation of the new alloy are 475 MPa and ~3.5%, respectively. In addition, we elucidate the effect of a Zn addition on variations in different mechanical properties and the microstructure characteristics of (Al96.3-xZnxCu3Si0.4Fe0.3) x=20, 30, 40, and 45 wt% alloys fabricated by a die casting process.

• Nuclear Engineering and Technology
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• v.54 no.7
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• pp.2359-2366
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• 2022

Selecting graphite grades with superior irradiation characteristics is important task for designers of graphite moderation reactors. To provide reference information and data for graphite selection, the effects of irradiation on three fine-grained, iso-molded nuclear grade graphites, ETU-10, IG-110, and NBG-25, were compared based on irradiation-induced changes in volume, thermal conductivity, dynamic Young's modulus, and coefficient of thermal expansion. Data employed in this study were obtained from reported irradiation test results in the high flux isotope reactor (HFIR)(ORNL) (ETU-10, IG-110) and high flux reactor (HFR)(NRL) (IG-110, NBG-25). Comparisons were made based on the irradiation dose and irradiation temperature. Overall, the three grades showed similar irradiation-induced property change behaviors, which followed the historic data. More or less grade-sensitive behaviors were observed for the changes in volume and thermal conductivity, and, in contrast, grade-insensitive behaviors were observed for dynamic Young's modulus and coefficient of thermal expansion changes. The ETU-10 of the smallest grain size appeared to show a relatively smaller VC to IG-110 and NBG-25. Drastic decrease in the difference in thermal conductivity was observed for ETU-10 and IG-110 after irradiation. The similar irradiation-induced properties changing behaviors observed in this study especially in the DYM and CTE may be attributed to the assumed similar microstructures that evolved from the similar size coke particles and the same forming method.