• 동의생리병리학회지
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• 제18권1호
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• pp.179-186
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• 2004

In order to search for the ways of use in distilled liquid of Shogunjung-tang, an oriental medical prescription, the study examined the differences in the activated degree of cells and immunological effects, which are supplied by restoratives such as the existing extracted liquid and distilled liquid of Shogunjung-tang. As seen from the above results, both the extracted liquid of Shogunjung-tang and distilled liquid have remarkable efficiency in the increase of cells, the efficient condition of immunity activation degree possibly formed by these two and activation of cells and organism, in which distilled liquid in the beginning and the extracted liquid later tend to show its efficiency.

• 동의생리병리학회지
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• 제18권1호
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• pp.148-156
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• 2004

In order to searched for the ways of use for distilled liquid of Cervus Elaphus Xanthopgus, the study examined the difference of immunological efficiency generally raised in the existing extracted liquid and distilled liquid of Cervus Elaphus Xanthopgus. As seen from the above results, both the extracted liquid of Cervus Elaphus Xanthopgus and distilled liquid have remarkable efficiency in the increase of cells, the efficient condition of immunity activation degree, the effect of anti-cancer possibly formed by these two and activation of cells and organism, in which distilled liquid in the beginning and the extracted liquid later tend to show its efficiency.

• The International Journal of Costume Culture
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• 제8권2호
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• pp.124-131
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• 2005

This study focused on the change of skin temperature by the emissivity and emission power of far-infrared for conformant far infrared effect to naked eyes. The study method is to manufacture the bra pad by each concentration on far-infrared materials of illite powder $(K,H_3O)AI_2(Si,Al)_4O_{10}(H_2O,OH)_2)$, liquid alumina ($Al_2O_3$), the extracted liquid from 29 kind of medical plants, then, measured change of skin temperature. Result are as follows. Far-infrared were emitted each $90.2\%,\;90.1\%,\;89.7\%$ from the illite powder, liquid alumina, extracted liquid from medical plants. When the testee weared the bra pad, the temperature of coated bra pad was $0.5^{\circ}C$ higher than the non finished bra pad. Washing fastness on far-infrared finishing was better dope addition method than coating method.

• Bulletin of the Korean Chemical Society
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• 제32권11호
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• pp.3923-3927
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• 2011

A noble method for pre-concentration and speciation of ultra trace As (III) and As (V) in urine and whole blood samples based on dispersive liquid-liquid microextraction (DLLME) has been developed. In this method, As (III) was complexed with ammonium pyrrolidine dithiocarbamate at pH = 4 and Then, As (III) was extracted into the ionic liquid (IL). Finally, As (III) was back-extracted from the IL with hydrochloric acid (HCl) and its concentration was determined by flow injection coupled with hydride generation atomic absorption spectrometry (FI-HGAAS). Total amount of arsenic was determined by reducing As (V) to As (III) with potassium iodide (KI) and ascorbic acid in HCl solution and then, As (V) was calculated by the subtracting the total arsenic and As (III) content. Under the optimum conditions, for 5-15 mL of blood and urine samples, the detection limit ($3{\sigma}$) and linear range were achieved 5 ng $L^{-1}$ and 0.02-10 ${\mu}g\;L^{-1}$, respectively. The method was applied successfully to the speciation and determination of As (III) and As (V) in biological samples of multiple sclerosis patients with suitable precision results (RSD < 5%). Validation of the methodology was performed by the standard reference material (CRM).

• 한국의류학회지
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• 제35권12호
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• pp.1507-1517
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• 2011

Berberine, palmatine, and Phellodendron bark dye was prepared in methanol for HPLC-DAD-MS analysis of liquid dye. Silk was dyed using berberine, palmatine, and Phellodendron bark dye prepared in water. The dye was extracted from the dyed silk using the HCl/methanol/water (2:1:1 v/v/v) solvent system with a slight modification. The liquid dyes and the dye extracted from the silk samples dyed with the three dye sources were examined using the HPLC-DAD-MS analysis to simultaneously detect berberine and palmatine from the plant dye and the dyeings. Colorimetric measurement was carried out using a spectrophotometer to examine the color and the intensities of berberine, palmatine, and Phellodendron bark dyed silk samples. From the liquid dyes, berberine eluted at 5.21 min with the molecular cation m/z=336 and the UV spectrum confirming that the product was berberine. Palmatine eluted at 5.12 min with the molecular cation m/z=352 and the UV spectrum confirming that the product was palmatine. From the silk dyed with berberine and palmatine dye, berberine and palmatine species eluted at 5.35 min and 5.24 min, respectively. From the silk dyed with Phellodendron bark, berberine and palmatine were detected simultaneously at 5.35 min and 5.26 min, respectively. All three dyes had yellow hue while palmatine dyed silk showed the highest hue and chroma. Palmatine dyed silk showed the highest K/S value that indicated the strongest color intensity and the highest dye uptake.

• 대한설비공학회지:설비저널
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• 제13권4호
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• pp.223-229
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• 1984

Experiments were performed for freezing of an initially superheated or nonsuperheated liquid phase in a cooled vertical tube. The liquid was placed in a copper tube whose surface maintained a uniform temperature during the data run and the freezing occurred in a copper tube. The phase change medium was n-odtadecane, a paraffin which freezes at about $61^{\circ}C$. Measurements were made which yielded information about the time dependence of the freezing front, of the amount of frozen mass, and of the various energy components extracted from the tube. The time-wise decay of the initial liquid superheat was also measured. Initial superheat of the liquid tends to moderately diminish the rozen mass and associated latent energy extraction at small times but has lit tie effect on these quantities at large tiems. Natural convection in the liquid Plays a modest role only at small times and disappears when the superheat decay to zero. Although the latent energy constitutes the largest contributor to the total extracted energy, the sensible energy components can make a significant contribution, especially at large tube wall subcoolings, large initial liquid superheating and short freezing time.

• Journal of the Korean Wood Science and Technology
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• 제24권2호
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• pp.81-93
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• 1996

To elucidate the structure of procyanidin in Korean red pine (Pinus densiflora S. et Z.), bark, the extractives were extracted with acetone-water mixture(7:3, v/v) from inner bark of Korean red pine. The extracts separated three fractions which were extracted by liquid-liquid extraction. The extracting solvents were chloroform and ethyl acetate and water. The part of ethylacetate soluble was chromatographed by liquid chromatography. The ethylacetate soluble portion yielded four natural procyanidin dimers, two known epicatechin-($4{\beta}{\rightarrow}6$)-catechin, catechin-($4{\alpha}{\rightarrow}8$)-catechin and two unknown catechin-($4{\beta}{\rightarrow}6$)-catechin and conformational isomer of epicatechin-($4{\alpha}{\rightarrow}6$)-catechin. The additional catechins was also isolated. The structures of these procyanidins were elucidated by their $^{13}C$-NMR spectra.

• Applied Biological Chemistry
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• 제41권8호
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• pp.595-599
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• 1998

An analytical method was developed to determine tricyclazole residues in rice grain, straw, and soil using high-performance liquid chromatography (HPLC) with ultraviolet absorption detection. Tricyclazole was extracted with methanol from moist rice grain, straw, and soil samples. n-Hexane washing was employed to remove nonpolar co-extractives during liquid-liquid partition. Tricyclazole was then extracted with dichloromethane from alkaline aqueous phase, while acidic interferences remained in the phase. Dichloromethane extract was further purified by silica gel column chromatography prior to HPLC determination. Reverse-phase HPLC using an octadecylsilyl column was successfully applied to separate and quantitate the tricyclazole residue in sample extracts monitored at ${\lambda}_{max}$ 225nm. Recoveries from fortified samples averaged $95.5{\pm}3.0%\;(n=6),\;87.5{\pm}20.%\;(n=6),\;and\;84.3{\pm}2.8%$ (n=12) for rice grain, straw, and soil, respectively. Detection limit of the method was 0.02 mg/kg for rice grain and soil samples while 0.05 mg/kg for rice straw samples. The proposed method was reproducible and sensitive enough to evaluate the safety of tricyclazole residues in rice grain, straw, and soil.

• 한국관광식음료학회지:관광식음료경영연구
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• 제13권2호
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• pp.119-127
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• 2002

본 연구는 Liquid egg yolk sabayon을 만들 때 버터 대신에 올리브오일과 마늘 첨가량을 달리하여 관능적 평가를 실시하여 조리표준화의 예시를 제시하고자 한다. 1, 맛에서는 마늘 10g 첨가에서 5.61로 대조군의 5.13보다 좋았다. 2. 색에서는 마늘 20g 첨가가 가장 높은 점수를 얻었고, 마늘 30g가 나쁘게 나타났다. 3. 향에서는 마늘 10g 첨가가 대조군 보다 좋았고 마늘 첨가군 모두가 대조군 보다 좋았다. 4. 종합적인 면에서도 마늘 10g첨가가 우수한 것으로 나타났다. 따라서 Liquid egg yolk sabayon을 만들 때 적당량의 마늘을 첨가하는 것이 좋을 것으로 사료되어 진다.

• 한국세라믹학회지
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• 제50권2호
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• pp.103-107
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• 2013

In this study, the ionic liquid 1-ethyl-3-methylimidazolium tetraflouroborate (EMI-BF4) was synthesized and purified using the liquid/liquid fractional distillation method to apply a supercapacitor. EMI-BF4 was extracted with dichloromethane from the liquid/liquid extraction method in acidic, neutral, and alkali conditions for removal of impurity, and then the electrical capacities of the purified ionic liquids were measured and compared. The electrical capacities of ionic liquids under acidic condition showed higher value than those of neutral or alkali conditions. As the ratio of ionic liquid to solvent became higher, the electrical capacity value was increased.