• 제목/요약/키워드: exposed specimen

검색결과 293건 처리시간 0.022초

분말 형태의 황산바륨을 현탁액으로 조제하는 과정에서 발생하는 미생물의 오염도 측정 (Measurement of Microbic Contamination Rate in the Dispensing Process Making Suspension of Barium Sulfate Powder)

  • 김영근;이양섭;조정찬;류명선;이경섭
    • 대한방사선기술학회지:방사선기술과학
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    • 제24권2호
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    • pp.53-57
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    • 2001
  • The purpose of this study is to investigate the contamination rate of barium sulfate suspension made in the exposed state in usual circumstances. This study was performed in four university hospital using the contrast media by barium sulfate powder. The specimen were detected at dispensing water, agitator and mixing tank. We also classified the suspension into general bacteria, mycete, and Bacillus coli infection. The tap water were used to dispense water in the all hospitals. Bacillus colt were not detected in the all. General bacteria and mycete were not detected in the one specimen, but detected in two specimen over defined value. In the contamination rate of agitator, mixing tank, and the manufactured, Bacillus coli were not detected in all. However, general bacteria and mycete were detected too numberous to count. In conclusion, the refined water must be used in dispensing water in manufacturing suspension. The disinfectant is also used in washing the agitator and mixing tank for sterilization. Hand washing is indispensible to manufacturing suspension for preventing from infection.

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코팅에 의한 고온재료의 내산화성 향상을 위한 연구 (A strudyon the improvement of the oxidation resistance for high temperature materials by coating process)

  • 강석철;민경안;안연상;김길무
    • 한국표면공학회지
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    • 제30권2호
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    • pp.93-103
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    • 1997
  • High temperature materials used in the elevated temperature and corrosive atmosphere must have the good oxidation resistance and preserve their own mechanical properties simultaneously. For the oxidation resistance, it is very important to form a protective oxide scale such as $Al_2O_3$ or $Cr_2O_3$ on the substrate. However, the additions of protective oxide forming elements such as Cr and Al in the alloy to enhance its oxidation resistance are limited due to the deleterious effects on their mechanical properties. PECVD(P1asma Enhanced Chemical Vapor Deposition) coating processes were employed to improve the oxidation resistance at high temperature. Cr and/or A1 were coated on the substrates of Ni and Inconel 600 at various temperatures of 400, 500, $600^{\circ}C$ and at different conditions of specimen surfaces. Then, coated specimens were exposed to isothermal and cyclic oxidation conditions in air at 1000 and $1100^{\circ}C$. In order to enhance the adhesion between the substrate and coated layer, heat treatments of the coated specimens were conducted in a vacuum. At isothermal oxidation experiments, Al-coated Ni specimen showed better oxidation resistance than pure Ni. At cyclic oxidation experiments at $1000^{\circ}C$. Cr and Al-coated specimen showed better oxidation resistance. Cr-coated Inconel 600 had also showed better oxidation resistance due to Cr in the substrate. By PECVD coating process, oxidation resistance could be improved, but it was not improved as expected due to the weakness of the adhesion between the substrate and the coated layer.

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Mitigation of steel corrosion in concrete by electrochemical chloride extraction at the AI-supporting electric source

  • Jiseok Kim;Ki Yong Ann;Woongik Hwang
    • Computers and Concrete
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    • 제33권6호
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    • pp.631-642
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    • 2024
  • The present study concerns the corrosion mitigation of electrochemical chloride extraction (ECE) in concrete structure. Concrete specimen was fabricated with 5.0% chloride in cast, while the other specimen was exposed to 4.0M NaCl solution for 1 year to accelerate corrosion of steel. Then, the ECE was applied to the concrete specimen with 1000 mA/m2 of the current density for 2, 4 and 8 weeks, respectively. During the ECE, the corrosion current density and corrosion potential were regularly monitored. As a result, the ECE was very effective in mitigating the degree of corrosion on the steel surface. The corrosion current density was significantly reduced from thousands to decades mA/m2, while the corrosion potential was mostly shifted to positive direction. Assuming that the corrosion starts at 1.0 mA/m2 of the corrosion current density or/and -275 mV vs SCE of the corrosion potential, the ECE could not fully achieve the repassivation of the steel, although its degree was lowered more or less depending on the duration of the treatment and type of chloride contamination. A visual examination confirmed that an increase in the duration of the treatment could lower the rust formation, but never fully removed all rust stains.

화학처리방법을 이용한 공기중에 노출된 Mg2Ni의 표면상태에 관한 연구 (The Study on the Surface State of Mg2Ni Exposed to Air by a Chemical Treatment)

  • 한정섭
    • 한국수소및신에너지학회논문집
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    • 제6권2호
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    • pp.91-100
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    • 1995
  • To investigate the surface state of $Mg_2Ni$ which was exposed to the air, a chemical treatment was undertaken with $H_2SO_4$ solution. During chemical treatment, the change of pH was measured continuously and the chemically treated specimen was hydrided to study the effect of chemical treatment on the hydrogenation. The pH changing behavior with the various $H_2SO_4$ concentration appeared very diffemrently. Especially in the solution including 3CC $H_2SO_4$, the behavior of pH change can be divided 3 steps. It is also shown that the $Mg_2Ni$ chemically treated with $H_2SO_4$ can be hydrided even under room temperature. By the SEM observation the was reasion that after chemical treatment the surface of a particle was covered with Ni layer.

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해양환경 폭로에 의한 슬래그 콘크리트의 내구성 평가 (Evaluation of Durability of Slag Concrete by Marine Environment Exposure)

  • 김현진;김규용;최경철;김홍섭;이보경;김래환
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2015년도 추계 학술논문 발표대회
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    • pp.111-112
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    • 2015
  • There is high possibility of steel corrosion on the reinforced concrete exposed to marine environment by chloride ion penetration. And it show a big difference of concrete durability under conditions of splash zone, tidal zone, and immersion zone. Therefore, in this paper, half-cell potential and chloride ion penetration depth was measured to evaluate the durability of slag concrete by marine exposure experiment. As a result, SC70 specimen showed no steel corrosion, regardless of the marine exposed conditions. Also, a deterrent effect on chloride ion penetration by replacement of slag in tidal zone and immersion zone could be confirmed.

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콘크리트 구조물의 철근 방식성능 실험평가 (An Evaluation of Corrosion Protective Systems for Reinforcing Steel in Concrete)

  • 허준;홍기섭;오승모;장지원;최응규;최완철
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1997년도 가을 학술발표회 논문집
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    • pp.275-280
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    • 1997
  • An experimental study to evaluate corrosion protection systems was undertaken with 47 reinforced concrete slab specimens subjected to cyclic wet and dry saltwater exposure. Corrosion measurements included monitoring marcrocell corrosion currents, which are generally accepted in United States practice. Test results indicate that specimens containing 2 kg/$\textrm{m}^3$ of NaCl an exposed to a 10 percent of NaCl show high values of corrosion currents. For the specimens with water repellent membrane currents kept relatively low numerical values, while test specimens with surface corrosion inhibitor hyprotective systems show high values of corrosion currents. No clear indication of the corrosion inhibitor protective systems might be due to the extremely high chloride exposure of the specimens, which has brought the accelerated corrosion. It would be expected that evaluation of the corrosion protective systems need long-term measurement with specimen exposed les chloride but simulating the real condition.

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반전지-전위 측정방법을 활용한 슬래그 콘크리트의 철근 부식 저항성능 평가 (Evaluation of Steel Corrosion of Slag Concrete by Half-cell Potential Method)

  • 이보경;김규용;김래환;윤민호;이영욱;최경철
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2014년도 추계 학술논문 발표대회
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    • pp.3-4
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    • 2014
  • There is high probability of steel corrosion on the reinforced concrete exposed to marine environment by penetration of chloride ion. When making concrete structure with slag as admixture in marine environment, salt damage can be prevented. Therefore, this paper presents experimental results of steel corrosion resistance of slag concrete considering marine environment through half-cell potential method which is one of the nondestructive test. As a result of half-cell potential experiment, it was assumed that every specimen exposed to marine environment was not corroded, and as a result of destroying specimens, it was confirmed that there was no corrosion in specimens.

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플렉서블 CIGS 태양전지의 고온고습 환경 고장 기구 분석 (Evaluation of Failure Mechanism of Flexible CIGS Solar Cell Exposed to High Temperature and Humid Atmosphere)

  • 김혁수;변재원
    • 한국신뢰성학회지:신뢰성응용연구
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    • 제16권1호
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    • pp.41-47
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    • 2016
  • Purpose: The purpose of this study was to evaluate electrical and structural degradation of flexible CIGS sollar cell exposed to high temperature and humid atmosphere. Method: Accelerated degradation was performed for various time under $85^{\circ}C/85%RH$ and then electrical and structural properties were analyzed by 4-point probe method, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD). Results: Sheet resistance of the top ITO layer increased with exposure time to the high temperature and humid atmosphere. Blunting of the protrusion morphology of ITO layer was observed for the degraded specimen, while no phase change was detected by XRD. Oxygen was detected at the edge area after 300 hours of exposure. Conclusion: Increase in electrical resistance of the degraded CIGS solar cell under high temperature and humid environment was attribute to the oxygen or water absorption.

고온 노출 콘크리트의 깊이별 수열온도 검토 (Review of Hydrothermal Temperature by Depth of High-temperature Exposed Concrete)

  • 권현우;김영민;이건철;허영선
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2021년도 가을 학술논문 발표대회
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    • pp.127-128
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    • 2021
  • In this study, a study was conducted to analyze thermal diffusion according to the depth of concrete exposed to high temperatures. For thermal diffusion analysis, a test specimen in which K-type sheath thermocouples were poured in 0, 10, 20, 30, and 40 mm sections was manufactured, and thermal diffusion measurement was performed through one-sided heating for 180 minutes under heating conditions. As a result of the review, it was shown that as the temperature condition increased, the heat diffusion increased as the depth increased.

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Effect of nonlocal-nonsingular Fractional Moore-Gibson-Thompson theory in semiconductor cylinder

  • Iqbal Kaur;Kulvinder Singh
    • Advances in nano research
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    • 제15권4호
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    • pp.305-313
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    • 2023
  • This study is aimed to investigate the electrically conductive properties of epoxy nanocomposites exposed to an acidic environment under various mechanical loads. For simultaneous assessment of the acidic environment and mechanical load on the electrical conductivity of the samples, the samples with and without carbon nanotubes were exposed to the acidic environment under three different loading conditions for 20 days. Then, the aged samples' strength and flexural stiffness degradation under crude oil and bending stress were measured using a three-point flexural test. The aged samples in the acidic environment and under 80 percent of their intact ultimate strength revealed a 9% and 26% reduction of their electrical conductivity for samples with and without CNTs, respectively. The presence of nanoparticles declined flexural stiffness by about 16.39%. Scanning electron microscopy (SEM) images of the specimen were used to evaluate the dispersion quality of CNTs. The results of this study can be exploited in constructing conductive composite electrodes to be used in petroleum environments such as crude oil electrostatic tanks.