• 제목/요약/키워드: ex-form

검색결과 139건 처리시간 0.028초

2-Bromoacetyl-6-methoxynaphthalene을 형광유도체화제로 HPLC와 SPE를 이용한 생약제제 중 Ursodeoxycholic acid의 정량 (Determination of Ursodeoxycholic Acid in Crude Drug Formulations by HPLC and SPE Using Selective Pre-column Derivatization with 2-Bromoacetyl-6-methoxynaphthalene)

  • 진창화;임수희;이기진;심형섭;조의환;염정록
    • 약학회지
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    • 제46권6호
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    • pp.392-397
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    • 2002
  • A simple and sensitive high performance liquid chromatographic method to quantitate ursodeoxycholic acid in crude drug pharmaceuticals was investigated. Ursodeoxycholic acid react with 2-bromoacetyl-6-methoxynaphthalene (Br-AMN) in the presence of triethylamine to form highly fluorescent derivative. The derivatization procedure was performed at 7$0^{\circ}C$ and completed within 30 min. The optimal wavelength of the fluorescence detector are λ$_{ex}$=300 nm and λ$_{em}$ = 460 nm. The LOD of the ursodeoxycholic acid was 25 ng/mι based on the S/N =3, and the LOQ was 80 ng/mι based on S/N = 10. Crude drug pharmaceuticals pretreated by solid phase extraction (Sep-pak $C_{18}$ cartridge) which were shown very good separation and recovery values for the compound.d.

Anabaena koreana sp. nov. (Cyanophyceae), a new species, and new record of fresh-water blue-green algae from Korea

  • Kim, Han Soon
    • Journal of Ecology and Environment
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    • 제36권4호
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    • pp.293-302
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    • 2013
  • The present study summarizes the occurrence, distribution and autecology of 12 taxa of the class Cyanophyceae collected from several swamps, reservoir and highland wetlands in South Korea from 2009 to 2012. A new species, Anabaena koreana sp. nov. and 11 taxa of blue-green algae newly recorded are described and illustrated. Anabaena koreana is similar to A. oumiana, A. spiroides and A. crassa in that the trichomes form regular coils. However, A. koreana is distinguished from these three species by the morphological characteristics of the vegetative cell, heterocyst, and akinet shape and size. This study considers 12 blue-green algal species, including a new species, Anabaena koreana sp. nov. and 11 species that are recorded for the first time in the Korean freshwater algal flora. Among them, the genus Nostochopsis Wood ex Bornet et Flahault 1886 had not previously been recorded in Korea.

Tow in 와류발생기에 의한 핀-관 열교환기의 성능실험 (Performance Evaluation in Fin-Tube Heat Exchanger by Tow-In Winglet Pairs)

  • 곽경민;;배철호
    • 설비공학논문집
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    • 제15권2호
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    • pp.87-94
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    • 2003
  • To reduce the air side pressure drop in air-cooled heat exchanger, tow-in type winglet vortex generators are applied. A specially designed multiple-channel test core was used in the experiments for the various geometry of winglet vortex generators. The proposed tow-in type vortex generator gives significant separation delay, reduces form drag, and removes the zone of poor heat transfer from near-wake of the tubes. The results show the significant pressure drop reduction for the tow-in win91e1 vortex generators with the similar enhancement of the heat transfer as other vortex generator applications in heat exchanger. In the range of Reynolds number of 350 to 2100 the pressure drop decrease 8∼15% and 34∼55% for the in-line and staggered tube banks, respectively, compared to those without vortex generators.

Interactive Multimedia Service Terminal for IMPRESS

  • Park, Jin-sang;Park, Jong-Hoon
    • 한국방송∙미디어공학회:학술대회논문집
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    • 한국방송공학회 1997년도 Proceedings International Workshop on New Video Media Technology
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    • pp.67-70
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    • 1997
  • This Paper describes the system configuration and implementation method of an IMPRES (Interactive Multimedia exPRESS) terminal. The terminal is developed in the form of a PC add-on board that is called MINIBA (Media and Network Interface Board Assembly). IMPRESS is a communication service platform that support various interactive multimedia services. The main objectives of developing IMPRESS are to implement DAVIC compliant services platform to verify DAVIC specification and to support testing environment. Currently IMPRESS terminal provides MPEG-2 quality movies on demand, switched video broadcasting, and home-shopping service to the service user, based on the ATM network.

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현대 실내공간디자인에 있어서 유리재료의 표현기법에 관한 연구 (A Study on the Representation Techniques of Glass Material in Contemporary Interior Space Design)

  • 김은정;홍관선
    • 한국실내디자인학회:학술대회논문집
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    • 한국실내디자인학회 2007년도 추계학술발표대회 논문집
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    • pp.134-138
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    • 2007
  • Presents age is diversified in all genres by fast development of information and digital, and expression of fixing is not. Architecture and interior space design is showing new paradigm through dematerializing, ex-formal, nonlinear. Glass material is expressing by various technique in space and outer skin to introduction of digital media and a high-tech technology. Expressive characteristics and Techniques of this glass material are showing form of homogenized life in this age, simulated life. Therefore, this study does theoretical investigation through dematerializing of glass material, and analyzes works after 2000. Wish to understand stream of indoor design of present age after analyzes expression special quality and technique of glass material that reflect age and make a study of symbolic expression characteristic.

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Purification, Structure Determination and Biological Activities of 20(29)-lupen-3-one from Daedaleopsis tricolor(Bull.ex Fr.)Bond.et Sing.

  • 김은미;정해룡;민태진
    • Bulletin of the Korean Chemical Society
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    • 제22권1호
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    • pp.59-62
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    • 2001
  • The dried fruit-body of Daedaleopsis tricolor was extracted by the petroleum ether. The extracts were purified by liquid-liquid extraction, column chromatography, and recrystallization. The purified compound was a colorless orthorhombic crystal form. Its melting point, molecular weight and molar extinction coefficient $(\varepsilon)$ were estimated $168-170^{\circ}C$, 424 and 3,935 at 208 nm, respectively. Its structure was elucidated to be 20(29)-lupen-3-one by UV-Vis, FT-IR, NMR and X-ray crystallographic analysis. It showed antifungal activities against Saccharomyces cerevisiae and Microsporum gypseum, and antibacterial activities against Escherichia coli, Proteus vulgaris, Pseudomonas pyocyanea, Bacillus subtilis, and Staphylococcus aureus. In addition, this compound showed an antioxidative activity on lipid-peroxidation by 6.4%.

Vibrational Analysis of Dopamine Neutral Bae based on Density Functional Force Field

  • 박선경;이남수;이상호
    • Bulletin of the Korean Chemical Society
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    • 제21권10호
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    • pp.1035-1038
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    • 2000
  • Vibrational properties of dopamine neutral species in powder state have been studied by means of the normal mode analysis based on the force constants obtained from the density functional calculation at B3LYP level and the results of Fourier trans form Raman and infrared spectroscopic measurements. Ab initio calculation at MP2 level shows that the trans conformer of dopamine has higher electronic energy about 1.4 kcal/mol than those of the gauche+ and the gauche-conformers, and two gauche conformers have almost the same energies. Free energies calculated at HF and B3LYP levels show very similar values for three conformers within 0.3 kcal/mol. Empirical force field has been constructed from force constants of three conformers, and refined upon ex-perimental Raman spectrum of dopamine to rigorous values. The major species of dopamine neutral base in the powder state is considered a trans conformer as shown in the crystallographic study of dopamine cationic salt.

『빌러비드』: 재기억을 통한 정체성 회복 (Beloved: Identity Recovery through Rememory)

  • 김혜진
    • 영미문화
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    • 제16권2호
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    • pp.29-45
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    • 2016
  • The purpose of this study is to research how the writer describes characters of the text who overcome traumatic experiences and restore their identity through rememory in Toni Morrison's Beloved. The writer, Morrison gives the female characters their voices to recover their ethnic identities. By breaking silence, they establish their identities and become Americans from "unspeakable thoughts" to "speaking subjects." The ex-slave Sethe and her daughter, Denver have experienced trauma which works from traces of memory and history after slavery was abolished. Sethe and Denver are isolated from the community at the 124 Bluestone Road. When Beloved, ghost who was killed by Sethe, appears, Sethe and Denver are wondering who she is. Rememorying in Beloved is the important form of narrative that Morrison uses to recover their trauma. Morrison emphasizes the need to reconcile with the community and the aid of community for Sethe and Denver to heal their truma. Thanks to Beloved who leads Sethe and Denver to the community, they can be finally one of the community members in America.

Micro-and nanofibrous scaffold for enhanced cartilage regeneration

  • Lee, Myung-Hee;Shim, In-Kyong;Hwang, Jung-Hyo;Ahn, Hyun-Jung;Lee, Sang-Hoon;Lee, Myung-Chul;Lee, Seung-Jin
    • 대한약학회:학술대회논문집
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    • 대한약학회 2003년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2-2
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    • pp.229.2-230
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    • 2003
  • Extracellular matrix(ECM) is composed of the ground materials(proteoglycan) and nano size diameter fibrous proteins(ex. collagens) that together form a composite-like structure. In this study, fibrous scaffold with biomimetic architecture based on collagen nanofibers interpenetrated in PLGA/chitosan microfibrous matrix. Chitosan was selected for its structure similarity to glycosaminoglycan and neutralizing capacity for PLGA acidic metabolite. Collagen nanofiber were prepared by electrospinning. (omitted)

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인기 TV 드라마에서 질병을 활용하는 방법 (Method of Using Disease in Television Drama)

  • 노동렬
    • 한국콘텐츠학회논문지
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    • 제17권8호
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    • pp.351-365
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    • 2017
  • 텔레비전 드라마에서 질병을 활용하는 방법은 여자주인공에게 육체적 질병이 극 후반에 발병하는 추세로부터 남자주인공에게 정신적 질병이 극 초반부터 발현되는 양상으로 변화하고 있다. 특히 질병이 여성에게 발병하는 경우는 사망으로 이어지며 갈등이 해결되는 반면, 남성의 발병은 캐릭터를 구축하는 도구인 동시에 스토리에 인과관계를 설정하고 갈등을 증폭시키는 소재로 활용된다. 따라서 정신적 질병은 스토리 전개에서 반전, 발견, 전환점을 지속적으로 만들어내며 시청자들에게 긴장감과 감정이입, 동일시, 그리고 서스펜스를 유발하는 기능을 수행하고 있다. 결국 질병 활용 방법은 여성을 죽음으로 몰아가며 스토리를 종결하는 데우스엑스마키나로부터 남성의 정신적 질병으로 인해 플롯의 다양성과 장르 핍진성이 강화되는 방향으로 진화하면서 드라마를 변화시키고 있다. 이는 우리 드라마산업이 멜로드라마 위주에서 다양한 장르 특성이 강화되고 있음을 의미한다.