• Title/Summary/Keyword: evaporation residue

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The Development of Nonvolatile Residue (NVR) Particle Monitoring System in Ultra Pure Water (초순수 물(Ultra Pure Water)내 비휘발성 잔류 물질(Nonvolatile Residue, NVR)의 모니터링을 위한 NVR 측정시스템의 개발)

  • Chung, Hyeok;Ahn, Jin-Hong;Ahn, Kang-ho
    • Journal of the Semiconductor & Display Technology
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    • v.9 no.1
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    • pp.55-59
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    • 2010
  • In this study, we developed nonvolatile residue (NVR) real-time monitoring system to measure the nonvolatile residue particle in ultra pure water (UPW). This device has a capability of measuring 4 different channels, i.e., 10 nm, 30 nm, 50 nm, and 100 nm. Until now, the light scattering method to detect RAE(residue after evaporation) was the only choice. However, this method can detect RAE larger than ca. 50 nm. In ultra pure water, RAE particles are usually very small and hard to detect with conventional laser scattering devices. To detect very small RAEs, a new system is developed and tested. The system consists of an atomizer that generates RAE particles and a four channel condensation particle counter (CPC). During the several months' operation in manufacturing line, the system was successfully tested and showed reliable results.

Quantitative Analysis of Soluble Residues by Correction of Starch Content in Paperboard Grade (전분 함량 보정을 통한 판지류의 가용성 잔류물질 정량 분석)

  • Lim, Chae-Hoon;Park, Joung-Yoon;Lee, Tai-Ju;Um, Gi Jeung;Kim, Hyoung-Jin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.6
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    • pp.78-87
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    • 2013
  • Even though the notice No. 2010-11 of the Ministry of Food and Drug Safety Administration that has been applied to analyze the content of the water soluble residue eluted from multi-layer paperboard was abolished in 2011, its application for the analysis on evaporation residue is still valid. There are very high possibilities that the noticed existing method gives the misleading result on the evaporation residue due to the water soluble starch eluted from the multi-layer paperboard. The quantitative analysis on water-soluble residue with starch content correction has been carried in the study using UV/Vis spectroscopy and HPLC. The UV/Vis spectroscopy absorbance analysis showed the large amount of the oxidized starch obtained from the aqueous residue eluted out of the multi-layer paperboard after the iodine, ${\alpha}$-amylase reaction, and starch hydrolysis. The residual content decreased by the correction through the enzyme hydrolysis.

Effects of the Decomposition Residue of Compound Additive on Resintering Behavior

  • Kim, H.S.;C.Y. Joung;Kim, S.H.;S.H. Na;Lee, Y.W.;D.S. Sohn
    • Nuclear Engineering and Technology
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    • v.34 no.4
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    • pp.323-330
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    • 2002
  • Various types of compounds were tested with the aspects of decomposition and formation of residue in a $CO_2$ or 7H$_2$+93$N_2$ atmosphere. The evaporation temperature range of each compound was determined from thermogravimetric curve. Decomposition of dicarbon amide, stearic acid, acrowax and zinc stearate was studied by thermogravimetry in $CO_2$ or in 7H$_2$+93$N_2$ atmosphere. All compounds were decomposed in $CO_2$ atmosphere at lower than 40$0^{\circ}C$, but the residue, ZnO remained for zinc stearate. ZnO did not decompose in $CO_2$ atmosphere up to 130$0^{\circ}C$, but reduced into Zn metal and disappeared in the temperature range of $600^{\circ}C$ to 120$0^{\circ}C$ in 7H$_2$+93$N_2$ atmosphere. The effect of residue, which trapped in closed pores of sintered pellet, on the thermal stability was studied using the resintering test at 1$700^{\circ}C$ in 7H$_2$+93$N_2$ atmosphere. In the case of oxidative sintered pellet with admixing zinc stearate, the cavity formation accompanied with a density drop after resintering is due to the pressure of the Zn gases trapped in the isolated pores.

Research on Improving Drying Technology For Sewage Waste Using Direct Flotation Using Heat Storage Media (축열메디아 활용 직접부상방식을 이용한 하수찌꺼기의 건조기술 향상에 관한 연구)

  • Sung-Il Noh;Ung-Yong Kim;Sung-Gyun Jo;Hyun-Gon Shin
    • Journal of the Korea Organic Resources Recycling Association
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    • v.31 no.4
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    • pp.5-11
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    • 2023
  • This study was conducted to improve energy efficiency and problems such as clumping and fouling in the glue zone that occur in the moisture content range of 40 to 60% when sewage dehydration residue is directly fed into the dryer. The temperature of the hot air is low at 270~300℃, and the paddle-type flotation method and dehydrated residue are applied to the circulated heat storage media to increase the contact area with the hot air, thereby reducing energy recovery and gas emissions. The water content of the dried residue is 2.7. ~7 .5%, the heat of evaporation of moisture was 608.0~690.6 kcal/kg·H2O, which confirmed an energy saving effect of about 8.8% compared to the heat of evaporation of moisture of 714.5 kcal/kg·H2O when no heat storage media was used.

Analysis of ultra-low radionuclide concentrations in water samples with baromembrane method

  • Vasyanovich, Maxim;Ekidin, Aleksey;Trapeznikov, Alexander;Plataev, Anatoly
    • Nuclear Engineering and Technology
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    • v.53 no.1
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    • pp.253-257
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    • 2021
  • This work demonstrates the use of baromembrane method based on reverse osmosis (RO) process. The method is realized on mobile complex, which allows to concentrate and determine ultra-low activity of radionuclides in water cooling ponds of Russian nuclear fuel cycle enterprises. The existence level of radionuclide background creates difficult conditions for identification the contribution of liquid discharges enterprise, as standard monitoring methods have a very high detection level for radionuclides. Traditional methods for determining the background radionuclides concentrations require the selection of at least 500 liters (l) of water, followed by their evaporation to form a dry residue. This procedure with RO membranes requires at least 5 days. It is possible to reduce the time and energy spent on evaporation of hundreds of water liters by pre-concentrating radionuclides in a smaller sample volume with baromembrane method. This approach allows preliminary concentration of water samples from 500 l volume till 20 l volume during several hours. This approach is universal for the concentration of dissolved salts of any heavy metals, other organic compounds and allows the preparation of water countable samples in much shorter time compared to the traditional evaporation method.

Color Index and Coloring Substances in Korean Sugar Maple, Acer mono Max.,Syrup (고로쇠나무(Acer mono Max.)수액(樹液) 표준농축액(標準濃縮液)의 색도지수(色度指數)와 착색물질(着色物質))

  • Ahn, Won Yung
    • Journal of Korean Society of Forest Science
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    • v.26 no.1
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    • pp.7-12
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    • 1975
  • The sap uses of Korean sugar maple, Acer mono Max., "Gorosoe-namoo," the most abundant growing stock in maples, for a medical beverage at every early spring have had the long history in Korea. The sap of Korean sugar maple (the maple) was prepared with a unique tapping method from the trees during the sap flow season of 1974, measured the sugar content in $2.6^{\circ}$ to $3.3^{\circ}Brix$ of sugar on average and the sugar concentration of the sap was enough for a sweetener resource comparing with those of American sugar maples in literature. The color of sirup was very dark and the color index was 2.69 for the sirup of $15.3^{\circ}Brix$ having 10 hours evaporation and 3.380 for the standard sirup, as shown in Table 3 and Figure 2, due to the prolonged evaporation in deep aluminium or stainless steel kettles. The alcohol extractives of standard sirup has the light color and the residue reddish brown and the absorption spectra have the maxima in wave length of 350 nm, 1,000 nm, 1,170 nm, 1,400 nm and 1900 nm, as shown in Figure 3. The extractives of ethanol and monoethanolamine mixture (97:3, v/v) has dark red and the residue darker redish brown.

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Fiber Analysis and Environmental Assessment of Recycled Waste paper for Eco-friendly Corrugated Box Manufacture (친환경 골판지 상자 제조를 위한 재활용 폐지 섬유의 물리적·환경적 특성 평가)

  • Park, Jung-Yoon;Lee, Tai-Ju;Kim, Hyoung-Jin;Kim, Jin-Mu
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.4
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    • pp.65-74
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    • 2013
  • In the manufacture of corrugated box, the fibrous raw materials are mainly consisted of recycled papers, such as KOCC(Korean Old Corrugated Container), kraft sack, and AOCC(American Old Corrugated Container). Among these recycled waste paper, the proportion of KOCC is relatively higher than others in fibrous raw materials. Generally, KOCC shows some poor fiber properties and contains hazardous heavy metal sources. Therefore, it is to evaluate the property of recycled paper sources for eco-friendly corrugated box manufacture. In this study, the physical and mechanical properties of 3 kinds of recycled fibers and their mixed stocks were analyzed. The environmental assessment was also evaluated by analyzing the 4 representative heavy metal contents and evaporation residues in waste papers. As the results, KOCC showed the poorest fiber qualities and had the highest heavy metal contents and evaporation residues among the recycled fibers. Finally, the mechanical strength properties were increased by decreasing KOCC proportion of mixed stock conditions. In addition, the heavy metal contents and evaporation residues were also decreased by increasing recycled AOCC and kraft sack proportion.

Industrial Waters of Taegu City and on the Objection of Iron for Water Softening (大邱市의 工業用水와 鐵의 軟化障害에 關하여)

  • Lee, Dae-Soo;Hong, Soon-Yung
    • Journal of the Korean Chemical Society
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    • v.6 no.2
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    • pp.117-121
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    • 1962
  • The waters throughout Taegu area for 87 points were analysed and according to the analytical data, following unfavorable characteristics for industrial uses were given: (1)Shows strong hardness, (2)Has high ratio of ignition residue to evaporation residue, (3) pH value is over 7, (4) Contains considerable quntities of iron.And then investigated the exchange rate and regeneration level of iron ion using cation exchange resin, Lewatit KS.When the hard water containing 2.2 ppm of iron with 18.4 ppm of calcium and 6.2 ppm of magnesium was passed through the ion exchange resin under $3cc/cm^2/min$ in exhaustant flow rate, exchange rate of iron reached to 42% after 300 hours flow. The exchange efficiency shows abrupt decreasing in initial stage of flow up to 100 hours flow. The exchanger which contains iron was regenerated with 10% sodium hydroxide aqua solution under SV (space velocity) 4. By this method, 57% of iron was eliminated from exchanger while calcium and magnesium are removed as much as 85% and 87% respectively.

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Salt Repellent Behavior of Superhydrophobic Filtration Membrane

  • Sin, Bong-Su;Kim, Ho-Yeong;Lee, Gwang-Ryeol;Mun, Myeong-Un
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.236-236
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    • 2012
  • In this study, we present the salt repellent behavior of superhydrophobic filtration membrane. Bio-fouling or mineral-fouling is the main factor of decreasing the performance of filtration membrane. The superhydrophobic modification of filtration membrane using PECVD (Plasma enhanced chemical vapor deposition) is introduced. The oxygen plasma was introduced for developing nano hairy structures and subsequent HMDSO (Hexamethyldisiloxane) coating was used for enhancing low surface energy. Saline water evaporation test was carried out to evaluate the difference of contamination of salt on superhydrophobic and moderately hydrophobic filtration membrane. EDS and EPMA were used for visualizing the residue of salt crystal.

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Mutagenicity of Diesel-Exhaust Particulates

  • Yoo, Young S.
    • Journal of Korean Society for Atmospheric Environment
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    • v.10 no.E
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    • pp.325-331
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    • 1994
  • Organic extracts of diesel- exhaust particulates were analyzed for mutagenicity using Ames Salmonella typhimurium assay system. An experimental diesel microbus used was drived on the chassis dynamometer according to CVS-75 mode. The samples were taken from the mixed gases in a dilution tunnel. With a high-volume air sampler equipped with double filter holders, particulate matters were collected on a teflon-coated glass fiber filter placed behind a activated carbon filter. After ultrasonic extraction with benzene- ethanol and evaporation to dryness, the residue was dissolved in dimethylsulfoxide. Each sample was tested toward 2 strains, TA100 and TA98 by the pre-incubation method in the absence and presence of S-9mix. Average concentration of diesel- exhaust particulates was about 116.6mg/m$^3$, and 44.1~62.2 % to the total weight of particulates, consisted of organic matters. The mutagenicities of diesel- exhaust particulate organic matters were 4,512 and 2,205 revertants/m$^3$ toward TA100 without and with S-9mix, respectively. Those toward TA98 were 13,367 and 3,715 revertants/m$^3$, respectively.

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