• Title/Summary/Keyword: epoxy bonding

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A Study on Mechanical Strength in AI7075/CFRP Hybrid Composite (AI7075/CFRP 하이브리드 복합재료의 기계적강도 평가에 관한 연구)

  • 유재환
    • Journal of the Korean Society of Safety
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    • v.12 no.4
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    • pp.57-62
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    • 1997
  • The combined structure of hybrid composite made through the bonding process of materials of different properties greatly defines its mechanical characteristics, as the results of the experiments on materials of different properties show much dissimilarity. When carbon/epoxy materials are applied to hybrid composite, the carbon materials helps to improve the mechanical properties of the hybrid composite, and the epoxy reduces its fracture strain and impact resistance. Carbon fiber which is now in general commercialization is classified as high modulus or high strength system, and its manufacturing methods are various. The study of the materials having combined structure is focused on the numerical analysis of the layers of bonding surface in materials with difference modulus. The hybrid composite made through the multilayered bonding of reinforced aluminium sheets with aramid fiber now faces the marketing phase, and especially its excellent fatigue resistance and mechanical properties promote active researches on the similar products of hybrid composite. This study aims to investigate the effects of CFRP volume ratio and fiber's orientation over the properties of mechanical strength and fatigue life of the hybrid composite, AI7075/CFRP. To carry out this study, static tensile and fatigue tests were given to some of the panels which, made through the co-cure processing in an autoclave, have different CFRP volume ratio and carbon fiber orientations.

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Effect of Surface Treatment on Adhesive Bonding Strengh of Composite Material for Cryogenic Application (극저온용 복합재료의 접착부 강도에 미치는 표면처리 효과에 대한 연구)

  • Ahn, Myoung-Ho;So, Yong-Shin;Park, Dong-Hwan
    • Proceedings of the KWS Conference
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    • 2010.05a
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    • pp.28-28
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    • 2010
  • The secondary barrier of cargo containment for membrane LNG tank is composed of composite materials such as rigid triplex (rigid secondary barrier, RSB) and flexible triplex (flexible secondary barrier, FSB). RSB and FSB are adhered to each other using an epoxy adherent and the quality of the secondary barrier depends on the bonding strength between them. The bonding strength between RSB and FSB is greatly influenced by the surface condition of RSB prior to joining. In this study, the effect of surface condition prior to joining on the joint strength and the fracture mode occurred between RSB and FSB have been examined in order to establish a proper surface treatment method for improving the bonding strength at the temperature of $-170^{\circ}C$.

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Adhesion of Model Molecules to Metallic Surfaces, the Implications for Corrosion Protection

  • de Wit, J.H.W.;van den Brand, J.;de Wit, F.M.;Mol, J.M.C.
    • Corrosion Science and Technology
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    • v.7 no.1
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    • pp.50-60
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    • 2008
  • The majority of the described experimental results deal with relatively pure aluminium. Variations were made in the pretreatment of the aluminum substrates and an investigation was performed on the resulting changes in oxide layer composition and chemistry. Subsequently, the bonding behavior of the surfaces was investigated by using model adhesion molecules. These molecules were chosen to represent the bonding functionality of an organic polymer. They were applied onto the pretreated surfaces as a monolayer and the bonding behavior was studied using infrared reflection absorption spectroscopy. A direct and clear relation was found between the hydroxyl fraction on the oxide surfaces and the amount of molecules that subsequently bonded to the surface. Moreover, it was found that most bonds between the oxide surface and organic functional groups are not stable in the presence of water. The best performance was obtained using molecules, which are capable of chemisorption with the oxide surface. Finally, it was found that freshly prepared relatively pure aluminum substrates, which are left in air, rapidly lose their bonding capacity towards organic functional groups. This can be attributed to the adsorption of contamination and water to the oxide surface. In addition the adhesion of a typical epoxy-coated aluminum system was investigated during exposure to water at different temperatures. The coating was found to quite rapidly lose its adhesion upon exposure to water. This rapid loss of adhesion corresponds well with the data where it was demonstrated that the studied epoxy coating only bonds through physisorptive hydrogen bonding, these bonds not being stable in the presence of water. After the initial loss the adhesion of the coating was however found to recover again and even exceeded the adhesion prior to exposure. The improvement could be ascribed to the growth of a thin oxyhydroxide layer on the aluminum substrate, which forms a new, water-stable and stronger bond with the epoxy coating. Two routes for improvement of adhesion are finally decribed including an interphasial polymeric thin layer and a treatment in boiling water of the substrate before coating takes place. The adhesion properties were finely also studied as a function of the Mg content of the alloys. It was shown that an enrichment of Mg in the oxide could take place when Mg containing alloys are heat-treated. It is expected that for these alloys the (hydr)oxide fraction also depends on the pre-treatment and on the distribution of magnesium as compared to the aluminium hydroxides, with a direct impact on adhesive properties.

A study on the bonding strength of co-cured T800/epoxy composite-aluminum single lap joint according to the forming and additional pressures (동시 경화법으로 제조된 T800/에폭시 복합재료-알루미늄 단면겹치기조인트의 성형압력 및 부가압력에 따른 접착강도에 관한 연구)

  • Son, Dae-Sung;Bae, Ji-Hun;Chang, Seung-Hwan
    • Composites Research
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    • v.24 no.5
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    • pp.23-28
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    • 2011
  • In this paper, the bonding strengths of co-cured T800 carbon/epoxy composite-aluminum single lap joints with and without additional pressures were investigated using the pressure information induced by the fiber tension during a filament winding process. The specimens of all the tests were fabricated by an autoclave vacuum bag de-gassing molding being controlled forming pressures (absolute pressures of 0.1MPa, 0.3MPa and 0.7MPa including vacuum). A special device which can act uniform additional pressures on the joining part of the single lap joint specimen was designed to measure the bonding strengths of composite-aluminum liners of type III hydrogen pressure vessel fabricated by a filament winding process. After the three different additional pressures (absolute pressures of 0.1MPa, 0.3MPa and 0.7MPa) were applied to the specimens the effect of the additional pressures on the bonding strengths of the co-cured single-lap joints were evaluated.

Interface Characteristics of Epoxy Composite Treated with Silane Coupling Agent (실란 결합제 처리된 에폭시 수지 복합재료의 계면 특성)

  • Lee, Jae-Yeong;Lee, Hong-Gi;Sim, Mi-Ja;Kim, Sang-Uk
    • Korean Journal of Materials Research
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    • v.11 no.12
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    • pp.1009-1013
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    • 2001
  • The effects of coupling agent on the interface characteristics between epoxy resin and natural zeolite were studied by SEM, optical microscope and universal testing machine (UTM). Epoxy resin as a matrix was diglycidyl ether of bisphenol A (DGEBA)/4,4'-methylene dianiline (MDA)/malononitrile (MN) system and natural zeolite as an inorganic fillet was produced in Korea. With the increment of zeolite content, tensile strength decreased and it was due to the different elastic moduli of two materials. When external stress was loaded on the composites, the stress concentrated on the weakly bonded interface and crack grew easily. To improve the interface characteristics, the surface of the natural zeolite was treated with the silane coupling agent and it was found that the tensile strength was increased. The morphology of the interface showed that the bonding characteristics were modified by coupling agent.

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Relaxation of Singular Stress in Adhesively Bonded Joint at High Temperature

  • Lee, Sang Soon
    • Journal of the Semiconductor & Display Technology
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    • v.17 no.1
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    • pp.35-39
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    • 2018
  • This paper deals with the relaxation of singular stresses developed in an epoxy adhesive at high temperature. The interface stresses are analyzed using BEM. The adhesive employed in this study is an epoxy which can be cured at room temperature. The adhesive is assumed to be linearly viscoelastic. First, the distribution of the interface stresses developed in the adhesive layer under the uniform tensile stress has been calculated. The singular stress has been observed near the interface corner. Such singular stresses near the interface corner may cause epoxy layer separated from adherent. Second, the interfacial thermal stress has been investigated. The uniform temperature rise can relieve the stress level developed in the adhesive layer under the external loading, which can be viewed as an advantage of thermal loading. It is also obvious that temperature rise reduces the bonding strength of the adhesive layer. Experimental evaluation is required to assess a trade-off between the advantageous and deleterious effects of temperature.

Evaluation of Shrinkage Properties of Tiles Reinforced with Epoxy Resin Adhesive (에폭시 수지 접착제를 보강한 타일의 수축특성 평가)

  • Lee, Sang-Kyu;Kim, Gyu-Yong;Hwang, Eui-Chul;Son, Min-Jae;Lee, Sang-yun;Nam, Jeong-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.11a
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    • pp.163-164
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    • 2020
  • The purpose of this study was to evaluate the shrinkage properties of a tile reinforced with epoxy resin, which has the advantages of high adhesion and low shrinkage, and causes a hardening reaction by chemical bonding with cement mortar. As a result, since the epoxy resin adhesive suppresses the moisture evaporation of the mortar, the drying shrinkage of the mortar itself is reduced, accordingly, the shrinkage of the tile itself is greatly reduced, and it is thought that it is possible to prevent a decrease in adhesion due to shear stress.

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The Study on Fine-Pitch Pattern Formation Using epoxy bonding film Surface modification and Semi-additive Method (Epoxy Bonding Film 표면 개질과 도금공정을 이용한 미세패턴형성에 관한 연구)

  • Kim, Wan-Joong;Park, Se-Hoon;Jung, Yeon-Kyung;Lee, Woo-Sung;Park, Jong-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.165-165
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    • 2009
  • 현재 반도체나 이동통신 분야는 사용자의 요구에 따라 PCB의 회로선폭이 갈수록 좁아지고 있다. 이러한 정밀 부품을 제조하기 위한 제조공정에서 각광받기 시작한 기술 중 하나가 대기압 플라즈마 기술이다. 본 연구에서는 미세패턴 형성이 가능한 에폭시 본딩 필름위에 무전해 도금공정을 통한 패턴 도금법을 이용하여 패턴을 형성하였고, 형성된 패턴에 대기압 플라즈마 처리 횟수에 따른 접촉각(Contact Angle)과 Peel Strength의 변화를 분석하였다. 또한 에폭시 본딩 필름을 이용한 Build-up공정을 거쳐 Micro Via를 형성하여 대기압 플라즈마 처리 횟수에 따른 Via 표면을 분석하였다. 대기압 플라즈마 기술은 진공식에 비해 소규모 장비를 이용한 전처리가 가능하고, 초기 설비비용을 절감하는데 탁월한 효과가 있어 널리 사용하는 기술 중 하나이다. 이 연구를 통하여 대기압 플라즈마 처리 횟수에 따른 표면에너지의 변화로 인한 접촉각이 좋아지는 것을 알 수 있으며, 대기압 플라즈마 처리를 한 패턴표면이 친수성으로 변하면서 현상된 드라이 필름 사이로 도금액이 원활히 공급되어서 미세패턴 모양이 우수하게 구현되었음을 알 수 있었다. 또한 Via Filling에도 뛰어난 효과가 있었음을 확인할 수 있었다.

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A Study on the Bonding Performance of COG Bonding Process (COG 본딩의 접합 특성에 관한 연구)

  • Choi, Young-Jae;Nam, Sung-Ho;Kim, Kyeong-Tae;Yang, Keun-Hyuk;Lee, Seok-Woo
    • Journal of the Korean Society for Precision Engineering
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    • v.27 no.7
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    • pp.28-35
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    • 2010
  • In the display industry, COG bonding method is being applied to production of LCD panels that are used for mobile phones and monitors, and is one of the mounting methods optimized to compete with the trend of ultra small, ultra thin and low cost of display. In COG bonding process, electrical characteristics such as contact resistance, insulation property, etc and mechanical characteristics such as bonding strength, etc depend on properties of conductive particles and epoxy resin along with ACF materials used for COG by manufacturers. As the properties of such materials have close relation to optimization of bonding conditions such as temperature, pressure, time, etc in COG bonding process, it is requested to carry out an in-depth study on characteristics of COG bonding, based on which development of bonding process equipment shall be processed. In this study were analyzed the characteristics of COG bonding process, performed the analysis and reliability evaluation on electrical and mechanical characteristics of COG bonding using ACF to find optimum bonding conditions for ACF, and performed the experiment on bonding characteristics regarding fine pitch to understand the affection on finer pitch in COG bonding. It was found that it is difficult to find optimum conditions because it is more difficult to perform alignment as the pitch becomes finer, but only if alignment has been made, it becomes similar to optimum conditions in general COG bonding regardless of pitch intervals.