• 제목/요약/키워드: elemental analysis

검색결과 1,140건 처리시간 0.039초

Analysis of Off-axis Integral Floating System Using Concave Mirror

  • Kim, Young Min;Jung, Kwang-Mo;Min, Sung-Wook
    • Journal of the Optical Society of Korea
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    • 제16권3호
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    • pp.270-276
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    • 2012
  • An off-axis integral floating system using a concave mirror is analyzed to resolve the image distortion incurred by the off-axis optical arrangement. The concave mirror can be adopted as the floating device to improve the optical efficiency. The image distortion due to the tilting axis of the concave mirror needs to be analyzed precisely to generate the pre-distortion image. In this paper, we calculate the image deformation in the off-axis structure of the concave mirror using the geometrical optics. Using the calculation results, the compensated elemental image can be generated for the pre-distortion integrated image, which can be projected to the floating 3D image without image distortion. The basic experiments of the off-axis integral floating are presented to prove and verify the proposal.

Flavin mononucleotide를 탈리기로한 백금 (II) 착체의 합성과 그 항암활성 (Synthesis of Pt(II) Complexes containing Flavin mononucleotide as Leaving Ligand and their Anticancer Activity)

  • 권영이;황규자
    • 약학회지
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    • 제43권6호
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    • pp.762-770
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    • 1999
  • A series of vitamin-containing Pt(II) complexes of the type [Pt (FMN) (L)] (FMN=flavin mononucleotide, L=ethylenediamine, 1,3-propanediamine, 1,4-bu-tanediamine) was synthesizd and characterized by IR, electronic absorption, elemental analysis and FAB=Mass. The coordination sites of FMN to Pt(II) ions were determined to be N(5) and O(6) with resultant chelate ring formation. Theses compounds have much better water solubility (30-35 mg/ml) than cisplatin (1 mg/ml). The anticancer activity of this vitamin-containing Pt(II) series was investigated by MTT assay against mouse and human leukemia cell lines in vitro. Among these compounds, FMN (1,4-butanediamine) Pt(II) having seven-membered ring structure as amine ligand showed moderate anticancer activity.

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유기 EL용 청색 발광 히드라존 유도체의 합성 (Synthesis of Blue Emission Hydrazone Derivatives for Organic Electroluminescence)

  • 정평진;임회득
    • 한국재료학회지
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    • 제13권8호
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    • pp.514-518
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    • 2003
  • As a fundamental study on organic electroluminescence(EL), blue emitting materials were synthesized and characterized. Individual blue colored hydrazone derivatives were synthesized from the reaction of aldehydes (phthalaldehyde, isophthalaldehyde) with the corresponding amnios (1-methyl -1-phenylhydrazine, 1,1-diphenylhydrazine hydrochloride). Recrystallization of hydrazones from chloroform revealed the melting temperature within $142∼156^{\circ}C$. Photoluminescence(PL) analysis on each hydrazone showed that emission range were blue(458∼478 nm). The structure of obtained hydrazones were elucidated by FT-IR, $^1$H-NMR and C, H, N elemental analyzer.

기능성 유기초박막의 제작기술과 성막물질의 합성 연구 (Fabrication of Functional Organic Ultrathin (LB) Film and Synthesis of Film Material - N-Alkylquinolium TCNQ Complexes -)

  • Shin, Dong-Myung;Sohn, Byung-Chung;Kim, Jung-Soo;Kang, Dou-Yol
    • 대한전기학회논문지
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    • 제41권7호
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    • pp.753-759
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    • 1992
  • For the fabrication of the microscale memory or electrical devices, Langmuir-Blodgett(LB) method is the most possible candidate. N-Alkylquinolium-TCNQ compounds were synthesized. The structure of the compounds were identified by the NMR spectroscopy and the purity were checked to be good by the elemental analysis. The surface pressure($\pi$) was measured at the air-water interface. The isotherm showed two transitions at 30mN/m and 45mN/m. The LB films were deposited by the home-made Kuhn type apparatus. The transfer ratio($\tau$) of the deposition was more than 0.95 for the up-stroke and less than 0.4 for the down-stroke. The absorbance peaks of the LB films appear at around 420nm and 700-820nm.

Experimental investigation for partial replacement of fine aggregates in concrete with sandstone

  • Chandar, K. Ram;Gayana, B.C.;Sainath, V.
    • Advances in concrete construction
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    • 제4권4호
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    • pp.243-261
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    • 2016
  • This research study focuses on utilizing sandstone which is overburden waste rock in coal mines to use in concrete as a replacement of fine aggregate. Physical properties of sandstone like water absorption, moisture content, fineness modulus etc., were found to be similar to conventional fine aggregate. Scanning Electron Microscope (SEM) analysis was carried out for analysing elemental composition of sandstone. There was no sulphur content in sandstone which is a good sign to carry the replacement. Fine aggregate was replaced with sandstone at 25%, 50%, 75% and 100% by volume and moulds of concrete cubes and cylinders were prepared. Compressive strength of concrete cubes was tested after 3, 7 and 28 days and split tensile & flexural strength was determined after 28 days. The strength was found to be increasing marginally with increase in sandstone content. Fine aggregate that was replaced by 100% sandstone gave highest strength among all the replacements for the compressive, split tensile and flexural strengths. Though increase in strength was marginal, still sandstone can be an effective replacement for sand in order to save the natural resource and utilize the waste sandstone.

Microstructure and Properties of High Nitrogen Sintered Stainless Steel

  • Pieczonka, Tadeusz;Stoytchev, Marin
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.568-569
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    • 2006
  • The use of the nickel free, high nitrogen stainless steel powder and nitriding during sintering of iron based materials have been shown as an alternative way to the conventional PM stainless steels containing nickel. Nitrogen as an alloying element for iron improves in an effective way the properties of sintered alloyed steels. The powder metallurgy route is a suitable way to introduce nitrogen into these alloys and, in particular, to produce high nitrogen (close to the solubility limit) stainless steels. The paper presents and discusses the nitriding behavior of nickel-free stainless steels produced by powder metallurgy method. Alloyed melt was atomized by nitrogen and in this way nitrogen was introduced into the powder. Further nitriding occurred during sintering in a nitrogen atmosphere. For comparison, compacts having the same composition as an alloyed powder were produced from elemental powders mixture. Sintering-nitriding behaviour of investigated materials has been controlled by dilatometry, chemical and X-Ray phase analysis and metallography. Mechanical properties of sintered compacts were also measured.

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Shape-Stabilized Phase Change Materials : Frozen Gels From Polypropylene and n-Paraffin for Latent Heat Storage

  • Ko, Jae-Wang;Son, Tae-Won
    • 한국염색가공학회:학술대회논문집
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    • 한국염색가공학회 2010년도 제3회 국제학회
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    • pp.80-81
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    • 2010
  • We prepared polymer-PCM gels such as prepared frozen gel from polypropylene and n-Paraffin for thermal storage and release materials, their basic properties and possible applications especially in latent heat storage. The preparation methods are used to melting method and absorption method respectively. The composition and properties of prepared frozen gels from polypropylene and n-Paraffin were observed by DSC, FT-IR spectra, ARES and Elemental analysis. We can prepare frozen gels in different temperature for latent heat storage materials as controlling composition of phase change material as well as using different incorporating phase change materials. These frozen gels can be used to latent heat storage materials for several applications.

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시아노에틸화 전처리가 면직물의 승화전사날염 공정에 미치는 영향 (Effect of Cyanoethylation Pretreatment on the Sublimation Transfer Printing of Cotton Fabric)

  • 배도규
    • 한국염색가공학회지
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    • 제32권3호
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    • pp.135-141
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    • 2020
  • The primary and secondary alcohols in cellulose reacted with acrylonitrile(AN) in the presence of strong alkalis to form cyanoethylated cellulose. The partially cyanoethylated cotton(CEC) fabric with AN in the presence of aqueous sodium hydroxide solution was described, including effects of treatment time and reagent concentrations. The weight increases of cotton fabric were shown to be linearly related to the treatment time, temperature and concentration of sodium hydroxide. The physical properties such as shrinkage ratio and tensile strength were proportional to the weight increases without significant impact on elongation. But the moisture regain decreased with decreasing hydrophilicity. The degree of substitution(DS) and transfer ratio were linearly related to the weight increases. In the CEC with increasing weight up to 24.9%, it has been obtained with DS up to 0.63-0.67 cyanoethyl groups per anhydroglucose and transferring ratio up to 87.7%. The color fastness to washing by sublimation transfer printing was improved by the cyanoethylation.

침전극 곡률반경에 따른 XLPE의 전계분포 해석 (Electric Field distribution Analysis according to radius of curvature in needle electronode)

  • 안병철;이혁진;김탁용;변두균;이종용;신종렬;이수원;홍진웅
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.234-235
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    • 2005
  • 본 논문에서는 전력용 케이블에서 초고압으로 사용되고 있는 가교폴리에틸렌 내부(XLPE)에 침투된 침전극의 곡률반경변화에 따른 XLPE의 전계분포를 경계요소법에 의한 3차원 시뮬레이션 프로그램을 통하여 해석하여, 곡률반경이 작을수록 전계가 집중되는 현상을 확인하였다.

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전자빔 증착기로 증착된 $CuInS_2$ 박막의 전기적 구조적 특성 (Electrical and Structural Properties of $CuInS_2$ thin films fabricated by EBE(Electronic Beam Evaporator) Method)

  • 양현훈;김영준;정운조;박계춘
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2006년도 춘계학술대회
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    • pp.170-173
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    • 2006
  • [ $CuInS_2$ ] filims were appeared from 0.84 to 1.27 of Cu/In composition ratio and sulfur composition ratios of $CuInS_2$ thin films fabricated, Also when Cu/In composition ratio was 1.03, $CuInS_2$ thin film with chalcopyrite structure had the highest XRD peak (112). And lattice constant (a) of and grain size of the film tin s ambient were appeared a little larger than those in only Vacuum The films in S ambient were p-type with resistive of around $10^{-1}{\Omega}cm$ and optical energy band gaps of the films in S ambient were appeared a little larger than those in only Vacuum. Analysis of the optical energy band gap of $CuInS_2$ thin films a value of 1.53eV.

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