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검색결과 320건 처리시간 0.02초

냉각판법에 의한 Mg-10Al-Mn 합금의 균질화 처리에 따른 미세조직 변화 (The Microstructural Evolution of Mg-10Al-Mn Alloy by Cooling Plate During Homogenization Treatment)

  • 김대환;최승화;김희경;심성용;임수근
    • 한국주조공학회지
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    • 제30권6호
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    • pp.235-240
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    • 2010
  • The evolution of microstructure and phases of Mg-10Al-Mn alloy by cooling plate method during homogenization treatment have been investigated with metallographic analysis, scanning electron microscopy and energy dispersive spectroscopy. The ingots used for this experiment were prepared by cooling plate and homogenization heat treatment was performed at 300 and $400^{\circ}C$ for various holding times (0, 1, 4, 8 and 12h). The casting ingots were consisted of the fine grains and eutectic phases. And, these eutectic phases were dissolved into the matrix during homogenization treatment at $400^{\circ}C$ but the lower temperature (at $300^{\circ}C$) did not be.

이중 음극층을 이용한 고휘도 전면발광(Top emission) 유기EL소자의 특성평가 (Characterization of the High Luminance Top Emission Organic Light-emitting Devices (TEOLEDs) Using Dual Cathode Layer)

  • 강윤호;이수환;신동원;김성준;김달호;이곤섭;박재근
    • 반도체디스플레이기술학회지
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    • 제5권3호
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    • pp.23-27
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    • 2006
  • Recently, Top emission organic light-emitting diode (TEOLED) has been attracted by their potential application for the development of flat panel display (FPD). We have fabricated the high luminance top emission organic-emitting diode (TEOLED) using dual cathode layer and three top emitting structure. These devices were characterized by electroluminescence (EL) and current density-voltage (J-V) measurements. After compared it with Au anode structure, luminance of the device using dual anode was better than using without Al device. Consequently, Al layers are very good candidates for a promising electron-injecting buffer layer for top emission light-emitting diode (TEOLED).

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Fungicidal Effect of Resveratrol on Human Infectious Fungi

  • Jung, Hyun-Jun;Hwang, In-Ah;Sung, Woo-Sang;Kang, Hyun-Gu;Kang, Beom-Sik;Seu, Young-Bae;Lee, Dong-Gun
    • Archives of Pharmacal Research
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    • 제28권5호
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    • pp.557-560
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    • 2005
  • Resveratrol, a phenolic antioxidant found in grapes, has been known to mediate various biological activities on the human body. In the present study, we tested the antifungal a ctivity of resveratrol against human pathogenic fungi before carrying out further studies to elucidate the antifungal mechanism(s) of resveratrol. Resveratrol displayed potent antifungal activity against human pathogenic fungi at concentration levels of 10-20 ${\mu}g$/mL. Furthermore, time-kill curve exhibited fungicidal effect of resveratrol on C. albicans, but the compound had no hemolytic activity against human erythrocytes. The destruction of C. albicans cells by resveratrol was confirmed by scanning electron microscopy. These results suggest that resveratrol could be employed as a therapeutic agent to treat fungal infections of humans.

Effects of the Redox Potential of the Acidogenic Reactor on the Performance of a Two-Stage Methanogenic Reactor

  • Phae, Chae-Gun;Lee, Wan-Kyu;Kim, Byung-Hong;Koh, Jong-Ho;Kim, Sang-Won
    • Journal of Microbiology and Biotechnology
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    • 제6권1호
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    • pp.30-35
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    • 1996
  • Distillery wastewater was used in a thermophilic laboratory-scale two stage anaerobic digester to test the effects of the redox potential of the first acidogenic reactor on the performance of the system. The digester consisted of first a acidogenic reactor and the an upflow anaerobic sludge blanket (UASB) reactor. The digestor was operated at a hydraulic retention time (HRT) of 48 h. Under these conditions, about 90% of the chemical oxygen demand as measured by the chromate method ($COD_{cr}$) was removed with a gas production yield of 0.4 l/g-COD removed. The redox potential of the acidogenic reactor was increased when the reactor was purged with nitrogen gas or agitation speed was increased. The increase in reduction potential was accompanied by an increase in acetate production and a decrease in butyrate formation. A similar trend was observed when a small amount of air was introduced into the acidogenic reactor. It is believed that the hydrogen partial pressure in the acidogenic reactor was decreased by the above mentioned treatments. The possible failure of anaerobic digestion processes due to over-loading could be avoided by the above mentioned treatments.

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The Preparation of Blue CoAl2O4 Powders by the Malonate Method: The Effect of the Amount of Malonic Acid Used, the Formation Pathway of CoAl2O4 Crystallites and the Characteristics of the Prepared Powders

  • Lee, Gong-Yeol;Ryu, Kwang-Hyun;Kim, Hong-Gun;Kim, Yoo-Young
    • Bulletin of the Korean Chemical Society
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    • 제30권2호
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    • pp.373-377
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    • 2009
  • A pathway for the formation of normal $CoAl_2O_4$ particles is suggested. The optimal amount of malonic acid was determined, and the characteristics of the obtained powders were investigated. Normal $CoAl_2O_4$ powders were prepared using solutions of malonic acid and metal nitrates. X-ray diffraction, Brunauer-Emmett-Teller (BET) and scanning electron microscope (SEM) measurements, as well as Fourier transform infrared (FTIR) and ultraviolet/visible (UV-Vis) spectroscopy were carried out. Normal $CoAl_2O_4$ crystallites were formed by a solid state reaction between $CoAl_2O_4$ and amorphous aluminum oxide. The optimal molar ratio of malonic acid to the nitrate anions present in the initial solution was found to be 0.30~0.35. The particles were composed of agglomerates of primary particles. The primary particles were 40 nm in size. This size was relatively constant regardless of the preparation temperature. However, the size of the agglomerated particles increased to 220 nm with increasing temperature.

CBD법으로 성장된 CdS 박막의 급속 열처리 효과 (Effect of Rapid thermal treated CdS Films prepared by CBD)

  • 박승범;송우창;임동건;양계준;심낙순;이상교
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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    • pp.227-227
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    • 2008
  • CdS is II-VI semiconductor with a wide band gap of approximately 2.42 eV. CdS is the most popularly employed heterojunction partner to p-CdTe due to its similar chemical properties. The as-deposited films are annealed in Rapid Thermal Annealing (RTA) system in various atmosphere(Air, Vacuum and $N_2$) at $500^{\circ}C$. In this work, X-ray diffraction (XRD), atomic force microscopy (AFM), scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) of chemical bath deposited (CBD) CdS films on glass is carried out. In case of the annealed CdS films in $N_2$, grain size was larger than as-annealed films.

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Al:Au 음극층을 이용한 양면발광(dual emission) 유기 EL 소자의 Al 두께별 특성 평가 (Characterization of Organic Light-Emitting Diode (OLED) with Dual Emission using Al:Au Cathode)

  • 이수환;김달호;양희두;김지헌;이곤섭;박재근
    • 반도체디스플레이기술학회지
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    • 제7권1호
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    • pp.47-51
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    • 2008
  • The Al:Au double-layer metal electrode for use in transparent, dual emission of organic light-emitting diode (OLED) was fabricated. The electrode of Al:Au metals with various thicknesses was deposited by the vacuum thermal evaporation technique. For Al thickness of 1 nm, a bottom luminance of $4880\;cd/m^2$ was observed at 8 V. Otherwise, top luminance of $2020\;cd/m^2$ were observed at 8 V. In addition, the threshold voltages of the electrodes were 2.2 V. It was forward that the inserting 1 nm Al between LiF and Au enhanced electron injection with tunneling effect.

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Experimental Evidence of the Mobility of Hydroperoxyl/Superoxide Anion Radicals from the Illuminated TiO2 Interface into the Aqueous Phase

  • Kwon, Bum-Gun;Yoon, Je-Yong
    • Bulletin of the Korean Chemical Society
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    • 제30권3호
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    • pp.667-670
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    • 2009
  • The understanding of behaviors of hydroperoxyl/superoxide anion radicals (${H_2O_2}^./{O_2}^{-.}$) generated from a photoirradiated $TiO_2$ surface is essential to improve the efficiency of $TiO_2$ photocatalytic reactions by decreasing the recombination of photoinduced electron-hole ($e^--h^+$) pairs. In contrast with previous studies, we found that ${H_2O_2}^./{O_2}^{-.}$ generated on the surface of illuminated $TiO_2$ particles are mobile. ${H_2O_2}^./{O_2}^{-.}$ formed by the photocatalysis of $TiO_2$ particles immobilized onto the inner surface of a coil-quartz tube were forced under a continuous flow through a knotted tubing reactor (KTR) and into the aqueous phase completely separated from the $TiO_2$ particles, and were measured by a chemiluminescence (CL) technique using 2-methyl-6-(p-methoxyphenyl)-3,7-dihydroimidazo[ 1,2-a]pyrazin-3-one (MCLA) as the reagent. The initial concentration of the ${H_2O_2}^./{O_2}^{-.}$ stream entering the KTR was determined by its half-life (98 s) at pH 5.8. We suggests that the efficiency of $TiO_2$ photocatalytic reactions may be further improved by utilizing the mobility of ${H_2O_2}^./{O_2}^{-.}$.

AlOx와 SiO2 형판위 CdSe와 CdS 박막의 우선방위(Preferred Orientation) 특성 (The Preferred Orientation of CdSe and CdS Thin Films on the AlOx and SiO2 Templates)

  • 이영건;장기석
    • 한국군사과학기술학회지
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    • 제15권4호
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    • pp.502-506
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    • 2012
  • In order to find the structural characteristics of the thin films of group II-VI semiconductor compounds compared with those of powder materials, films were made of 4 powders of ZnS, CdS, CdSe, and CdTe(Aldrich), each with 99.99 % purity. For the ZnS/CdS multi-layers, the ZnS layer was coated over the CdS layer on an $AlO_x$ membrane, which served as a protective layer within a vacuum at the average speed of 1 ${\AA}$/sec. After studying the structures of the group II-VI semiconductor thin films by using X-ray spectroscopy, we found that the ZnS, ZnS/CdS, CdS, and CdSe films were hexagonal and exhibited some degree of preferred orientation. Also, the particles of the thin films of II-VI semiconductor compounds proved to be more homogeneous in size compared to those of the powder materials. These results were further verified through scanning electron microscopy(SEM), EDX analysis, and powder and thin film X-ray diffraction.

기계 화학적 방법을 통한 Eu3+ 도핑된 (Y,Gd)BO3 형광체의 분말제조 (Synthesis of Eu3+ Doped (Y,Gd)BO3 Powder by Mechanochemical Process)

  • 원희섭;이완재;김제석;홍근영;이근재;좌용호
    • 한국분말재료학회지
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    • 제15권2호
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    • pp.136-141
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    • 2008
  • The mechanochemical process were employed to prepare the red phosphors (Y,Gd)$BO_3:Eu^{3+}$. The main factors affecting particle size, particle distribution, and luminescent properties of the product were investigated in details. Particles sized around 200-600 nm are formed after intensive milling. The phosphors were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and photoluminescence spectrum. Results revealed that phosphors with different morphology, small particle size and high luminescence intensity could be obtained by mechanochemical process.