• The Journal of Advanced Prosthodontics
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• 제9권2호
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• pp.130-137
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• 2017

PURPOSE. The purpose of this study was to evaluate the effect of nano-structured alumina surface coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements. MATERIALS AND METHODS. A total of 90 disk-shaped zirconia specimens (HASS CO., Gangneung, Korea) were divided into three groups by surface treatment method: (1) airborne particle abrasion, (2) tribochemicalsilica coating, and (3) nano-structured alumina coating. Each group was categorized into three subgroups of ten specimens and bonded with three different types of dual-cured resin cements. After thermocycling, shear bond strength was measured and failure modes were observed through FE-SEM. Two-way ANOVA and the Tukey's HSD test were performed to determine the effects of surface treatment method and type of cement on bond strength (P<.05). To confirm the correlation of surface treatment and failure mode, the Chi-square test was used. RESULTS. Groups treated with the nano-structured alumina coating showed significantly higher shear bond strength compared to other groups treated with airborne particle abrasion or tribochemical silica coating. Clearfil SA Luting showed a significantly higher shear bond strength compared to RelyX ARC and RelyX Unicem. The cohesive failure mode was observed to be dominant in the groups treated with nano-structured alumina coating, while the adhesive failure mode was prevalent in the groups treated with either airborne particle abrasion or tribochemical silica coating. CONCLUSION. Nano-structured alumina coating is an effective zirconia surface treatment method for enhancing the bond strength between Y-TZP ceramic and various dual-cured resin cements.

• The Journal of Advanced Prosthodontics
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• 제7권6호
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• pp.446-453
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• 2015

PURPOSE. To compare the push-out bond strength of feldspar and zirconia-based ceramic inlays bonded to dentin with different resin cements following simulated aging. MATERIALS AND METHODS. Occlusal cavities in 80 extracted molars were restored in 2 groups (n=40) with CAD/CAM feldspar (Vitablocs Trilux forte) (FP) and zirconia-based (Ceramill Zi) (ZR) ceramic inlays. The fabricated inlays were luted in 2 subgroups (n=20) with either etch-and-bond (RelyX Ultimate Clicker) (EB) or self-adhesive (RelyX Unicem Aplicap) (SA) resin cement. Ten inlays in each subgroup were subjected to 3,500 thermal cycles and 24,000 loading cycles, while the other 10 served as control. Horizontal 3 mm thick specimens were cut out of the restored teeth for push out bond strength testing. Bond strength data were statistically analyzed using 1-way ANOVA and Tukey's comparisons at ${\alpha}=.05$. The mode of ceramic-cement-dentin bond failure for each specimen was also assessed. RESULTS. No statistically significant differences were noticed between FP and ZR bond strength to dentin in all subgroups (ANOVA, P=.05113). No differences were noticed between EB and SA (Tukey's, P>.05) bonded to either type of ceramics. Both adhesive and mixed modes of bond failure were dominant for non-aged inlays. Simulated aging had no significant effect on bond strength values (Tukey's, P>.05) of all ceramic-cement combinations although the adhesive mode of bond failure became more common (60-80%) in aged inlays. CONCLUSION. The suggested cement-ceramic combinations offer comparable bonding performance to dentin substrate either before or after simulated aging that seems to have no adverse effect on the achieved bond.

• Korea-Australia Rheology Journal
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• 제13권4호
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• pp.205-217
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• 2001

This review article summarizes results of recent viscoelastic and dielectric studies for entangled cis-polyisoprene (PI) chains. The PI chains have the so-called type-A dipoles parallel along the chain backbone, and their slow viscoelastic and dielectric relaxation processes reflect the same global chain motion. However, this motion is differently averaged in the viscoelastic and dielectric properties, the former representing the isochronal orientational anisotropy of individual entanglement segments while the latter detecting the orientational correlation of the segments at two separate times (0 and t). On the basis of this difference, the viscoelastic and dielectric data of the entangled PI chains were compared to elucidate detailed features of the chain dynamics. Specifically, the molecular picture of dynamic tube dilation (DTD) incorporated in recent models was tested for linear and star PI chain. The comparison revealed that the DTD picture was valid for linear PI chains but failed for the star PI chains in the dominant part of the terminal relaxation. The failure for the star chains was related to the pre-requisite for the DTD process, rapid equilibration of successive entanglement segments through their constraint release (CR) motion: For the star chains, the dilated tube diameter expected in the terminal regime was considerably large because of a broad distribution of motional modes of the chains, so that the CR-equilibration required for DTD could not occur in time. The terminal relaxation of the star chain appeared to occur through the CR process before the expected DTD process was completed. The situation was different for the linear chain exhibiting narrowly distributed motional modes. The dilated tube expected for the linear chain was rather thin and the required CR-equilibration occurred in time, resulting in the success of the DTD picture. These detailed features of the chain dynamics was revealed only when the viscoelastic and dielectric properties were compared, demonstrating the importance of this comparison.

• 대한기계학회논문집A
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• 제30권6호
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• pp.653-661
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• 2006

Metallic sandwich plates with various inner cores have important new features with not only ultra-light material characteristics and load bearing function but also multifunctional characteristics. Because of production possibility on the large scale and a good geometric precision, sandwich plates with inner dimpled shell structure from a single material have advantages as compared with other solid sandwich plates. Inner dimpled shell structures can be fabricated with press or roll forming process, and then bonded with two face sheets by multi-point resistance welding or adhesive bonding. Elasto-plastic bending behavior of sandwich plates have been predicted analytically and measured. The measurements have shown that elastic perfectly plastic approximation can be conveniently employed with less than 10% error in elastic stiffness, collapse load, and energy absorption. The dominant collapse modes are face buckling and bonding failure after yielding. Sandwich plates with inner dimpled shell structure can absorb more energy than other types of sandwich plates during the bending behavior.

• Steel and Composite Structures
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• 제34권6호
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• pp.803-818
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• 2020

Semi-rigid connections with blind bolts could solve the difficulty that traditional high strength bolts were unavailable to splice a steel/composite beam to a closed section column. However, insufficient investigations have focused on the performance of semi-rigid connection to square concrete filled double-skin steel tubular (CFDST) columns. In this paper, a component model was developed to evaluate the mechanical behavior of semi-rigid composite connections to CFDST columns considering the stiffness and strength of column face in compression and column web in shear which were determined by the load transfer mechanism and superstition method. Then, experimental investigations on blind bolted composite joints to square CFDST columns were conducted to validate the accuracy of the component model. Dominant failure modes of the connections were analyzed and this type of joint behaved semi-rigid manner. More importantly, strain responses of CFDST column web and tubes verified that stiffness and strength of column face in compression and column web in shear significantly affected the connection mechanical behavior owing to the hollow part of the cross-section for CFDST column. The experimental and analytical results showed that the CFDST column to steel-concrete composite beam semi-rigid joints could be employed for the assembled structures in high intensity seismic regions.

• Composites Research
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• 제18권1호
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• pp.30-37
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• 2005

본 연구에서는 3점 굽힘 실험과 코어의 실제 형상을 모델링한 유한요소 시뮬레이션을 병행하여 외피층의 항복, 층간분리 코어의 전단 및 국부적 좌굴과 같은 다양한 파손모드를 고려한 하니컴 샌드위치 복합재료의 강도 특성과 변형거동을 검토하였다. 외피층과 하니컴 코어층 사이를 완전 접착한 시험편과 부분 층간분리 시험편을 대상으로 하니컴 코어의 셀 크기와 외피층 두께를 변화시켜 시험편의 굽힘 강성, 굽힘 강도. 굽힘 응력, 변형 및 파손 거동을 해석하였다. 결론적으로 하니컴 코어의 셀 크기와 외피층의 두께가 하니컴 샌드위치 복합재료의 굽힘 강성과 강도, 변형/파괴 거동에 주된 영향을 미쳤으며 코어의 셀 크기가 크고 외피층의 두께가 얇은 경우 굽힘 강도는 $30\~68\%$ 정도까지 저하됨을 알 수 있었다.

• Steel and Composite Structures
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• 제31권1호
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• pp.99-112
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• 2019

Semi-rigid joints have been widely studied in literature in recent decades because they affect greatly the structural response of frames. In literature, the behavior of semi-rigid joints is commonly assumed to be identical under positive and negative moments which are obviously incorrect in many cases where joint details such as bolt arrangement or placement of haunch are vertically asymmetrical. This paper evaluates two common types of steel frames with asymmetrical beam-to-column joints by Direct Analysis allowing for plasticity. A refined design method of steel frames using a proposed simple forth order curved-quartic element with an integrated joint model allowing for asymmetrical geometric joint properties is presented. Furthermore, the ultimate behavior of six types of asymmetrical end-plate connections under positive and negative moment is examined by the Finite Element Method (FEM). The FEM results are further applied to the proposed design method with the curved-quartic element for Direct Analysis of two types of steel frames under dominant gravity or wind load. The ultimate frame behavior under the two different scenarios are examined with respect to their failure modes and considerably different structural performances of the frames were observed when compared with the identical frames designed with the traditional method where symmetrical joints characteristics were assumed. The finding of this research contributes to the design of steel frames as their asymmetrical beam-to-column joints lead to different frame behavior when under positive and negative moment and this aspect should be incorporated in the design and analysis of steel frames. This consideration of asymmetrical joint behavior is recommended to be highlighted in future design codes.