• Journal of Hydrogen and New Energy
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• v.26 no.2
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• pp.114-119
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• 2015

Nowdays, fossil fuels have been used as an important resource in development of industry. But it is limited and caused climate change such as pollution and global warming. So nuclear fusion research is being issued with tritium to develop eco-friendly and sustainable energy. Republic of Korea is in charge of Storage and Delivery System (SDS) in the International Thermonuclear Experimental Reactor (ITER), weld present in the SDS bottles are easily exposed to the hydrogen embrittlement of special characteristics of the hydrogen in hydrogen atmosphere, When the hydrogen embrittlement is rapidly progresses, the cracking is generated in the weld zone. Due to this cracking, the risk of leakage of tritium into the atmosphere occurs. In this study, hydrogen heat treatment was processed through the Pressure-Composition-Temperature (PCT) device according to the time variation. Also mechanical properties such as rupture strength test, three point bend test and hardness test in accordance with the respective time have been conducted and the fracture was observed by scanning electron microscopy(SEM) after the mechanical properties evaluation.

• Archives of Pharmacal Research
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• v.22 no.3
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• pp.288-293
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• 1999

Postabsorptive serum iron level was determined after oral administration of the compounds to human. In serum and whole blood, $Fe^{3+}$ was measured by ion chromatography (IC) using a pyridine-2,6-dicarboxylic acid (PDCA) as an eluent. The serum sample solutions were pretreated with I N HCI and 50% TCA. The whole blood sample solutions were treated with 3 N HCI for 30 min at $125^{\circ}C$. The limit of detection (LOD) of the IC technique is $0.2 {\mu}M$ for$Fe^{2+}$and 0.1 $\mu$M for $Fe^{3+}$. The area under concentration (AUC) can be obtained by the above analytical condition. In addition, to compare the stability of $Fe^{2+}$ to that of $Fe^{3+}$ in pharamaceutical preparations, accelerated stability test was carried out. After storing the samples under $40^{\circ}C$, 75%RH in light-resistant container for various time intervals, the contents of iron of different valencies were determined separately by the IC technique and the change and/or the interchange of among those iron species in preparations was investigated. Iron raw materials are stable, but $Fe^{2+}$ in$Fe^{3+}$ source materials was slightly converted to $Fe^{3+}$ by oxidation. $Fe^{2+}$ in$Fe^{3+}$ source raw materials and $Fe^{3+}$ in $Fe^{2+}$ raw materials are determined as impurities. Therefore, IC technique is found to be an appropriate method for comparative evaluation of dissimilar bioavailability of $Fe^{2+}$ and $Fe^{3+}$, stability of $Fe^{2+}$ and $Fe^{3+}$ raw materials and preparations.

• Journal of Welding and Joining
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• v.35 no.1
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• pp.26-33
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• 2017

This study aims to investigate the suitability of requirement for post-weld heat treatment(PWHT) temperature when different P-No. materials are welded, which is defined by ASME Sec. III Code. For SA-516 Gr. 60 and SA-106 Gr. B carbon steels that are typical P-No. 1 material, simulated heat treatment were conducted for 8 h at $610^{\circ}C$, $650^{\circ}C$, $690^{\circ}C$, and $730^{\circ}C$, last two temperature falls in the temperature of PWHT for P-No. 5A low-alloy steels. Tensile and Charpy impact tests were performed for the heat-treated specimens, and then microstructure was analyzed by optical microscopy and scanning electron microscopy with energy-dispersive spectrometry. The Charpy impact properties deteriorated significantly mainly due to a large amount of cementite precipitation when the temperature of simulated heat treatment was $730^{\circ}C$. Therefore, when dissimilar metal welding is carried out for P-No. 1 carbon steel and different P-No. low alloy steel, the PWHT temperature should be carefully selected to avoid significant deterioration of impact properties for P-No. 1 carbon steel.

• Transactions of Materials Processing
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• v.29 no.1
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• pp.11-19
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• 2020

For microstructural analysis of a friction stir welded (FSWed) joint of advanced high-strength steels, dual phase (DP) and complex phase (CP) steels, are studied. FSWed joints are successfully fabricated in the following four cases: (i) DP/DP; (ii) CP/CP; (iii) DP/CP, where the advancing side is DP and the retreating side is CP; (iv) CP/DP, where the advancing side is CP and the retreating side is DP. The stir zone (SZ) of (i) the DP/DP joint mainly consists of lath martensite, while the stir zone of (ii) the CP/CP joint consists not only of lath martensite but also of bainite. In the case of (iii) DP/CP and (iv) CP/DP, they exhibit a similar microstructure including acicular-shaped phases in the joints; however, cross-sections of the joints show differences in material mixing in each case. In (iv) the CP/DP joint, temperature towards the CP steel is sufficient to cause softening, thus leading to better mixing than that in (iii) DP/CP. The phases of the SZ in each of the four cases are formed by phase transformation during the FSWed process; however, the transformed phase volume fraction of CP steel is lower than that of DP steel, indicating that dynamic recrystallization occurs mainly in CP steel. The hardness values of the SZ are significantly higher than those of the base materials, especially, the SZ of (iii) the DP/CP joint has the highest value due to highest fraction of lath martensite.

• Journal of the Korean Society of Safety
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• v.28 no.4
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• pp.14-18
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• 2013

Blades of horizontal axis are nowadays made of composite materials. Generally, composite materials satisfy design provides lower weight and good stiffness, while laminate composites have often damages as like the delamination and cracks at the interface of laminates. The box spar and tail parts of a blade are composed of the CFRP/GFRP hybrid laminate composites. However, delamination and the interfacial crack often occur in the interface of CFRP/GFRP hybrid laminate composites under the mixed mode fracture condition, especially mode I and mode II. Therefore, there is a need for the evaluation of the mixed mode fracture behavior during the delamination of CFRP/GFRP hybrid laminates. This study shows the experimental results for the delamination fracture toughness in CFRP/GFRP hybrid laminate composites. Fracture toughness experiments and estimation are performed by using DMMB(Dissimilar mixed mode bending) specimen. The materials used in the test are a commercial woven type CFRP(Carbon fiber reinforced plastic) prepreg(CF3327) and UD type GFRP(Glass fiber reinforced plastic) prepreg(HD224A). A CFRP/GFRP hybrid laminate composite is composed by the 10 plies CFRP and GFRP prepreg for DMMB. A thickness of CFRP and GFRP layer is 2.5mm and 3.0mm, respectively. Also the fulcrum location which is a loading parameter is changed from 80 to 100mm on the specimen of length 120mm because it defines the ratio of mode I to mode II. In this study, the effects of the fulcrum location are evaluated in the viewpoint of energy release rate in mode I and mode II contribution. The results show that the delamination crack initiates at higher displacement and lower load according to the increase of the fulcrum location ratio. And the variation of the energy release rate for mode I and II contributions for the mode mixity are shown.

• Journal of Welding and Joining
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• v.27 no.4
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• pp.54-59
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• 2009

In the process to manufacture for metallic structures, control of welding deformation is one of an important problems connected with reliability of the manufactured structures so that welding deformation should be measured and controlled with quickly and actively. Also, welding parameters which have as lot of effects on welding deformation such as arc voltage, welding current and welding speed can also be controlled. The objectives for this study were to develop a simple 2-D FEM to calculate not only the transient thermal histories but also the sizes of fusion and heat-affected zone (HAZ) in multi pass arc welds including the butt and fillet weld type with dissimilar thickness, and to concentrate on a developed model for the finding the parameters of Godak's moving heat source model based on a GA. The developed model includes a GA program using MATLB and GA toolbox, and a batch mode thermal model using ANSYS software. Not only the thermal model was verified by comparison with Goldak's work but also the developed model was validated with molten zone section experimental data.

• Advances in materials Research
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• v.8 no.1
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• pp.47-73
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• 2019

Joining of Mg/Ti hybrid structures by welding for automotive and aerospace applications has attracted great attention in recent years due mainly to its potential benefit of energy saving and emission reduction. However, joining them has been hampered with many difficulties due to their physical and metallurgical incompatibilities. Different joining processes have been employed to join Mg/Ti, and in most cases in order to get a metallurgical bonding between them was the use of an intermediate element at the interface or mutual diffusion of alloying elements from the base materials. The formation of a reaction product (in the form of solid solution or intermetallic compound) along the interface between the Mg and Ti is responsible for formation of a metallurgical bond. However, the interfacial bonding achieved and the joints performance depend significantly on the newly formed reaction product(s). Thus, a thorough understanding of the interaction between the selected intermediate elements with the base metals along with the influence of the associated welding parameters are essential. This review is timely as it presents on the current paradigm and progress in welding and joining of Mg/Ti alloys. The factors governing the welding of several important techniques are deliberated along with their joining mechanisms. Some opportunities to improve the welding of Mg/Ti for different welding techniques are also identified.

• International Journal of Naval Architecture and Ocean Engineering
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• v.2 no.1
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• pp.45-56
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• 2010

Polymer composite materials offer high strength and stiffness to weight ratio, corrosion resistance, and total life cost reductions that appeal to the marine industry. The advantages of composite construction have led to their incorporation in U.S. yacht hull structures over 46 meters (150 feet) in length. In order to construct even larger hull structures, higher quality composites with lower cost production techniques need to be developed. In this study, the effect of composite hull fabrication processes on mechanical properties of glass fiber reinforced plastic (GFRP) composites is presented. Fabrication techniques investigated during this study are hand lay-up (HL), vacuum infusion (VI), and hybrid (HL+VI) processes. Mechanical property testing includes: tensile, compressive, and ignition loss sample analysis. Results demonstrate that the vacuum pressure implemented dining composite fabrication has an effect on mechanical properties. The VI processed GFRP yields improved mechanical properties in tension/compression strengths and tensile modulus. The hybrid GFRP composites, however, failed in a sequential manor, due to dissimilar failure modes in the HL and VI processed sides. Fractography analysis was conducted to validate the mechanical property testing results.

• Laser Solutions
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• v.17 no.2
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• pp.11-18
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• 2014

This research was conducted as a fundamental study to apply tailored blank welding technique into automotive production process. Specially we tried to apply the TWB technique to exhaust system. The materials used in this work were ferritic 439 stainless steel sheet with a thickness of 1.2mm and 0.8mm. Welding tests were conducted for BOP test and dissimilar thickness (0.8 to 1.2t) cases. Major process parameters were position of focus, travel speed, shielding gas and joint (gap) condition. As a result, there are nothing significant welding characteristic compare with TWB of carbon steel. Stainless steel shows the good weldability and mechanical properties (tensile, hardness and forming strength) also shows high level. Just problem is gap condition. However, also in this case, it shows not only good forming strength but also base metal fracture after tensile test. And to conclude, it is good opportunity to make lightweight design muffler using TB welding technique.

• Applied Microscopy
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• v.19 no.1
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• pp.59-69
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• 1989

Ultrastructure of the secretory portion of the small ampullate gland in the orb web spider, Nephila clavata, has been investigated using the electron microscope. The secretory portion of this gland comprise two different regions which are a S-shaped storage sac and a long, convoluted tail. By the internal textures of the secretory granules, the sac is subdivided into two regions ; the proximal region near the tail and the distal region near the duct. Commonly single layered connectives cover the basal portion of the sac epithelium, and apical portion of the epithelial cells is occupied by the thick cuticles. Within the epithelial cells of both the proximal and distal region, several types of the secretory granules surrounded by a limiting membrane and had characteristic crystalloid are scattered throughout the cytoplasm. The granular size and its electron densities are not coincide with each other according to the maturation level of the granules. The wall of the tail is composed of single layer of columnar epithelial cells, and their nuclei are found at the basal portion of the cells. Dissimilar to the epithelial cells of the sac, apical cuticles are not found at this portion. In the cytoplasm of these cells, numerous secretory granules, synthesized from the rough endoplasmic reticula commonly and had fine fibrous materials, are found. At the cell surface bordering the lumen, microvilli are seen, arid along the cellular boundaries specialized septate junctions and desmosomes appeared.