• Journal of the Korean Wood Science and Technology
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• v.42 no.5
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• pp.516-522
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• 2014

Old architectural wood materials damaged by a fire were evaluated on the basis of wood species and scanning electron microscopy (SEM) observation of wood tissues in combination with energy dispersive X-ray spectroscopy (EDXS) analysis. Results of SEM observation showed that tracheid wall thickness of burned parts was very thin compared with undamaged and sound wood, and tylosoid in the resin canals disappeared after the exposure to fire. SEM-EDXS analysis indicated that carbon and oxygen peaks occurred in the original energy band, and the carbon peak was higher than that of the oxygen in the burned part. A computerized tomography was also undertaken to investigate the carbonization layer formed by fire and possible internal defects.

• Journal of the Korean Ceramic Society
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• v.48 no.2
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• pp.147-151
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• 2011

In this study, we prepared graphene by using the modified Hummers-Offeman method and then introduced the metals (Pt, Pd and Fe) for dispersion on the surface of the graphene for synthesis of metal-graphene composites. The characterization of the prepared graphene and metal-graphene composites was performed by X-ray diffraction (XRD), scanning electron microscopy (SEM) with energy dispersive X-ray (EDX) analysis and transmission electron microscopy (TEM). According to the results, it can be observed that the prepared graphene consists of thin stacked flakes of shapes having a well-defined multilayered structure at the edge. And the metal particles are dispersed uniformly on the surface of the graphene with an average particle size of 20 nm.

• Journal of the Korean Ceramic Society
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• v.49 no.2
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• pp.155-160
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• 2012

This paper reported a simple deposition-precipitation method, introducing the metal (Ni, Ag and Sn) and $Na_2S{\cdot}5H_2O$ to preparedispersion metal sulfide nanoparticles on the surface of the Multi-walled carbon nanotube for synthesis of CNT-$M_xS_y$ ($NiS_2$, $Ag_2S$, SnS) composite photocatalysts. The characterization of the prepared CNT-$M_xS_y$ ($NiS_2$, $Ag_2S$, SnS) composites was performed by X-ray diffraction, scanning electron microscopy with energy dispersive X-ray analysis and BET analysis. Furthermore, the MB degradation rate constant for CNT-SnS composite was $5.68{\times}10^{-3}$ under visible light irradiation, which was much higher than the corresponding values for other samples. The detailed formation and photocatalytic mechanism are also provided here.

• Journal of the Korean Ceramic Society
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• v.47 no.4
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• pp.269-275
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• 2010

In this study, we successfully prepared CNT/$TiO_2$, Pt/CNT and Pt/CNT/$TiO_2$ composites and investigated their photocatalytic activity in MB solution by irradiation under UV light. Fourier transform infrared (FT-IR) spectroscopy was used to characterize the functional group on the surface of MWCNTs, which oxidized by MCPBA. Brunauer-Emmett-Teller (BET) surface area, transmission electron microscopy (TEM), X-ray diffraction (XRD) and energy dispersive X-ray (EDX) were used to analyze the prepared composites. The results of the decomposition of the MB solution indicated that the Pt/CNT/$TiO_2$ composite had the best photocatalytic activity among the three kinds of composites.

• Journal of Electrochemical Science and Technology
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• v.3 no.1
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• pp.35-43
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• 2012

Highly ordered and perforated anodic aluminum oxide membranes were prepared by anodic oxidation and subsequent removal of the barrier layer. By using these homemade anodic aluminum oxide membranes as templates, metal selenide nanowires and nanotubes were synthesized. The structure and composition of these one-dimensional nanomaterials were studied by field emission scanning electron microscopy as well as transmission electron microscopy and energy dispersive X-ray spectroscopy. The growth process of metal selenide inside anodic aluminum oxide channel was traced by investigating the series of samples using scanning electron microscopy after reacting for different times. Straight and dense copper selenide and silver selenide nanowires with a uniform diameter were successfully prepared. In case of nickel selenide, nanotubes were preferentially formed. Phase and crystallinity of the nanostructured materials were also investigated.

• Journal of the Korean Society of Costume
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• v.58 no.5
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• pp.211-231
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• 2008

To conserve historic textiles, analyses of textile materials, pollutants and deterioration are prerequisite steps. Based upon analytical results, guides for conservation of historic textiles are established. In analyses of textile materials, pollutants and deterioration, there are chemical methods(burning, solubility and staining), physical methods(microscopy and density) and instrumental analysis(Fourier Transform Infrared Spectroscopy (FT-IR), Fourier Transform Raman Spectroscopy(FT-Raman), Gas Chromatography(GC), Mass Spectroscopy(MS), X-Ray Fluorescence (EDXRF, WDXRF), Energy Dispersive Spectroscopy(EDS), and X-Ray Diffraction(XRD), Tensile Testing Machine etc.). Combination of qualitative and quantitative analyses makes accurate diagnosis of textile condition possible. As examples of analyses and conservation of historic textiles, Chuninsan(19 century) similar to sunshade with handing down historic textile and golden decorative skirt(17 century) with excavated costume are taken.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.30 no.3 s.246
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• pp.342-348
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• 2006

A new magnetostrictive patch array transducer for the generation and detection of torsional waves is developed fur the on-line health monitoring of rotating shafts. Even though the torsional wave is useful in nondestructive evaluation due to its non-dispersive property, a transducer generating torsional waves in rotating shafts has not been developed so far. In this research, a torsional wave transducer using the magnetostrictive effect is newly developed. By bonding an away of magnetostrictive rectangular patches on the outer surface of the shaft at an oblique angle of $45^{\circ}$ and encircling the array by a solenoid coil, we have successfully generated and measured torsional waves by the developed transducer. Several experiments were carried out to check the transducer performance.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.3 no.3
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• pp.17-23
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• 2004

The performance and life of a die are influenced by the machining methods. In order to examine the effects of machining methods on surface charactenstics, simple experiments are devised and performed. A die steel STD11, commonly used as a die material in press working, is selected. Three ways of machining methods to manufacture a die are considered. Those are (1) milling and then grinding, (2) wire-cut electric discharge dachining (W-EDM) and (3) heat treatment after W-EDM. The resulting surface roughnesses are measured. Also, the changes of surface microstructures are investigated using the scanning electron microscope(SEM) with energy dispersive X-ray spectrometer(EDS) and the results are discussed in details.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1999.10a
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• pp.393-398
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• 1999

The temperature dependence of the viscosity was determined for an electrorheological(ER) fluid consisting of 35 weight% zeolite particles in hydraulic oil 46cSt. Thermal activation analysis were performed by changing the ER fluid's temperature from -1$0^{\circ}C$ to 5$0^{\circ}C$ at fixed electric field. According to the analysis, the activation energy for flow was about 79.64kJ/mole at E=0kV/mm. Generally, the hydraulic oil 46cSt will be operated at the temperature of about 4$0^{\circ}C$, the ER fluid's electric field dependence of viscosities were investigated at this temperature. also, the influence of adding the dispersant(Carbopl 940) on electrorheological effect of the ER fluid was discussed.

• Journal of Auto-vehicle Safety Association
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• v.7 no.2
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• pp.39-43
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• 2015

NDIR (Non-dispersive infrared Rays) alcohol sensor has been prototyped and its temperature characteristics were measured. In order to design novel optical alcohol sensor, elliptical structures with one common foci were modeled and analyzed their optical properties. After analyzing elliptic optical structures, a prototype alcohol sensor module was tested according to the temperature variations from $-20^{\circ}C$ to $35^{\circ}C$. The offset voltages of alcohol sensor decreased from 1.1056 V at the temperature $-20^{\circ}C$ to 0.7339 V at $35^{\circ}C$. However, the highest sensitivity of alcohol sensor showed about $303{\mu}V/ppm$ at room temperature.