• 한국전자현미경학회:학술대회논문집
• /
• 2004.05a
• /
• pp.74-77
• /
• 2004

• 한국전자현미경학회:학술대회논문집
• /
• 1993.06a
• /
• pp.33-33
• /
• 1993

• Journal of the Korean Ceramic Society
• /
• v.40 no.6
• /
• pp.513-518
• /
• 2003

La/sub 2/3-x/Li/sub 3x/□/sub 1/3-2x/TiO₃ compounds with x=0.13 and 0.12 were prepared by slow cooling (x=0.13) and rapid quenching (x=0.12) into the liquid nitrogen after sintering at 1350℃ for 6 h. Their crystal structure has been determined by Rietveld refinement of both the powder neutron and X-ray diffraction data. From neutron diffraction data, we found that the main phase was not tetragonal (P4/mmm), but trigonal (R3cH). The refinement of neutron diffraction for the slow cooled samples were in a good agreement with a new model; a mixture of trigonal (R3cH, 45.7 wt％), tetragonal (p4/mmm, 37.0 wt％), and Li/sub 0.57/Ti/sub 0.86/O₂(pbnm, 17.2 wt%), but the quenched sample was found not to contain tetragonal (p4/mmm). X-ray diffraction data couldn't be well fitted because of the Poor scattering factor of lithium ions and the similar reflection patterns among trigonal (R3cH), tetragonal (p4/mmm), and cubic (Pm3m). We also knew that one transport bottlenecks is destroyed by one La vacancy in the case of trigonal (R3cH).

• Carbon letters
• /
• v.16 no.3
• /
• pp.215-218
• /
• 2015

Carbon micro particles with dimple patterns were produced by electro-spraying a solution of pitch in tetrahydrofuran. Particle formation depended on separation in an electrical field and volatilization of the solvent. More than 80% of the obtained carbon exhibited an average particle size of less than 50 μm. X-ray diffraction analysis suggests that the carbon with dimple patterns has increased crystallinity after heat treatment.

• Molecules and Cells
• /
• v.43 no.3
• /
• pp.298-303
• /
• 2020

Cryo-electron microscopy (cryo-EM) is now the first choice to determine the high-resolution structures of huge protein complexes. Grids with two-dimensional arrays of holes covered with a carbon film are typically used in cryo-EM. Although semi-automatic plungers are available, notable trial-and-error is still required to obtain a suitable grid specimen. Herein, we introduce a new method to obtain thin ice specimens using real-time measurement of the liquid amounts in cryo-EM grids. The grids for cryo-EM strongly diffracted laser light, and the diffraction intensity of each spot was measurable in real-time. The measured diffraction patterns represented the states of the liquid in the holes due to the curvature of the liquid around them. Using the diffraction patterns, the optimal time point for freezing the grids for cryo-EM was obtained in real-time. This development will help researchers rapidly determine high-resolution protein structures using the limited resource of cryo-EM instrument access.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.27 no.5
• /
• pp.223-228
• /
• 2017

Aluminum nitride (AlN) powder was successfully synthesized at low temperature via carbothermal reduction and nitridation (CRN) assisted by microwave heating. The synthesis processes of AlN powder were investigated with X-ray diffraction, FE-SEM, FT-IR and TGA/DSC. Aluminum nitrate was used as an oxidizer and aluminum source, urea as fuel, and glucose as carbon source. These starting materials were mixed with D.I water and reacted in a flask at $100^{\circ}C$ for 20 minutes. After the reaction was finished, black foamy intermediate product was formed, which was considered to be an amorphous $Al_2O_3$ particles through intermediate product obtained by solution combustion synthesis (SCS) at the results of X-ray diffraction patterns and FT-IR. This intermediate product was nitridated at temperatures of $1300^{\circ}C$ and $1400^{\circ}C$ in $N_2$ atmosphere by a microwave heating furnace and then decarbonated at $600^{\circ}C$ for 2 hours in air. It should be noticed from FE-SEM images that as nitridated particles, identified as AlN from X-ray diffraction patterns, are covered with carbon residues. After decarbonating the nitridated powders, the spherical pure AlN powders were obtained without alumina and their particle sizes were dependent on the nitridating temperature with high temperature of $1400^{\circ}C$ giving large particles of around 70~100 nm.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.21 no.6
• /
• pp.672-676
• /
• 1992

Retrogradation properties of cowpea and mung bean starch gels were investigated by rate of retrogradation, X-ray diffraction patterna and syneresis of gels. Retrogradation time constant of mung bean starch gel(30%) by Avrami equation had a similar value to that of cowpea starch gel. X-ray diffraction patterns of the two retrograded starch gels(10%) were B-type. The extent of retrogradation determined by syneresis showed that cowpea starch gel was a little larger than that of mung bean starch gel(6~10%).

• The Journal of Korean Institute of Communications and Information Sciences
• /
• v.16 no.10
• /
• pp.934-940
• /
• 1991

A modified quantizing method is introduced to teach single layer learning algorithm, which is implemented optically. The proposed optical system consists of input masks, holographic diffraction grating. LCD and CCD camera. The 2 dimensional interconnections between input neurons and output neurons are realized using holographic phase grating, which is fabricated for equal intensity distribution of diffraction orders. The two gray levels of LCD act as binary weights for each interconnection. The weights are compensated according to the learning algorithm in which the amount of weights to be compensated is determined by comparing the output patterns with target patterns. The learning process is iterated until the predetermined conditions are satisfied. Optical experiments are performed for two learning rates, 0.5 and 0.9 and the experimental results show that the proposed system is useful for optical neural networks.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.27 no.12
• /
• pp.797-802
• /
• 2014

In this study, in order to develop the capacitor composition ceramics with the good dielectric properties, $(Ba_{1-x}Ca_x)(Ti_{0.85}Zr_{0.12}Sn_{0.03})O_3$ (abbreviated as BCTZ) ceramics were prepared by the conventional solid-state reaction method. The effects of Ca substitution on the microstructure and dielectric properties was investigated. The X-ray diffraction patterns demonstrated that all the specimens showed perovskite phase, and secondary phases are indicated in the measurement range of X-ray diffraction. Also, all the specimens indicated an rhombohedron phase structure. It was identified from the X-ray diffraction patterns that the secondary phase formed in grain boundaries and then decreased the dielectric properties. For all the specimens, observed one peak was tetragonal cubic phase transition temperature($T_c$), which is located in the vicinity of room temperature.

• Current Optics and Photonics
• /
• v.2 no.2
• /
• pp.140-146
• /
• 2018

In this paper, mesoscale optical surface structures are found to possess both geometric and wave optics features. The study reveals that geometric optic analysis cannot correctly predict the experimental results of light transmission or reflection by mesoscale optical structures, and that, for reliable analyses, a hybrid approach incorporating both geometric and wave optic theories should be employed. By analyzing the transmission patterns generated by the mesoscale periodic pyramid prism plates, we show that the wave optic feature is mainly ascribed to the edge diffraction effect and we estimate the relative contributions of the wave optic diffraction effect and the geometric refraction effect to the total scattering field distribution with respect to the relative dimension of the structures.