• 제목/요약/키워드: densification

검색결과 1,022건 처리시간 0.021초

흔합 및 합금고속도강 소결체의 치밀화에 미치는 구성성분의 역할 (Role of Alloyed Components on Densification of Mixed and Prealloyed High Speed Steel Powder Compacts)

  • 임태환
    • 한국분말재료학회지
    • /
    • 제1권2호
    • /
    • pp.153-158
    • /
    • 1994
  • The effect of the role of alloyed components on the densification of two kind of high speed steel (mixed and prealloyed powder), which were sintered at 1403~ 1573 K for 7.2 ks in vacuum, was investigated. The results obtained were as follows. (1) Without the presence of Vanadium (V), the relative density of sintered compacts (Ds) could not reached the density of 100% regardless of the. elements in the compacts. (2) The addition of V up to 2 mass% did not result In the complete densification when the carbon content was fixed at 2% in the compact. (3) With the fixed amount of V of 7%, Ds decreased with the increase of the carbon content. (4) The addition of mixed fine powder to the prealloyed powder in the range of 20 to 40% provided the complete densification and carbide panicles of 1~2 $\mu\textrm{m}$ through the solid phase sintering. (5) The V element played important role in controlling the complete or incomplete densification of the sintered compacts in the alloyed component because of its formation of stable oxide and carbide as well as the low equilibrium pressure of CO gas.

  • PDF

압전변압기용 $Pb(Mn_{1/3}Sb_{2/3})O_3-PZT$ 세라믹스에서 승온속도 및 $V_2O_5$ 첨가가 치밀화 및 전기적 특성에 미치는 영향 (Effect of Heating Rate and $V_2O_5$ Addition on Densification and Electrical Properties of $Pb(Mn_{1/3}Sb_{2/3})O_3-PZT$ Ceramics for Piezoelectirc Transformer)

  • 허수정;손준호;손정호;이준형;김정주;정우환;박명식;조상희
    • 한국세라믹학회지
    • /
    • 제37권4호
    • /
    • pp.295-301
    • /
    • 2000
  • The effect of V2O5 addition on the low temperature sintering of Pb(Mn1/3Sb2/3)O3-PZT ceramics, which is known as a prominent material for piezoelectric transformer application was studied, and the densification behavior and piezoelectric characteristics of the samples as a function of heating rate were also examined. V2O5 led the system to liquid phase sintering by forming liquid phase during sintering, which accelerated densification through the particle rearrangement in the early stage of sintering. The liquid phase mostly existed at grain boundaries retarded the evaporation of PbO, while the densification temperature and the weight loss of V2O5-free samples were higher than those of samples with V2O5. Faster heating improved the densification of the samples regardless of V2O5 addition. The low temperature sintering at 100$0^{\circ}C$ was achieved in PMS-PZT ceramics with high density and reasonable dielectric and piezoelectric characteristics. This result revealed optimistic way to the development of multi-layered piezoelectric transformers.

  • PDF

침엽수단판의 수지함침처리에 의한 압밀화 특성 (Densification Characteristics of Softwood Veneers Treated by Resin Impregnation)

  • 서진석
    • 한국가구학회지
    • /
    • 제14권2호
    • /
    • pp.21-29
    • /
    • 2003
  • This study was carried out to investigate characteristics of plywood overlaid with softwood veneers densified by resin impregnation and compression. The resin impregnability of Korean pine veneer under atmospheric pressure soaking was greater than that of larch, and impregnability of melamine resin was slightly greater than phenolic resin. It was suggested that resin impregnation ratio was affected by density and thickness of veneer. The largest melamine resin impregnation ratio of 50.7% was obtained with 1.26mm thick Korean pine veneer, and the lowest phenolic resin impregnation ratio of 11.7% with 3.41mm thick larch veneer. Therefore, it was suggested that the vacuum-pres sure-soak treatment is required at thick larch veneer. In densifying resin-impregnated veneers, densification ratio from 13.4 to 31.2% was obtained by high pressure from 15.6 to $20.8kgf/cm^2$. Impregnation of melamine resin also showed relatively greater at densification than that of phenolic resin. So it showed the degree of densification of about 20% or greater. It was seemed that adhesive bonding strength of plywood(base panel) which was directly pressed and overlaid with resin-impregnated veneer was affected by resin tackiness after resin impregnation followed by semi-drying. In laboratory scale, melamine resin impregnation was more favorable for the development of adhesive bonding strength owing to moisture control.

  • PDF

알루미나 분말 성형체의 고온 치밀화 성형 공정 해석을 위한 모델 (Model for High Temperature Densification)

  • 권영삼;김기태
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 1994년도 춘계학술대회 논문집
    • /
    • pp.159-166
    • /
    • 1994
  • A constitutive model was proposed to analyze creep densification and grain growth of alumina powder compacts during high temperature processing. Theoretical results from the constitutive model were compared with various experimental data of alumina powder compacts in the literature including pressureless sintering, sinter forging and hot pressing. The proposed constitutive equations were implemented into finite element analysis program (ABAQUS) to simulate densification for more complicated geometry and loading conditions. High temperature forming processing of alumina compact with complicated shape was simulated. Processing of Alumina Powder Compacts

  • PDF

알루미나-활석계에서 알루미나의 입자 크기가 테이프 케스팅 및 소결 거동에 미치는 영향 (Effects of Particle Size of Alumina on the Behaviors of Tape Casting and Sintering of Alumina-Talc System)

  • 윤원균;김호양;이정아;김정주
    • 한국세라믹학회지
    • /
    • 제34권12호
    • /
    • pp.1213-1220
    • /
    • 1997
  • Effect of particle size of alumina and amount of talc on tape casting and densification behaviors of alumina-talc system were investigated. The pseudoplastic behaviors of slurries increased with increase in amount of talc addition and decrease in alumina particle size. In case of using coarse alumina powder, densification of specimens were accelerated with increase of sintering temperature and amount of talc addition. On the contrary, fine alumina powder retarded of rearrangement of alumina particle during liquid phase sintering due to premature densification of alumina matrix region before formation of liquid phase and then densification of specimens were suppressed with increase of sintering temperature and amount of talc addition.

  • PDF

파랑작용에 의한 모래지반의 액상화에 관한 대형 수리모형실험 (Large-Scale Experiments on the Wave-Induced Liquefaction of Sandbed)

  • 강윤구;스즈끼고지로
    • 한국해양공학회지
    • /
    • 제21권3호
    • /
    • pp.26-32
    • /
    • 2007
  • A series of large-scale experiments were carried out in order to examine wave-induced liquefaction in a loosely packed sandbed, its afterward high densification and liquefaction by oscillatory pore pressure. The experiments were conducted in a Large Hydro-Geo Flume that can nearly solve the problems of scale effects of the sandbed, and the 50% sieve diameter of sand was 0.2 mm. The generation of residual pore pressure and its afterward high densification which had observed by Takahashi et al. (1999) in a wave flume experiment using fine sand with the size of 0.08 mm. As a result, the relative density of the sandbed after high densification was increased up to 79% and liquefaction by oscillatory pore pressure was not observed.

등통로각압축이 결합된 압출 공정에 의한 알루미늄 분말의 치밀화 거동 (Analysis of Aluminum Powder Densification by Continuous Front Extrusion-Equal Channel Angular Pressing)

  • 윤승채;김형섭
    • 한국분말재료학회지
    • /
    • 제15권3호
    • /
    • pp.204-209
    • /
    • 2008
  • Aluminum alloys are not only lightweight materials, but also have excellent thermal conductivity, electrical conductivity and workability, hence, they are widely used in industry. It is important to control and enhance the densification behavior of metal powders of aluminum. Investigation on the extrusion processing combined with equal channel angular pressing for densification of aluminum powders was performed in order to develop a continuous production process. The continuous processing achieved high effective strain and full relative density at $200^{\circ}C$. Optimum processing conditions were suggested for good mechanical properties. The results of this simulation helped to understand the distribution of relative density and effective strain.

비정질/다이아몬드 복합재료에서 상분율과 비정질-다이아몬드 입자 크기 비가 성형특성에 미치는 영향 (Effects of Phase Fraction and Metallic Glass-Diamond Size Ratio on the Densification of Metallic Glass/Diamond Composite)

  • 신수민;김택수;강승구;김정곤
    • 한국분말재료학회지
    • /
    • 제16권3호
    • /
    • pp.173-179
    • /
    • 2009
  • In the present study, Zr-base metallic glass(MG)/diamond composites are fabricated using a combination of gas-atomization and spark plasma sintering (SPS). The densification behaviors of mixtures of soft MG and hard diamond powders during consolidation process are investigated. The influence of mixture characteristics on the densification is discussed and several mechanism explaining the influence of diamond particles on consolidation behaviour are proposed. The experimental results show that consolidation is enhanced with increasing diamond/Metallic Glass(MG) size ratio, while the diamond fraction is fixed.

확산과 Power- law 크립을 고려한 압분체 열간정수압압축 공정의 해석 (Analysis of Hot Isostatic Pressing of Powder Compacts Considering Diffusion and Power-Law Creep)

  • 서민홍;김형섭
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 2000년도 추계학술대회 논문집
    • /
    • pp.66-69
    • /
    • 2000
  • In order to analyze the densification behaviour of stainless steel powder compacts during hot isostatic pressing (HIP) at elevated temperatures, a power-law creep constitutive model based on the plastic deformation theory for porous materials was applied to the densification. Various densification mechanisms including interparticle boundary diffusion, grain boundary diffusion and lattice diffusion mechanisms were incorporated in the constitutive model, as well. The power-law creep model in conjunction with various diffusion models was applied to the HIP process of 316L stainless steel powder compacts under 50 and 100 MPa at 1125 $!`\acute{\dot{E}}$. The results of the calculations were verified using literature data It could be found that the contribution of the diffusional mechanisms is not significant under the current process conditions.

  • PDF

The Effect of Pressure on the Properties of Carbon/Carbon Composites during the Carbonization Process

  • Joo, Hyeok-Jong;Oh, In-Hwan
    • Carbon letters
    • /
    • 제3권2호
    • /
    • pp.85-92
    • /
    • 2002
  • 4D carbon fiber preforms were manufactured by weaving method and their carbon fiber volume fractions were 50% and 60%. In order to form carbon matrix on the preform, coal tar pitch was used for matrix precursor and high density carbon/carbon composites were obtained by high densification process. In this process, manufacture of high density composites was more effective according to pressure increasement. When densificating the preform of 60% fiber volume fraction with 900 bar, density of the composites reached at 1.90 $g/cm^3$ after three times processing. Degree of pressure in the densification process controls macro pore but it can not affect micro pore. During the carbonization process, micro pore of the preform were filled fully by once or twice densification processing. But micro pore were not filled easily in the repeating process. Therefore, over three times densification processing is the filling micro pore.

  • PDF