• Korean Journal of Materials Research
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• v.26 no.7
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• pp.353-358
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• 2016

The hydrogen embrittlement of two austenitic high-manganese steels was investigated using tensile testing under high-pressure gaseous hydrogen. The test results were compared with those of different kinds of austenitic alloys containing Ni, Mn, and N in terms of stress and ductility. It was found that the ultimate tensile stress and ductility were more remarkably decreased under high-pressure gaseous hydrogen than under high-pressure gaseous argon, unlike the yield stress. In the specimens tested under high-pressure gaseous hydrogen, transgranular fractures were usually observed together with intergranular cracking near the fracture surface, whereas in those samples tested under high-pressure gaseous argon, ductile fractures mostly occurred. The austenitic high-manganese steels showed a relatively lower resistance to hydrogen embrittlement than did those with larger amounts of Ni because the formation of deformation twins or microbands in austenitic high-manganese steels probably promoted planar slip, which is associated with localized deformation due to gaseous hydrogen.

• Nuclear Engineering and Technology
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• v.53 no.7
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• pp.2304-2311
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• 2021

The dislocation density in strain-hardened Alloy 690 was analyzed using scanning transmission electron microscopy (STEM) to study the relationship between the local plastic strain and susceptibility to primary water stress corrosion cracking (PWSCC) in nuclear power plants. The test material was cold-rolled at various thickness reduction ratios from 10% to 40% to simulate the strain-hardening condition of plant components. The dislocation densities were measured at grain boundaries (GB) and in grain interiors of strain-hardened specimens from STEM images. The dislocation density in the grain interior monotonically increased as the strain-hardening proceeded, while the dislocation density at the GB increased with strain-hardening up to 20% but slightly decreases upon further deformation to 40%. The decreased dislocation density at the GB was attributed to the formation of deformation twins. After the PWSCC growth test of strain-hardened Alloy 690, the fraction of intergranular (IG) fracture was obtained from fractography. In contrast to the change in the dislocation density with strain-hardening, the fraction of IG fracture increased remarkably when strain-hardened over 20%. From the results, it was suggested that the PWSCC growth behavior of strain-hardened Alloy 690 not only depends on the dislocation density, but also on the microstructural defects at the GB.

• Korean Journal of Materials Research
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• v.18 no.7
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• pp.394-399
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• 2008

The hydrogen embrittlement susceptibility of high strength TRIP/TWIP steels with the tensile strength of 600Mpa to 900Mpa grade was investigated using cathodically hydrogen charged specimens. TWIP steels with full austenite structure show a lower hydrogen content than do TRIP steels. The uniform distribution of strong traps throughout the matrix in the form of austenite is considered beneficial to reduce the hydrogen embrittlement susceptibility of TWIP steels. Moreover, an austenite structure with very fine deformation twins formed during straining could also improve the ductility and reduce notch sensitivity. In Ubend and deep drawing cup tests, TWIP steels show a good resistance to hydrogen embrittlement compared with TRIP steels.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1995.03a
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• pp.90-106
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• 1995

The "O"S' BONDING make metallic and non-metalic crystal structures and form localized superconducting orbitals , which induce electrical conduction , semi-conduction, and superconduction. The orbitals are proced by Ampere's law, Faraday's law , Meissner effect, highcritical temperature of thecopper oxide layers. abnomal trans-membrane signal in cancer cell and plastic deformations bytwins and dislocations, In the case of alloying metals, the most deterimentla cases of electrical conduction are those of solid solution and intermetalic compound . The highest case for the hardness are also those of solid solution and intermetallic compound. It explains the contributions of the "O"S' BONDING for conduction bands and plastic deformation by twins and dislocations.ns and dislocations.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.393-396
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• 2009

The mechanical properties, press formability and texture of a TWIP steel were investigated. This steel combines both high strength and high ductility due to so called TWIP effect which are related to the microstructural changes. The formation of twins during deformation leads to an increase of its mechanical properties. In this study, the texture and mechanical properties evolutions of a TWIP steel subjected to tensile tests and press trials at room temperature were investigated in relation to the feasibility of the application to automotive body parts.

• Korean Journal of Metals and Materials
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• v.47 no.11
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• pp.694-698
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• 2009

The $Co_{3}Ti$ phase hardens appreciably by the fine precipitation of disordered fcc Co-rich phase upon aging after quenching from solution annealing temperature. Transmission electron microscope (TEM) observations revealed that the precipitates are platelet in shape, lying nearly parallel to the {100} planes of the $Ll_{2}$-ordered matrix, and perfectly coherent with the matrix lattice at the beginning of aging. The high temperature strength increases appreciably with the fine precipitation of disordered Co-rich phase over the whole temperature range investigated. TEM observations of the under-aged and deformed alloys revealed that superdislocations are pinned by precipitates indicating an attractive interaction between dislocations and precipitates. In the over-aged state, thin twins are introduced in the fcc Co-rich precipitates during deformation.

• Korean Journal of Metals and Materials
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• v.49 no.2
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• pp.112-120
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• 2011

The out-of-phase thermo-mechanical fatigue (OP TMF) in a <001> oriented single crystal nickel-based superalloy CMSX-4 has been studied. OP TMF life was less than a half of low cycle fatigue(LCF) life in spite of a small hysteresis loop area of OP TMF compared to that of LCF. The failure was caused by the initiation of a crack at the oxide-layered surface followed by its planar growth along the <100> ${\gamma}$ channel in both LCF and OP TMF. However, deformation twins appeared near the major crack of OP TMF. The multiple groups of parallel twin plates on {111} planes provided a preferential path for crack propagation, which caused a significant decrease in OP TMF life. Additionally, the analysis on the surface crack morphology revealed that the tensile strain at the minimum temperature of OP TMF was found to accelerate the crack propagation.

• Transactions of Materials Processing
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• v.29 no.3
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• pp.163-171
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• 2020

We present a multi-step cold drawing for a non-equiatomic Co₁₀Cr₁₅Fe₂₅Mn₁₀Ni₃₀V₁₀ high entropy alloy (HEA) with a simple face-centered cubic (FCC) crystal structure. The distribution of strain in the cold-drawn Co₁₀Cr₁₅Fe₂₅Mn₁₀Ni₃₀V₁₀ HEA wires was analyzed by the finite element method (FEM). The effective strain was expected to be higher as it was closer to the surface of the wire. However, the reverse shear strain acted to cause a transition in the shear strain behavior. The critical effective strain at which the shear strain transition behavior is completely shifted was predicted to be 4.75. Severely cold-drawn Co₁₀Cr₁₅Fe₂₅Mn₁₀Ni₃₀V₁₀ HEA wires up to 96% of the maximum cross-sectional reduction ratio were successfully manufactured without breakage. With the assistance of electron back-scattering diffraction and transmission electron microscope analyses, the abundant deformation twins were found in the region of high effective strain, which is a major strengthening mechanism for the cold-drawn Co₁₀Cr₁₅Fe₂₅Mn₁₀Ni₃₀V₁₀ HEA wire.

• Applied Microscopy
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• v.44 no.1
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• pp.34-39
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• 2014

Electron backscatter diffraction (EBSD) is widely used for quantitative microstructural analysis of the crystallographic nature of variety of materials such as metals, minerals, and ceramics. EBSD can provide a wide range of information on materials including grain size, grain orientation, texture, and phase identity. In the case of metallic alloys, EBSD now has become an essential technique to analyze the texture, particularly when severe deformation is applied to the alloys. In addition, EBSD can be one of the very useful tools in identification of twin, particularly in Mg alloys. In Mg alloys different type of twin can occur depending on the c/a ratio and stacking fault energy on the twinning plane. Such an occurrence of different type of twin can be most effectively analyzed using EBSD technique. In this article, the recent development of Mg alloys and occurrence of twin in Mg are reviewed. Then, recently published example for identification of tension and compression twins in AZ31 and ZX31 is introduced to explain how EBSD can be used for identification of twin in Mg.

• Korean Journal of Metals and Materials
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• v.48 no.6
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• pp.498-505
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• 2010

Wrought magnesium alloys show a low formability at room temperature, and a remarkable anisotropy of mechanical properties make it difficult to use them in a deformation process in industry. The microstructure and crystallographic texture of metals are developed during thermo-mechanical processes, and they are significant to the understanding of the mechanical properties of metals. This work studies the microstructure, texture development and tensile properties of the extruded AZ31 Mg alloy after rolling at 100 and $300^{\circ}C$. After 40% rolling at $100^{\circ}C$, many deformed twins were observed and a relatively weak texture developed. The basal poles were split and rotated towards the rolling direction about $20^{\circ}$. During 60% rolling at $300^{\circ}C$, the dynamic recrystallization (DRX) took place and developed a strong <0001>II ND fiber texture, which influenced the poor formability at room temperature.