• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1999년도 춘계학술대회 논문집
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• pp.548-551
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• 1999

The cure characteristics of metal particle filled DGEBA/MDA/SN/ zeolite epoxy resin composite system for EMI shielding were investigated by dynamic DSC run method and FT-lR spectroscopy. As the heating rate increased, the peak temperature on dynamic DSC curve increased because of the rapid cure reaction. From the straight line of the Kissinger plot, the curing reaction activation energy and pre-exponential factor could be obtained. As the post-curing time at 15$0^{\circ}C$ increased, the glass increased the glass transition temperature or the thermal stability increased. When the post curing time is too long, the system filled with metallic Al particle can be thermally oxidized by the catalytic reaction of metal filler and the thermal stability of the composite for the EMI shielding application may be decreased.

• Composites Research
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• 제21권1호
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• pp.16-21
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• 2008

일반적인 아미드형 가교제(HD)를 함유한 에폭시 수지의 가교거동을 캐슈너트 외피유(CNSL) 및 CNSL-포름알데하이드 수지(CFR) 그리고 피마자유 존재 하에서 시차열량계(DSC)를 이용하여 조사하였다. 가교반응에 대한 활성화 에너지를 여러 가지 가열속도에서 비등온 DSC 열량그래프로부터 계산하였다. 피마자유 존재 하에서 에폭시 수지의 가교는 1단계 반응을 나타낸 반면 CNSL 및 CFR 존재 하에서는 2단계 가교거동을 나타내었다. 즉, 에폭시 수지/CNSL(혹은 CFR)/HD 블렌드의 경우 경쟁적인 가교반응이 나타났다. HD가 없는 에폭시 수지/CNSL(혹은 CFR) 블렌드의 경우 CFR 시스템이 CNSL보다 낮은 가교엔탈피 값을 나타내었고, CNSL 및 CFR 함량이 증가할수록 가교활성화 에너지는 증가하였다.

• Journal of the Korean Wood Science and Technology
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• 제34권2호
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• pp.37-45
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• 2006

The viscoelastic properties of blends of melamine-formaldehyde (MF) resin and poly(vinyl acetate) (PVAc) for engineered flooring used on the Korean traditional ONDOL house floor heating system were investigated by dynamic mechanical thermal analysis (DMTA). Because MF resin is a thermosetting adhesive, the effect of MF rein was shown across all thermal behaviors. The addition of PVAc reduced the curing temperature. The DMTA thermogram of MF resin showed that the storage modulus (E') increased as the temperature was further increased as a result of the cross-linking induced by the curing reaction of the resin. The storage modulus (E') of MF resin increased both as a function of increasing temperature and with increasing heating rate. From isothermal DMTA results, peak $T_{tan{\delta}}$ values, maximum value of loss modulus (E") and the rigidities (${\Delta}E$) of MF/PVAc blends at room temperature as a function of open time, peak $T_{tan{\delta}}$ and maximum loss modulus (E") values were found to increase with blend MF content. Moreover, the rigidities of the 70:30 and 50:50 MF/PVAc blends were higher than those of the other blends, especially of 100% PVAc or MF. We concluded that blends the MF/PVAc blend ratios correlate during the adhesion process.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2007년도 춘계학술논문 발표대회
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• pp.1-4
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• 2007

This study investigated the applicability of insulation curing method with double layer bubble sheets to the man concrete subjected to cold weather. Temperature history of the mass concrete indicated that the highest temperature of center section was exhibited at $34^{\circ}C$ while the that of surface section was $25^{\circ}C$. Difference between center and surface was shown to be less $10^{\circ}C$ when the temperature of center section was peak section, and thereby associated temperature cracking index was calculated 1.5, and occurrence probability of temperature cracking was 5%, so there was no temperature cracking caused by internal restraint. No temperature crack was observed by naked eye. It was clear that early frost demage and temperature cracking could be restrained due to reducing temperature difference between inner part and outside in the case double bubble sheets applied to insulation curing method in cold weather. The maturity of mass concrete is higher than outside about $72\sim89^{\circ}$ DD, so it was demonstrated to prevent early frost demage and ensure strength excellently. Insulation curing method with double bubble sheets was more economic than heating curing method.

• 한국건축시공학회지
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• 제3권2호
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• pp.135-139
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• 2003

The purpose of this study is to analyze the curing effect of planar surface heater for concreting in cold weather. Some experiments were conducted to evaluate the temperature history of concrete cured with heating sheets in the laboratory conditions. As the results, It was showed that the 130W/$m^2$-heater could raise the inner temperature more than $20^{\circ}C$ under the environmental condition of -5~$-20^{\circ}C$. And the temperature of concrete cured by the 200W/$m^2$-heater was 5~$10^{\circ}C$ higher than that of concrete cured by 130W/$m^2$-heater. Finally, through the curing by the planar surface heater during the first 1.5~2 days, it is possible to secure the sufficient maturity of concrete.

• Composites Research
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• 제33권2호
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• pp.55-60
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• 2020

구조용 일액형 에폭시 접착제에 나노 및 마이크로 크기의 Fe₃O₄ 분말을 첨가하여 유도가열용 접착제를 제조하였고, 제조된 접착제를 이용하여 GFRP 피착재의 두께 및 Fe₃O₄ 분말의 첨가량 변화에 따른 가열 성능을 평가하였다. 실험 결과, 접착제의 승온 거동이 유도 가열로 가열한 경우 오븐경화에 비해 GFRP 피착재의 두께에 영향을 작게 받는 것이 관찰되었으며 접착제 내의 Fe₃O₄ 분말의 함량이 증가할수록 가열 속도와 전단 강도가 증가하는 경향을 나타냈다.

• 한국콘텐츠학회논문지
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• 제16권1호
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• pp.52-59
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• 2016

동절기에 타설되는 대부분의 콘크리트 구조물에서 가설 초기단계에서의 양생방법의 선정은 매우 중요한 요소이다. 동절기에는 초기균열과 강도저하를 방지하기 위하여 열선과 조강시멘트를 이용한 발열양생방법을 주로 적용하게 된다. 하지만 그 적용기법의 단순화 및 경험적 판단에의 의존으로 인하여 대부분의 건설현장에서 최적의 양생방법을 선정하지 못하고 있는 실정이다. 이에 따라 본 논문에서는 비정상상태의 열전달 해법을 통하여 가장 적절한 열선의 가열온도, 기간, 열선 배치간격을 선정하는 평가 알고리즘을 개발하였다. 이를 위하여 관리 매개변수에 주안점을 둔 구조해석 시스템을 통한 사용자 중심의 OOP 루틴을 적용하였다. 본 시스템에서는 입력모듈, DB 모듈, DB저장 모듈, 해석모듈 및 결과분석모듈로 구분하였으며, 각 모듈간의 연계는 visual c# 루틴으로 처리하였다. 또한 그래픽 인터페이스와 DB 테이블은 사용자 편의성을 고려하여 개발하였다.

• 국제학술발표논문집
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• The 7th International Conference on Construction Engineering and Project Management Summit Forum on Sustainable Construction and Management
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• pp.89-98
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• 2017

The floor heating method generally uses a wet construction method including the installation of resilient material, lightweight foam concrete, heating piping, and finishing mortar. Such a wet construction method not only delays other internal finishing processes during curing period for two mortar pouring process, but also has a disadvantage that it is difficult to replace the floor heating layer when it deteriorated because it is integrated with the frame. Dry floor heating construction method can be a good alternative in that it can solve these defects. Conversely, when it applied to the wall structure that is vulnerable to the interlayer noise compared with the column-beam structure, the question about the heavy-impact sound(HIS) insulation performance is raised. Therefore, conventional dry floor heating method is hard to apply to the wall structure apartments. Therefore, for the purpose to improve the applicability of dry floor heating method in wall structure apartments, this study investigated the change of floor impact sound, especially HIS insulation performance which is one of the required performance for the floor structure. This study tried to examine whether the change of heavy-impact sound pressure level(SPL) shows a tendency at the significant level according to the shape and mass of the floor structure. Through filed experiments on wall structure apartment, this study confirmed that the form of the raised floor shows better HIS insulation performance than the fully-supported form. In addition, it was also confirmed that the HIS insulation performance increases with the mass on the upper part. Moreover, this study found the fact that a mass of about 30 kg/m² or more should be placed on the upper structure to reduce the heavy-impact SPL according to the bang machine measuring method. Although this study has a limit due to insufficient experiment samples, if the accuracy of this study is increased, it will contribute to the diffusion of dry floor heating by setting the HIS insulation performance target and designing the dry floor heating structure that meets the target.

• Elastomers and Composites
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• 제29권2호
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• pp.121-130
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• 1994

The physical properties of rubber blend between natural rubber(NR) and ethylene propylene diene terpolymer(EPDM) were investigated as a study of EPDM composite materials. For EPDM/NR blends, the effects of ethylene and diene contents in EPDM, blend ratio, dicumyl peroxide(DCP) curing system on the physical properties, interfacial adhesion force and dynamic crack growth etc. were studied. EPDM/NR blends loaded with carbon black were prepared by mechanical mixing and cured by plate heating cure press. Crosslinking density was measured by swelling method with toluene. The physical properties of all blends were measured with Instron, fatigue to failure(FTF), Demattia flex cracking tester(DMFC), scanning electron microscopy (SEM), etc. As the ethylene and diene contents in EPDM increased, the physical properties, such as dynamic crack growth, adhesion to other component were increased too. Interfacial adhesion force of EPDM/NR blends to dissimilar layer was improved by the use of optimum peroxide curing system.

• 콘크리트학회논문집
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• 제29권2호
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• pp.141-148
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• 2017

본 연구는 PC부재의 공장생산에 있어서 여러 가지 증기양생 조건의 변수에 따른 고강도 콘크리트의 초기 압축강도 발현성상을 실험적으로 검증하고, 최적 양생조건을 확인하기 위한 것이다. 40 MPa 이상의 고강도 콘크리트 제조에는 보통 포틀랜드 시멘트를 사용하였으며, 콘크리트의 배합조건은 물-시멘트비 3종류(W/C 25%, 35% 및 45%)를 대상으로 하였다. 본 연구의 증기양생 변수로 (1) 전치양생 시간 3종류, (2) 최고 양생온도 3종류, (3) 최고온도 유지시간 3종류, (4) 승온 및 강온양생 온도 1종류 등을 대상으로 재령별 압축강도 시험을 실시하였다. 또한, 증기양생 및 표준양생에 따른 재령별 강도발현을 비교하였다. 실험결과, (1) 전치양생은 콘크리트의 초기 응결시간 이상, (2) 최고 양생온도는 $55^{\circ}C$ 이하, (3) 최고온도 유지시간은 6시간 이하로 하는 것이 증기양생 고강도 콘크리트의 강도발현에 적합한 양생조건으로 나타났다. 또한, 재령 28일에서 증기양생과 표준양생의 압축강도 발현성상의 역전현상이 발생하였다. 따라서 이러한 양생조건으로 PC부재의 생산성 및 현장관리를 위한 기초자료로 제시하고자 한다.