• Title/Summary/Keyword: curing methods

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Degree of conversion of two dual-cured resin cements light-irradiated through zirconia ceramic disks

  • Kim, Min-Jeong;Kim, Kyo-Han;Kim, Young-Kyung;Kwon, Tae-Yub
    • The Journal of Advanced Prosthodontics
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    • v.5 no.4
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    • pp.464-470
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    • 2013
  • PURPOSE. The aim of this Fourier transform infrared (FTIR) spectroscopic study was to measure the degree of conversion (DC) of dual-cured resin cements light-irradiated through zirconia ceramic disks with different thicknesses using various light-curing methods. MATERIALS AND METHODS. Zirconia ceramic disks (KT12) with three different thicknesses (1.0, 2.0, and 4.0 mm) were prepared. The light transmittance of the disks was measured using ultraviolet visible near-infrared spectroscopy. Four different light-curing protocols were used by combining two curing light modes (Elipar TriLight (standard mode) and bluephase G2 (high power mode)) with light-exposure times of 40 and 120 seconds. The DCs of the two dual-cured resin cements (Duo-Link and Panavia F2.0) light-irradiated through the disks was analyzed at three time intervals (3, 7, and 10 minutes) by FTIR spectroscopy. The data was analyzed using repeated measures ANOVA (${\alpha}$=.05).Two-way ANOVA and Tukey post hoc test were used to analyze the 10 minute DC results. RESULTS. The 1.0 mm thick disk exhibited low light transmittance (<25%), and the transmittance decreased considerably with increasing disk thickness. All groups exhibited significantly higher 10 minute DC values than the 3 or 7 minute values (P<.05), but some exceptions were observed in Duo-Link. Two-way ANOVA revealed that the influence of the zirconia disk thickness on the 10 minute DC was dependent on the light-curing methods (P<.001). This finding was still valid even at 4.0 mm thickness, where substantial light attenuation took place. CONCLUSION. The curing of the dual-cured resin cements was affected significantly by the light-curing technique, even though the additional chemical polymerization mechanism worked effectively.

Temperature Properties of Vertical Reinforcements in Wall Structures in Relation to the Different Methods of Bubble Sheet Installation in Winter (겨울철 버블시트 포설방법 변화에 따른 벽식구조 수직철근의 온도 특성)

  • Kim, Tae-Woo;Lee, Jea-Hyeon;Kyung, Yeong-Hyeok;Lee, Jong-Gyo;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.05a
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    • pp.11-12
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    • 2017
  • This study aims to analyze the properties of the temperature change in vertical reinforcements in outdoor wall structures in winter in relation to the different methods of bubble sheet installation, and to subsequently determine the possibility of initial frost damage to the concrete as a result of low temperature. As for the experimental variables, double bubble sheets were used as curing materials, and the curing method was to model the part where the slab and the wall intersect and the rebar is exposed, and to measure the change of temperature around the exposed rebar in accordance with the change of the coating curing. It was found that by employing curing method B, which is to install the bubble sheet between the vertical reinforcements, the most vulnerable area, which is 50mm below(④) the surface of the concrete, would be lowered to sub-zero temperature 20 hours later than when using curing method A, and that therefore it is more effective to install the bubble sheet between the vertical reinforcements for the prevention of initial frost damage.

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A STUDY OF POLYMERIZATION SHRINKAGE OF COMPOSITE RESIN ACCORDING TO FILLING METHODS USING STRAIN GAUGE (스트레인 게이지를 이용한 적층방법에 따른 복합레진의 중합수축에 관한 연구)

  • Kim, Eung-Hag;Kim, Jong-Soo;Yoo, Seung-Hoon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.35 no.1
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    • pp.18-29
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    • 2008
  • The purpose of this study was to compare the polymerization shrinkage of several filling methods using strain gauges. In this study, a light-emitting diode(LED) curing unit(Elipar Freeligh2, 3M EPSE, USA) and plasma arc lamp(PAL) curing unit(Flipo, LOKKI, France) were used for curing, Filtek $Z350^{TM}$(3M EPSE, USA) composite resin was used for the cavity filling. Sixty permanent bicuspid teeth, that were extracted for orthodontic treatment, were studied. The cavities were prepared on the occlusal surface and were filled using the following methods : 1) bulk filling, 2) parallel filling, 3) oblique filling The strain was recorded on the buccal, lingual, mesial and distal surfaces and the strain values were computed into stress values. The shear bond strength of each filling method was tested using a Micro Universal Testing machine. The results can be summarized as follows: 1. In the strain changes, all LED and PAL curing groups showed an increase on the buccal surface and a slow decrease as time elapsed. 2. In the strain changes of the mesial and distal surfaces, the decreases and increases were shown repeatedly and reduced as time elapsed. 3. There were no significant statistical strain changes among filling methods in the LED or PAL curing groups. 4. There were significant statistical strain changes between the LED and PAL curing groups on the buccal surface(p<0.05). 5. From the shear bond strength results, in the LED curing group, filling method 3 showed lower surface stress than filling method 1 and 2(p<0.05). In the PAL curing group, there were no significant statistical strain changes between each filling method. 6. The surface stress of each group was lower than the shear bond strength.

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An Analytic Study on Early aged Freezing Damage Prevention and Thermal Crack Control of Concrete in Cold-Weathering Mat Foundation Construction (동절기 매트기초공사시 콘크리트의 초기동해방지 및 온도충격제어에 관한 해석적 연구)

  • 이도범;김효락;박지훈;최일호
    • Proceedings of the Korea Concrete Institute Conference
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    • 2001.05a
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    • pp.807-812
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    • 2001
  • This study is peformed for checking the limitation and application of each curing/heating methods on cold-weathering mat foundation construction, considering temperature control, early strength security and temperature declination range limit, by means of concrete material properties and thermal analysis technique that were published previously. In the result of this analysis, we checked the open air temperature and mat depth that are possible to apply each curing/heating methods on cold-weathering construction and found curing/heating time of each methods that is able to prevent early aged freezing damage and thermal crack

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Comparison of Surface Microhardness of the Flowable Bulk-Fill Resin and the Packable Bulk-Fill Resin according to Light Curing Time and Distance

  • Hyung-Min Kim;Moon-Jin Jeong;Hee-Jung Lim;Do-Seon Lim
    • Journal of dental hygiene science
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    • v.23 no.2
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    • pp.123-131
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    • 2023
  • Background: As a restorative material used to treat dental caries, the light-curing type resin is widely used, but it has the disadvantage of polymerization shrinkage. The Bulk-Fill composite resin was developed to solve these shortcomings, but the existing research mainly focused on comparing the physical properties of a composite resin and a Bulk-Fill resin. A study on the light curing time and distance of the Bulk-Fill resin itself tend to be lacking. Methods: This study compares the surface microhardness of specimens prepared by varying the light curing time and distance of smart dentin replacement (SDR) as a flowable Bulk-Fill resin and Tetric N-ceram as a packable Bulk-Fill resin, and confirms the polymerization time and distance that becomes the optimum hardness. To determine the hardness of the specimen, it was measured using the Vickers Hardness Number (Matsuzawa MMT-X, Japan). Results: In SDR, the surface microhardness decreased as the distance increased in all time groups in the change distance from the curing tip. In the change of light curing time with respect to the distance from curing tip, the surface microhardness increased as the time increased. In Tetric N-ceram, the surface microharness showed no significant difference in the change of the distance of curing tip in the group of 20 and 60 second. But in the group of 10 and 40 seconds, decreased as the distance increased. The surface microharness increased as the light curing time increased in all distance groups. Conclusion: When using SDR and Tetric N-ceram in clinical practice, it is considered that as the distance from the polymerization reactor tip increases, a longer light curing time than the polymerization time recommended by the manufacturer is required.

Flexural strength of composite resin fabricated by various polymerization method (다양한 중합 방법으로 제작한 간접 수복물용 복합레진의 굴곡 강도)

  • Kim, Dong-Yeon;Park, Jin-Young;Kang, Hoo-Won;Kim, Ji-Hwan;Kim, Woong-Chul
    • Journal of Technologic Dentistry
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    • v.40 no.2
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    • pp.57-62
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    • 2018
  • Purpose: The aim of this study is to evaluate composite resins of indirect restorations for testing of flexural strength according to various polymerization methods. Methods: Specimen was produced a total of 40 to 10 per each group with a length 25 mm, width 2 mm, thickness 2 mm using a Teflon zig. The polymerization groups were classified into four groups. The first group proceeded with light curing only(LC group). The second group proceeded with light and heat curing(LHC group). The third group proceeded with air press and light curing(ALC group). The fourth group proceeded with air press, light and heat curing(ALHC group). Each prepared group was evaluated by flexural strength test. Statistical analysis was performed by one-way ANOVA. Post-test was performed with Tukey test. Results: The lowest in the ALC group was 119.18 MPa and the highest in the ALHC group was 168.15 MPa. There were statistically significant differences. Conclusion : The composite resin of the indirect restoration is recommended to heat curing along with the air press.

A STUDY ON THE BOND STRENGTH OF REPAIR RESIN TO THE SURFACE TREATED COMPOSITE RESINS (표면처리된 복합레진에 대한 수리용 레진의 결합강도에 관한 연구)

  • Kang, Hyun-Sook;Choi, Ho-Young
    • Restorative Dentistry and Endodontics
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    • v.20 no.2
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    • pp.487-507
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    • 1995
  • Composite resin repair requires strong bond strength between the new and old materials. The objective of the current study was to identify the optimal treatments for sufficient bond strengths. Bondings between same kinds of materials and cross bondings using chemical curing composites and light curing composites were tested. Surface treatments included the methods of sand-blasting, acid etching and coating of bonding agent. Seven kinds cases of combinations from three kinds of methods were experimented and compared with a control group of which surfaces were highly polished. Measurements of shear bond strength and observations of surface morphologic changes using a scanning electron microscope were done. Following conclusions were drawn : 1. The highest bond strength among composite resins were exhibited by the treatment of the sand-blasting and the coating of bonding agent. 2. Acid etched surfaces showed the lowest bond strength. Bond strengths obtained from experimental groups including acid etching were lower than those obtained from same kinds of experimental groups without acid etching. 3. Simple method of the coating of bonding agent produced the slightly increased bond strength on chemical curing composite and reduced bond strength on light curing composite. 4. Bonding surfaces of chemical curing composite resin showed slightly higher bond strengths than light curing composite resin, however significant differences were not confirmed statistically. 5. More significant irregular surfaces were created by sand-blasting method than acid etching method. 6. A principal component of fillers of both resins was silicon. Acid etching method produced the seperations and degradations of fillers, these were significant on light curing composite resins which containing barium fillers.

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A Study on the Mix Design and the Control System of Thermal Crack for High Quality Mass Concrete (고품질 매스콘크리트 시공을 위한 배합설계 및 온도균열제어 시스템에 관한 연구)

  • Kim, Sun-Gu;Lee, Sang-Soo;Won, Cheol;Park, Sang-Joon;Kim, Dong-Seok
    • Journal of the Korea Institute of Building Construction
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    • v.1 no.2
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    • pp.174-178
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    • 2001
  • This study was performed to control the thermal crack of the mat footing slab in the multi-purposed buildings. In this study, we executed the mixing design of concrete to satisfy the workability and the quality according to the site conditions. And, we evaluated quantitatively about the possibility of thermal crack by using hydration heat analysis system. Finally, we proposed the optimal mixing conditions, curing methods and curing period which all factors are considered. As a result, the optimal mixing conditions were : W/B 41%, unit binder 375kgf/$\textrm{m}^3$, FA replacement ratio 20%. Lowest thermal stress was 22.0kgf/$\textrm{cm}^2$ and at that time thermal crack index was over 1.5, when the coefficient of thermal conductivity was lowest among the curing conditions. And, the total curing time was estimated at 6.7 days according to curing steps.

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Application of Curing Method Using the Heating Cable for Cold Weather Concreting (매입형 열선에 의한 한중콘크리트의 보양방법 적용에 관한 연구)

  • 김형래;이정철;김찬수;이명진;김봉주
    • Proceedings of the Korea Concrete Institute Conference
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    • 2001.05a
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    • pp.769-774
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    • 2001
  • The purpose of this study is to analyze the curing effect of heating cable for concreting in cold weather. An experiment was conducted to evaluate the temperature history of concrete structures cured with embedded heating cables. Results are as follows : In comparison with the non-heating case, applying of heating cable resulted in the rise of temperature in the range of $10^{\circ}C$. In order to get successful results, the optimal pitch length for the embedded heating cables ranged from 20cm to 25cm. When working with the existing curing methods, applying this heating cable would be more effective in concrete curing. Finally, a formula and process was suggested to predict the Internal temperature history of concrete structures under the various curing conditions.

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A Study on the Mix Design and the Control of Thermal Crack of Mass Concrete (매스콘크리트의 배합설계 및 온도균열제어에 관한 연구)

  • Lee, Sang-Soo;Won, Cheol;Park, Sang-Joon;Kim, Dong-Seok
    • Proceedings of the Korea Concrete Institute Conference
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    • 2001.05a
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    • pp.533-538
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    • 2001
  • This study was peformed to control the thermal crack of the mat footing slab in the multi-purposed buildings. In this study, we executed the mixing design of concrete to satisfy the workability and the quality according to the site conditions. And, we evaluated quantitatively about the possibility of thermal crack by using hydration heat analysis system. Finally, we proposed the optimal mixing conditions, curing methods and curing period which all factors are considered. As a results, the optimal mixing conditions were : W/B 41%, unit binder 375kg/$cm^{2}$, FA replacement ratio 20%. Lowest thermal stress was 22.0kgf/$cm^{2}$ and at that time thermal crack index was over 1.5, when the coefficient of thermal conductivity was lowest among the curing conditions. And, the total curing time was estimated at 6.7 days according to curing steps.

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