• Title/Summary/Keyword: conventional curing

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A Development on the Non-Photomask Plate Making Technology for Screen Printing (III) (포토마스크가 필요 없는 스크린 제판 기술 개발(III))

  • Kang, Hyo-Jin;Park, Kyoung-Jin;Kim, Sung-Bin;Nam, Su-Yong;Ahn, Byung-Hyun
    • Journal of the Korean Graphic Arts Communication Society
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    • v.26 no.2
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    • pp.55-64
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    • 2008
  • We designed a UV-LED exposure system which has 365nm dominant wavelength due to the environment-friendly and economical maskless screen plate making. And the photoresist applied on the screen stretched was exposed without mask by beam projector with UV-LED light source. Then it was developed by air spray with $1.7\;kgf/cm^2$ of injection pressure. The pencil hardness and solvent resistance of curing photoresist film were excellent as those of conventional photoresist film and the maximum resolution of line image formed by maskless screen plate making. was $100{\mu}m$, so we could establish the possibility of environment-friendly maskless screen plate making technology. But the sharpness of the patterns were ${\pm}40{\mu}m$ since the exposure system for maskless plate making has weak light intensity and the diffusion of light.

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Effect of Polytriazolesulfone Addition on Fracture Toughness of DGEBA Epoxy Resin (DGEBA에 대한 폴리트리아졸술폰의 강인화 효과 연구)

  • Kwon, Woong;Lee, Minkyu;Han, Minwoo;Jeong, Euigyung
    • Textile Coloration and Finishing
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    • v.31 no.2
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    • pp.118-126
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    • 2019
  • This study aims to investigate the effect of polytriazolesulfone(PTS) addition on fracture toughness of diglycidyl ether of bisphenol A(DGEBA) and 4,4'-diaminodiphenylsulfone(DDS). Various amounts of PTS were added to DGEBA/4,4'-DDS in diazide and dialkyne monomer forms and polymerized during the epoxy curing process. Fracture toughness(K1C), tensile properties and thermal stability of the PTS added epoxy resin were evaluated and compared with those of PES, the conventional high Tg toughening agent, added epoxy resin. Fracture toughness of the PTS added epoxy resin was dramatically improved up to 133%, as the amount of PTS added increased, whereas that of the PES added epoxy resin was improved by only 67%. The tensile strength of PTS added DGEBA/4,4'-DDS was similar to the epoxy resin without PTS and tensile modulus was improved by 20%. And thermal stability of the PTS added epoxy resin was improved up to 14%. Therefore, PTS addition to DGEBA/4,4'-DDS, as a toughening agent, is very effective way to improve its fracture toughness without any lowering in other properties.

Bulk-fill 복합레진, 믿고 사용해도 될까?

  • Koh, Kyeol;Park, Jeong-Won
    • The Journal of the Korean dental association
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    • v.57 no.3
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    • pp.162-168
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    • 2019
  • Composite resin restorations in posterior teeth are increasing due to the aesthetic needs of patients and the development of materials. This trend will accelerate in line with domestic insurance policies. However, resin composites generate stresses due to their contraction during the polymerization process. To reduce the polymerization shrinkage stress of resin composites, incremental layering technique has been recommended for decades. This technique reduces stress at the cavity wall interface and allows a more efficient light curing of the material. Bulk-fill resin composites have been designed to simplify the restorative technique because they can be placed into cavities in a single increment of 4-5mm. The simplification of the operative procedures is desirable in clinical daily practice. In this context, bulk-fill resin composites are an attractive alternative for posterior restorations. However, a clearer understanding of the clinical performance of this relatively new class of materials in comparison to conventional resin composites is required. Based on previous studies, the aim of the current review was to present the clinical criteria for the use of bulk-fill composites in direct restorations of posterior teeth.

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Dual-curable Flame-Retardant Finish of Silk Fabrics Using a Water-soluble Cyclophosphazene Derivative (수용성 Cyclcophosphazene 유도체를 이용한 견섬유의 이중경화형 방염가공)

  • Kim, Jeong-Hwan;Baek, Ji-Yun;Jang, Jinho
    • Textile Coloration and Finishing
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    • v.34 no.4
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    • pp.217-223
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    • 2022
  • Flame-retardant finished silk fabrics could release carcinogenic formaldehyde resulting from the conventional finishing agents. New water-soluble cyclophosphazene derivative can be used as a formaldehyde-free flame retardant for the silk protein. Dichloro tetrakis{N-[3-dimethylamino)propyl]methacrylamido}cyclophosphazene(DCTDCP) can be cured by heat or UV irradiation as a durable flame retardant for the silk fabrics. Treatment conditions were optimized including curing temperature and time, finishing formulations, and UV energy. At the 30% DCTDCP application, peak HRR and THR decreased by 42.6% and 49.6% respectively compared to the pristine silk fabrics. Also char residue increased up to 48% from 11% indicating solid-phase retarding mechanism. The flame-retardant silk fabrics showed a LOI of 31.1 and the washed sample maintained a LOI of 26.8 even after ten laundering cycles.

Tribological Improvement of Lubricants Using Silicone Rubber Powders in Hydrogen Compressors

  • Sung-Jun Lee;Chang-Lae Kim
    • Tribology and Lubricants
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    • v.40 no.3
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    • pp.78-83
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    • 2024
  • The development of eco-friendly alternative energy sources has become a global priority owing to the depletion of fossil fuels and an increase in environmental concerns. Hydrogen energy has emerged as a promising clean energy source, and hydrogen compressors play a crucial role in the storage and distribution of compressed hydrogen. However, harsh operating conditions lead to the rapid deterioration of conventional lubricants in hydrogen compressors, thereby necessitating the development of advanced lubrication technologies. This study introduces micrometer-sized silicone rubber powders as lubricant additives to enhance the lubrication performance of hydraulic oils in hydrogen compressors. We prepare silicone rubber powders by varying the ratio of the silicone rubber base to the curing agent and investigate their effects on interfacial properties, friction behavior, and wear characteristics. The findings reveal that the incorporation of silicone rubber powders positively influences the surface affinity, wettability, friction reduction, and wear resistance of the lubricants on the 304SS substrate. Moreover, we identify the optimal lubricant formulations, with a 15:1 ratio demonstrating the most effective friction reduction and a 5:1 ratio exhibiting the highest wear resistance. The controlled surface modification by the silicone rubber powder and the enhanced interfacial characteristics of the powder-containing lubricants synergistically contribute to the improved lubrication performance. These results indicate the potential of silicone rubber powder additives for the development of long-life lubrication solutions for hydrogen compressors and related applications, ultimately contributing to the advancement of sustainable energy technologies.

Three Dimensional Comparative Study On The Accuracy Of Impression Technique Using New Impression Coping (새로운 인상용 코핑을 이용한 임플란트 인상법의 정확성에 대한 3차원적 비교 연구)

  • Kim, Se-Ra;Kim, In-Soo;Park, Sung-Jae;Lee, Byung-Ok;Ko, Sok-Min
    • Journal of Dental Rehabilitation and Applied Science
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    • v.26 no.3
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    • pp.323-337
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    • 2010
  • The objective of this study was to examine the availability of the new impression coping by comparing with conventional coping in implant pick-up impression technique. Five implant fixtures were installed on #14, 21, 23, 25, 27 in acrylic resin model. That model with 5 fixtures was standard model, which was divided 3 groups; using new flag type impression coping, conventional impression coping splinted with self-curing resin, conventional impression coping without splinting. We made metal circular cones for calculation 3-dimensional coordinates by attaching to implant fixtures or analogs. Three-dimensional relationships of each model were calculated. Data was analyzed by multiple ANOVA and Bonferroni. The accuracy of impression between using new flag type impression coping and conventional impression coping did not show differences in 3 - dimensional analysis.Within limitations of this study, the new flag type impression coping is available in implant pick-up impression technique.

BI-AXIAL FRACTURE STRENGTH OF RESIN MODIFIED GLASS IONOMERS (레진강화형 글라스아이오노머의 2 축 굽힘강도)

  • Lee, Yong-Keun;Im, Mi-Kyung;Koo, Dae-Hoi;Lee, Chung-Sik
    • Restorative Dentistry and Endodontics
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    • v.22 no.2
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    • pp.751-760
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    • 1997
  • Resin-modified glass ionomers were introduced in 1988 to overcome the problems of moisture sensitivity and low early mechanical strengths of the conventional glass ionomers, and to maintain their dinical advantages. The purpose of this study was to evaluate the bi-axial fracture strength of four resinmodified glass-ionomers(Fuji II LC, Vitremer, Dyract, VariGlass), one resin composite material(Z-100), and one conventional glass-ionomer(Fuji II). Three specimens of each material and shade combination were made according to the manufacturers' instructions. Materials were condensed into metal mold with a diameter of 10mm and a thickness of 2.0mm and pressed between two glass plates. Resin-modified glass ionomers were polymerized using a Visilux II light curing unit by irradiating for 60 seconds from both sides, and conventional glass ionomer was cured chemically. After specimens were removed from the molds, surfaces were polished sequentially on wet sandpapers up to No. 600 silicone carbide paper. The specimens were thermocycled for 2,000 cycles between $5^{\circ}C$ and $55^{\circ}C$ distilled water. After thermocycling, bi-axial fracture strengths were measured using a compressive-tensile tester(Zwick 1456 Z020, Germany) with the cross head speed of 0.5mm/minute. The results were as follows: 1. Two factors of the kind and color of materials had a main effect on bi-axial fracture strength (p<0.01), and bi-axial fracture strength was influenced significantly by the kinds of materials (p<0.01). But there was no significant interaction between two variables of the kind and color of materials (p>0.05). 2. Comparing the mechanical properties of the materials, the elastic modulus of Z100 was higher than any other material, and there was no difference in the displacement at fracture among materials. The bi-axial fracture strength of Z100 was significantly higher than any other material, and that of resin-modified glass ionomers was significantly higher than that of conventional glass ionomer (p<0.05). 3. In the same material group, the color of material had little influence on the mechanical properties.

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The study on the shear bond strength of resin and porcelain to Titanium (티타늄에 대한 레진과 도재의 결합 강도에 관한 연구)

  • Park, Ji-Man;Kim, Yeong-Soon;Jun, Sul-Gi;Park, Eun-Jin
    • The Journal of Korean Academy of Prosthodontics
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    • v.47 no.1
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    • pp.46-52
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    • 2009
  • Statement of problem: Recently, titanium has become popular as superstructure material in implant dentistry because titanium superstructure can be easily milled by means of computer-aided design and manufacture (CAD/CAM) technique. But retention form such as nail head or bead cannot be cut as a result of technical limitation of CAD/CAM milling and bond strength between titanium and porcelain is not as strong as that of conventional gold or metal alloy. Purpose: The objective of this study was to evaluate the shear bond strength of three different materials: heat curing resin, composite resin, porcelain which were bonded to grade II commercially pure Titanium (CP-Ti). Material and methods: Thirty seven CP-Ti discs with 9 mm diameter, 10 mm height were divided into three groups and were bonded with heat curing resin (Lucitone 199), indirect composite resin (Sinfony), and porcelain (Triceram) which were mounted in a former with 7 mm diameter and 1 mm height. Samples were thermocycled for 1000 cycles at between $5-55^{\circ}C$. Shear bond strength (MPa) was measured with Instron Universal Testing Machine with cross head speed of 1 mm/min. The failure pattern was observed at the fractured surface and divided into adhesive, cohesive, and combination failure. The data were analyzed by one-way ANOVA and Scheffe's multiple range test (${\alpha}=0.05$). Results: Lucitone 199 ($17.82{\pm}5.13\;MPa$) showed the highest shear bond strength, followed by Triceram ($12.97{\pm}2.11\;MPa$), and Sinfony ($6.00{\pm}1.31\;MPa$). Most of the failure patterns in Lucitone 199 and Sinfony group were adhesive failure, whereas those in Triceram group were combination failure. Conclusion: Heat curing resin formed the strongest bond to titanium which is used as a CAD/CAM milling block. But the bond strength is still low compared with the bond utilizing mechanical interlocking and there are many adhesive failures which suggest that more studies to enhance bond strength are needed.

A STUDY ON THE MODE OF POLYMERIZATION OF LIGHT-CURED RESTORATIVE MATERIALS CURED WITH PLASMA ARC LIGHT CURING UNIT (Plasma arc light curing unit을 이용한 광중합형 수복재의 중합양상)

  • Woo, Youn-Sun;Jeong, Tae-Sung;Kim, Shin
    • Journal of the korean academy of Pediatric Dentistry
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    • v.29 no.2
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    • pp.262-269
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    • 2002
  • The purpose of this study was to compare the effect of distance of light tip to resin surfaces and exposure time on the polymerization of surface and 2 mm subsurface of composite resins cured with two light sources; conventional halogen light (XL 3000, 3M, U.S.A.) and plasma arc light (Flipo, LOKKI, France) and compare the uniformity of polymerization from the center to the periphery of resin surfaces according to polymerization diameter cure with two light sources. From the experiment, the following results were obtained. 1. Difference of relative light intensity decrease in plasma arc light smaller than that of conventional halogen light(p<0.05). 2. In all groups, microhardness of top surfaces was decreased when distance of the light tip to resin surfaces is more than 2mm and increased according to increase of exposure time(p<0.05). 3. Difference of microhardness of the 2mm subsurface was rapidly decreased when distance of light tip to resin surfaces is more than 4mm(except, plasma arc light exposure time of 3 seconds). and the distance of light tip to resin surfaces and exposure time more affected 2mm subsurface rather than top surface(p<0.05). 4. Although exposure time was increased, difference of microhardness of the 2mm subsurface with the distance of light tip to resin surfaces was relatively high in groups between below 4mm and 6 mm(p<0.05). 5. Plasma arc light exposure time of 6 to 9 seconds produced microhardness values and microhardness change according to various distance similar to those produced with 40 to 80 second exposure to a conventional halogen light(p>0.05). 6. In all groups, microhardness was decreased gradually from the center to the periphery of resin surfaces(p<0.05).

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A Study on the pH Reduction of Controlled Low Strength Material with Coal Ash (석탄회를 활용한 CLSM의 pH 저감에 관한 연구)

  • Kim, Youngil;Jee, Sunghyun;Chun, Byungsik
    • Journal of the Korean GEO-environmental Society
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    • v.11 no.9
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    • pp.39-45
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    • 2010
  • Controlled low strength material(CLSM) is produced by mixing portland cement, fine aggregates, water and chemical admixtures. Sand is the most commonly used as the fine aggregates in the conventional CLSM. It is getting more and more difficult to obtain sand in Korea so it is required that the alternative materials be developed as the replacement of sand. Since the engineering characteristics of coal ash are similar to the sand, it becomes necessary to examine the application of the coal ash as the alternative material for CLSM and as the environment-friendly material. When the results meet the optimum pH level that plants can live, it can be expanded the scale of application of the study on the plant as the important field. This study was subjected to present the method to reduce the pH range of CLSM to a suitable condition that plants can survive. To verify this method, the care of neutralization was conducted by immersing the specimen to Ammonium monohydrogen phosphate. Before curing and neutralization, the maximum pH of developmental CLSM is approximately 11. However, the pH value of developmental CLSM has under 9.5 after peaceful curing and neutralization management.