• Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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• 2001.06a
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• pp.1511-1511
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• 2001

Energy content, expressed as calories per gram, is an important part of the evaluation and marketing of foods in developed countries. Currently accepted methods of measurement of energy by U.S. food labeling legislation include measurement of gross calories by bomb calorimetry with an adjustment for undigested protein and by calculation using specific factors for the energy values of protein, carbohydrate less the amount of insoluble dietary fiber, and total fat. The ability of NIRS to predict the energy value of diverse, processed and unprocessed cereal food products was investigated. NIR spectra of cereal products were obtained with an NIR Systems monochromator and the wavelength range used for analysis was 1104-2494 nm. Gross energy of the foods was measured by oxygen bomb calorimetry (Parr Manual No. 120) and expressed as calories per gram (CPGI, range 4.05-5.49 cal/g). Energy value was adjusted for undigested protein (CPG2, range 3.99-5.38 cal/g) and undigested protein and insoluble dietary fiber (CPG3, range 2.42-5.35 cal/g). Using a multivariate analysis software package (ISI International, Inc.) partial least squares models were developed for the prediction of energy content. The standard error of cross validation and multiple coefficient of determination for CPGI using modified partial least squares regression (n=127) was 0.060 cal/g and 0.95, respectively, and the standard error of performance, coefficient of determination, bias and slope using an independent validation set (n=59) were 0.057 cal/g, 0.98, -0.027 cal/g and 1.05 respectively. The PLS loading for factor 1 (Pearson correlation coefficient 0.92) had significant absorption peaks correlated to C-H stretch groups in lipid at 1722/1764 nm and 2304/2346 nm and O-H groups in carbohydrate at 1434 and 2076 nm. Thus the model appeared to be predominantly influenced by lipid and carbohydrate. Models for CPG2 and CPG3 showed similar trends with standard errors of performance, using the independent validation set, of 0.058 and 0.088 cal/g, respectively, and coefficients of determination of 0.96. Thus NIRS provides a rapid and efficient method of predicting energy content of diverse cereal foods.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.26 no.4
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• pp.293-297
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• 1981

An attempt has been made to determine the optimum size of sampling unit and the number of samples for a given precision in wheat, using the data collected from the various experiments in 1979/80. It was found that the coefficients of variation for number of spikes except the case of high-ridge broadcasting by 8HP rotarized seeder are in the same order of those for yield of wheat, and the regression coefficients associated with the coefficients of variation and the size of sampling unit were significant at 1% level of type I error. A wide range of variation in the size of sampling unit was observed for different methods of seeding, indicating the proper sizes of sampling units for 40cm \times 18cm, 60cm \times 18cm, 20cm \times 5cm, 120cm \times 90cm to be 0.40$m^2$, 0.17$m^2$, , 0.11$m^2$, , 0.55$m^2$, , respectively. The variance component for the experimental error was not physically possible to estimate due probably to high variability among the sampling units. The number of the sampling units per plot for a given precision of CV=12% was estimated to be one in an experiment with 4 replicates.

• Journal of Korea Water Resources Association
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• v.50 no.6
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• pp.419-427
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• 2017

In mountainous rivers, the drag force acting on cobbles abundant in the riverbed surface is important in predicting behavior and response of the river. However there is little research for the drag coefficients of cobbles. This paper is to carry out the experiments for drag force of cobble and analyze the relation between the cobble shape and the drag coefficient. The effects of the shape factor on the drag coefficients $C_D$ when the long axis or the short axis of the cobbles are parallel to the direction of flow velocity were analyzed. The coefficient of drag force increased with the nominal diameter Reynolds number $R_{ep}$. The drag coefficients are greater in short axis than long axis. The coefficient of determination of the relation between $C_D$ and $R_{ep}$ is greater in long axis than short axis. This means that the drag forces acting on the irregularly-shaped cobbles depend on the axis. A change of the drag force distribution has brought about the alternative swing of cobbles. For $R_{ep}$ > 12,000, the amplitude of the swing has been increased sharply and especially was greater in short axis than long axis.

• Journal of Institute of Control, Robotics and Systems
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• v.13 no.7
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• pp.637-648
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• 2007

This paper presents a sensor fusion method based on indirect Kalman filter(IKF) for error compensation of low-cost inertial sensors and its application to the determination of attitude and position of small flying robots. First, the analysis of the measurement error characteristics to zero input is performed, focusing on the bias due to the temperature variation, to derive a simple nonlinear bias model of low-cost inertial sensors. Moreover, from the experimental results that the coefficients of this bias model possess non-deterministic (stochastic) uncertainties, the bias of low-cost inertial sensors is characterized as consisting of both deterministic and stochastic bias terms. Then, IKF is derived to improve long term stability dominated by the stochastic bias error, fusing low-cost inertial sensor measurements compensated by the deterministic bias model with non-inertial sensor measurement. In addition, in case of using intermittent non-inertial sensor measurements due to the unreliable data link, the upper and lower bounds of the state estimation error covariance matrix of discrete-time IKF are analyzed by solving stochastic algebraic Riccati equation and it is shown that they are dependant on the throughput of the data link and sampling period. To evaluate the performance of proposed method, experimental results of IKF for the attitude determination of a small flying robot are presented in comparison with that of extended Kaman filter which compensates only deterministic bias error model.

• Journal of the Korean Chemical Society
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• v.30 no.6
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• pp.538-547
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• 1986

The 8 rare earth elements were determined in the monazite concentrates by X-ray fluorescence spectrometry. The spectral line overlapping interferences from the other elements were investigated and the correction methods of interferences were studied using line overlap coefficients. The coefficients were calculated from the ratios of the intensities measured at the diffracted angle (2${\theta}$) of the analytical lines of other elements to the intensity of pure rare earth oxide. The coefficients were used to correct the line overlaps by a regression analysis. The linearities of calibration curves from the corrected intensities were remarkably improved, and their standard deviations were decreased. The analytical results agreed with that of the inductively coupled plasma(ICP) spectrometry within an allowable error range.

• Journal of Biosystems Engineering
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• v.43 no.4
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• pp.331-341
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• 2018

Purpose: This study was conducted to develop a linear Proportional-Integral-Derivative (PID) control algorithm for the ascending and descending system of a rice transplanter and to analyze its response characteristics. Methods: A hydraulic model using a single-acting actuator, proportional valve and a PID control algorithm were developed for the ascending and descending system. The PID coefficients are tuned using the Ziegler-Nichols (Z-N) method and the characteristics of unit step response are analyzed to select the PID coefficients at various pump speeds. Results: Results showed that the performance of the PID controller was superior in any condition. It was found that the highest settling time and maximum overshoot were less than 0.210 s and 5%, respectively at all pump speed. It was determined that the steady state errors were 0% in all the cases. The lowest overshoot and settling time were calculated to be nearly 2.56% and 0.205 s, respectively at the pump rated speed (2650 rpm). Conclusions: The results indicated that the developed PID control algorithm would be feasible for the ascending and descending system of a rice transplanter. Finally, it would be helpful to plant the seedlings uniformly and improve the performance of the rice transplanter.

• Korean Journal of Pharmacognosy
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• v.49 no.1
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• pp.76-83
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• 2018

A traditional herbal formula, Gyeji-tang has been used to treat the early colds, headache, chills, and fever in Asian countries. In this study, we were performed simultaneous determination of the 14 bioactive marker compounds, gallic acid, spinosin, paeoniflorin, albiflorin, liquiritin apioside, liquiritin, 6'''-feruloylspinosin, liquilitigenin, coumarin, cinnmamic acid, benzoylpaeoniflorin, cinnamaldehyde, glycyrrhizin, and 6-gingerol in Gyeji-tang using an ultra-performance liquid chromatography-electrospray ionization-mass spectrometry (UPLC-ESI-MS/MS). Analytical column was used a Waters Acquity UPLC BEH $C_{18}$ analytical column ($2.1{\times}100mm$, $1.7{\mu}m$) and maintained at $45^{\circ}C$ with a flow rate of 0.3 mL/min. The mobile phase consists of 0.1% (v/v) formic acid in water and acetonitrile with gradient elution. The MS analysis was conducted using multiple reaction monitoring in the positive and negative modes by a Waters ACQUITY TQD LC-MS/MS system. The calibration curves of 14 bioactive marker compounds showed linearity with correlation coefficients ${\geq}0.9798$. The limits of detection and quantification values were in the range of 0.11-6.66 ng/mL and 0.34-19.99 ng/mL, respectively. As a result of the analysis using the established LC-MS/MS method, the amounts of tested 14 compounds in the lyophilized Gyeji-tang sample were detected up to $85.7{\mu}g/g$. These results may be useful for quality assessment of a traditional herbal formulas.

• Journal of Food Hygiene and Safety
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• v.23 no.3
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• pp.271-275
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• 2008

Choline is important an organic compound for normal membrane function, acetylcholine synthesis, lipid transport, and methyl metabolism. In biological tissues and foods, there are multiple choline compounds that contribute to choline content. There are so many analytical methods for choline determination, such as radioisotopic, high-performance liquid chromatography, and gas chromatography/mass spectrometry. However, these existing methods are expensive, unmanageable, and time-consuming. In this study, we modified enzymatic method, which is applicable for the determination of choline in milk and infant formulas, and applied to bovine serum and muscle. The calibration curves were linear with higher correlation coefficients than 0.994. Recoveries obtained by calibration curves from the spiked bovine serum and muscle samples varied between 70.6 and 85.2%. The method may be suitable for use as a routine method in the determination of choline for biological tissue and food samples.

• YAKHAK HOEJI
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• v.60 no.3
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• pp.112-117
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• 2016

A liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed and validated for the determination of caffeine in forensic aqueous sample. The centrifuged sample ($100{\mu}l$) was diluted 50-fold with distilled water. The diluted sample ($400{\mu}l$) was then diluted further with $200{\mu}l$ of 0.1% formic acid solution and $400{\mu}l$ of acetonitrile containing 500 ng of caffeine-(3-methyl-$^{13}C_3$) prior to LC-MS/MS analysis. The mobile phase was composed of 0.1% formic acid in distilled water (A) and acetonitrile (B). Chromatographic separation was performed by using a Zorbax SB-C18 ($100mm{\times}2.1mm$ i.d., $3.5{\mu}m$) column and caffeine was eluted within 1.1 min. Linear least-squares regression with a 1/x weighting factor was used to generate a calibration curve with the coefficients of determination ($r^2=0.9983$). The lower limit of quantification was $25ng/ml$ for the analyte. The process efficiency was 98.6~100.1%. Intra- and inter-day precisions were not more than 2.1% and 1.7%, while intra- and inter-day accuracies were ranged from -6.8 to 4.5%, respectively. The suitability of the method was examined by analyzing unknown forensic aqueous samples.

• Korean Journal of Computational Design and Engineering
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• v.9 no.4
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• pp.397-405
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• 2004

Texture mapping is the process of covering 3D models with texture images in order to increase the visual realism of the models. For proper mapping the coordinates of texture images need to coincide with those of the 3D models. When projective images from the camera are used as texture images, the texture image coordinates are defined by a camera calibration method. The texture image coordinates are determined by the relation between the coordinate systems of the camera image and the 3D object. With the projective camera images, the distortion effect caused by the camera lenses should be compensated in order to get accurate texture coordinates. The distortion effect problem has been dealt with iterative methods, where the camera calibration coefficients are computed first without considering the distortion effect and then modified properly. The methods not only cause to change the position of the camera perspective line in the image plane, but also require more control points. In this paper, a new iterative method is suggested for reducing the error by fixing the principal points in the image plane. The method considers the image distortion effect independently and fixes the values of correction coefficients, with which the distortion coefficients can be computed with fewer control points. It is shown that the camera distortion effects are compensated with fewer numbers of control points than the previous methods and the projective texture mapping results in more realistic image.