• Title/Summary/Keyword: coefficient region

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Study for Residue Analysis of Fluxametamid in Agricultural Commodities

  • Kim, Ji Young;Choi, Yoon Ju;Kim, Jong Soo;Kim, Do Hoon;Do, Jung Ah;Jung, Yong Hyun;Lee, Kang Bong;Kim, Hyochin
    • Korean Journal of Environmental Agriculture
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    • v.38 no.1
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    • pp.1-9
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    • 2019
  • BACKGROUND: Accurate and simple analytical method determining Fluxametamid residue was necessary in various food matrices. Additionally, fulfilment of the international guideline of Codex (Codex Alimentarius Commission CAC/GL 40) was required for the analytical method. In this study, we developed Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) method to determine the Fluxametamid residue in foods. METHODS AND RESULTS: Fluxametamid was extracted with acetonitrile, partitioned and concentrated with dichloromethane. To remove the interferences, silica SPE cartridge was used before LC-MS/MS (Liquid Chromatography-Tandem Mass Spectrometry) analysis with $C_{18}$ column. Five agricultural commodities (mandarin, potato, soybean, hulled rice, and red pepper) were used as a group representative to verify the method. The liner matrix-matched calibration curves were confirmed with coefficient of determination ($r^2$) greater than 0.99 at calibration range of 0.001-0.25 mg/kg. The limits of detection and quantification were 0.001 and 0.005 mg/kg, respectively. Mean average accuracies were shown to be 82.24-115.27%. The precision was also shown to be less than 10% for all five samples. CONCLUSION: The method investigated in this study was suitable to the Codex guideline for the residue analysis. Thus, this method can be useful for determining the residue in various food matrices as routine analysis.

Experimental study on energy dissipation and damage of fabricated partially encased composite beams

  • Wu, Kai;Liu, Xiaoyi;Lin, Shiqi;Tan, Chengwei;Lu, Huiyu
    • Computers and Concrete
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    • v.30 no.5
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    • pp.311-321
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    • 2022
  • The interfacial bond strength of partially encased composite (PEC) structure tends to 0, therefore, the cast-in-place concrete theoretically cannot embody better composite effect than the fabricated structure. A total of 12 specimens were designed and experimented to investigate the energy dissipation and damage of fabricated PEC beam through unidirectional cyclic loading test. Because the concrete on both sides of the web was relatively independent, some specimens showed obvious asymmetric concrete damage, which led to specimens bearing torsion effect at the later stage of loading. Based on the concept of the ideal elastoplastic model of uniaxial tensile steel and the principle of equivalent energy dissipation, the energy dissipation ductility coefficient is proposed, which can simultaneously reflect the deformability and bearing capacity. In view of the whole deformation of the beam, the calculation formula of energy dissipation is put forward, and the energy dissipation and its proportion of shear-bending region and pure bending region are calculated respectively. The energy dissipation efficiency of the pure bending region is significantly higher than that of the shear-bending region. The setting of the screw arbors is conducive to improving the energy dissipation capacity of the specimens. Under the condition of setting the screw arbors and meeting the reasonable shear span ratio, reducing the concrete pouring thickness can lighten the deadweight of the component and improve the comprehensive benefit, and will not have an adverse impact on the energy dissipation capacity of the beam. A damage model is proposed to quantify the damage changes of PEC beams under cyclic load, which can accurately reflect the load damage and deformation damage.

Analysis of Contrast Medium Dilution Rate for changes in Tube Current and SOD, which are Parameters of Lower Limb Angiography Examination (하지 혈관조영검사 시 매개변수인 관전류와 SOD에 변화에 대한 조영제 희석률 분석)

  • Kong, Chang gi;Han, Jae Bok
    • Journal of the Korean Society of Radiology
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    • v.14 no.5
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    • pp.603-612
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    • 2020
  • This study has a purpose to look into the effect of the relationship between the Tube current (mA) and SOD(Source to Object Distance), which is a parameter of lower limb angiography examination, and the dilution rate of the contrast medium concentration (300, 320, 350) on the image. To that end, using 3 mm vessel model water phantom, a vessel model custom made in the size of peripheral vessel diameter, this study measured relationships between change of parameters, such as tube current (mA), SOD and varying concentrations (300, 320, 350) of contrast medium dilution into SNR and CNR values while analyzing the coefficients of variance(cv<10). The software used to measure SNR and CNR values was Image J 1.50i from NIH (National Institutes of Health, USA). MPV (mean pixel value) and SD (standard deviation) were used after verifying numerically the image signal for region of interest (ROI) and background on phantom from the DICOM (digital imaging and communications in medicine) 3.0 file transmitted to PACS. As to contrast medium dilution by the change of tube current, when 146 mA and 102 mA were compared, For both SNR and CNR, the coefficient of variation value was less than 10 until the section of CM: N/S dilution (100% ~ 30% : 70%) but CM: N/S dilution rate (20%: 80% ~ 10% : 90%) the coefficient of variation was 10 or more. As to contrast medium dilution by concentration for SOD change, when SOD's (32.5 cm and 22.5 cm) were compared,For both SNR and CNR, the coefficient of variation value was less than 10 until the section of CM: N/S dilution (100% ~ 30% : 70%) but CM: N/S dilution rate (20%: 80% ~ 10% : 90%) the coefficient of variation was 10 or more. As to contrast medium dilution by concentration for SOD change, when SOD's (32.5 cm and 12.5 cm) were compared,For both SNR and CNR, the coefficient of variation value was less than 10 until the section of CM: N/S dilution (100% ~ 30% : 70%) but CM: N/S dilution rate (20%: 80% ~ 10% : 90%) the coefficient of variation was 10 or more. As a result, set a low tube current value in other tests or procedures including peripheral angiography of the lower extremities in the intervention, and make the table as close as possible to the image receiver, and adjust the contrast agent concentration (300) to CM: N/S dilution (30%: 70%). ) Is suggested as the most efficient way to obtain images with an appropriate concentration while simultaneously reducing the burden on the kidney and the burden on exposure.

Enhancement of the Performance a Centrifugal Compressor in an Automobile Turbocharger by Modifying the Circumferential Inlet Height of Volute (원주방향 볼류트 입구 높이를 수정한 자동차용 터보차저 원심압축기의 성능 향상)

  • Zhou, Tianjun;Lee, Geun Sik
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.38 no.2
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    • pp.115-120
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    • 2014
  • To enhance the performance of an automobile turbocharger compressor, the circumferential inlet heights of the volute were modified and the flow field for the combined region of the diffuser and volute was numerically investigated using commercial software. Basically, a well-designed volute should have a high pressure recovery coefficient and a low loss coefficient for the total pressure. In this study, two circular volutes with the same cross sectional shape and tongue angle, but circumferentially different volute inlet heights, were selected. One volute had the middle inlet in the cross-section at the circumferential angle of $90^{\circ}$ but gradually lower inlet heights for the angles between $90^{\circ}$ to $360^{\circ}$ with respect to the cross sectional center of the volute, while maintaining the same height between the tangential line connecting the lowest positions of the cross section and the line connecting the volute inlets in the circumferential direction (case 1 volute). The other volute has an inlet height that is 2 mm lower than in case 1 volute such that the tongue section has a tangential inlet (case 2 volute). The results showed that the case 2 volute had a higher total pressure ratio because of its higher pressure recovery coefficient and higher isentropic efficiency, resulting from the lower loss coefficient along the circumferential position than the case 1 volute.

Application of SAR DATA to the Study on the Characteristics of Sedimentary Environments in a Tidal Flat (SAR 자료를 이용한 갯벌 퇴적환경 특성 연구)

  • Kim, Kye-Lim;Ryu, Joo-Hyung;Kim, Sang-Wan;Choi, Jong-Kuk
    • Korean Journal of Remote Sensing
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    • v.26 no.5
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    • pp.497-510
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    • 2010
  • In this study, comparisons of the backscattering coefficients and the coherence values which had been extracted from SAR (Synthetic Aperture Radar) images such as JERS-1, ENVISAT and ALOS satellites with surface roughness, surface geometric and soil moisture content were carried out. As the results of analysis using the backscattering coefficient and coherence values from SAR images, the coherence was shown high in the region containing more of mud fraction due to higher viscosity of fine grain-size. A lot of tidal channels were well developed in the Ganghwa tidal flat, affecting the drainage of seawater and subsequent soil moisture content by exposure time of tidal flat. The backscattering coefficient. consequently, appeared to be lower in sand flat and mix flat with decrease of soil moisture. In contrast, most mud flats were distributed at high elevation so that soil moisture was not much influenced by seawater. The backscattering coefficient in mud flat seemed to have a relationship with the density of tidal channel. In addition, lowering backscattering coefficients in the all Ganghwa tidal flat was observed when surface remnant water increased according to the amount of rainfall. The correlation between backscattering coefficient, coherence and sediment environment factors in the Ganghwa tidal flat was investigated. In the future, more quantitative spatial analysis will be helpful to well understand the sedimentary influence of various sediment environment factors.

Characteristic of Power Consumption for Paddle Impeller in Various Agitated Vessels (여러 가지 교반조에서 Paddle 임펠러의 교반소요동력 특성)

  • Lee, Young Sei;Kato, Yoshihito
    • Applied Chemistry for Engineering
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    • v.16 no.5
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    • pp.698-704
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    • 2005
  • Power consumption for paddle impeller in spherical and cylindrical agitated vessel was measured over a wide range of Reynolds number from laminar to turbulent flow regions. The power correlation was obtained for both spherical and cylindrical vessels, where the apparent diameter of the spherical vessel was equal to the diameter of the cylindrical vessel (height equal to its diameter and had the same volume as the spherical vessel). The power consumption well correlated with the experimental results of Nagata, et al. and Hixson-Baum. Also the critical Reynolds numbers was directly related to the transition coefficient $C_{tr}$ characterizing the transition from a laminar to a turbulent flow region in the correlation proposed here.

Green Generation and Investigation of Optical Properties of Amorphous BaTiO3 by Poling (폴링에 의한 비정질 BaTiO3 박막의 광학적 특성 조사 및 녹색광 발생)

  • Kim, Eung-Soo
    • The Journal of the Korea institute of electronic communication sciences
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    • v.15 no.1
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    • pp.39-44
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    • 2020
  • BaTiO3 thin films was deposited on the slide glass by RF sputter. We have investigated the optical properties of BaTiO3 film after corona poling process. The transmission characteristics was very good over 80% in visible region and second order nonlinear optical coefficient depends on the poling conditions. The nonlinear optical coefficient of poled BaTiO3 films was about 1.15pm/V. The relaxation of second order nonlinear optical was remained around 60% of the initial value for a long time. In addition we have observed the green light generation from BaTiO3 films.

An Experimental Study on the Effect of Air Space on the Absorption Property of Composite Absorption System (배후공기층이 복합흡음구조의 흡음특성에 미치는 영향에 관한 실험적 연구)

  • Oh, Yang-Ki
    • KIEAE Journal
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    • v.1 no.2
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    • pp.47-54
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    • 2001
  • Single sound absorbers such as porous materials, panels, and Helmholts resonators have limited performance with some extents of frequency region. For example, porous materials do not attenuate low frequency sounds, while panels do not absorb high frequency sounds. Composite absorption structure with coverings, porous materials, and air gaps are an alternative for wide band sound absorption. Slits, panels, perforated panels are those materials for coverings, glass wool, mineral wool, polyester, and polyurethane are frequently used porous materials. Air gap between the porous material and background surface is one of major factors which governs the absorption characteristics of composite absorption structures, especially in the low frequency area. Calculations and measurements show that the absorption coefficients of composite absorption structure, in mid and low frequency bands, are getting higher with increased air gaps. Perforated panels rather than slits and panels are good coverings with higher number as far as absorption coefficient is concerned. Perforated panels with porous materials and 37 cm of air gaps in background have high absorption coefficients for all frequency bands, above 0.7 to 1.0. All measurements are performed in reverberation chamber, Mokpo National University, according to ISO 354 and ISO 3382.

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A Study of an Airfoil for Optimal Aerodynamic Performance of Flapping Motion (Flapping운동의 최적공력성능을 위한 익형 연구)

  • Lee J. S.;Kim C.;Rho O. H.
    • Journal of computational fluids engineering
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    • v.8 no.2
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    • pp.24-32
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    • 2003
  • In this work, we propose a new idea of flapping airfoil design for optimal aerodynamic performance from detailed computational investigations of flow physics. Generally, flapping motion which is combined with pitching and plunging motion of airfoil, leads to complex flow features such as leading edge separation and vortex street. As it is well known, the mechanism of thrust generation of flapping airfoil is based on inverse Karman-vortex street. This vortex street induces jet-like flow field at the rear region of trailing edge and then generates thrust. The leading edge separation vortex can also play an important role with its aerodynamic performances. The flapping airfoil introduces an alternative propulsive way instead of the current inefficient propulsive system such as a propeller in the low Reynolds number flow. Thrust coefficient and propulsive efficiency are the two major parameters in the design of flapping airfoil as propulsive system. Through numerous computations, we found the specific physical flow phenomenon which governed the aerodynamic characteristics in flapping airfoil. Based on this physical insight, we could come up with a new kind of airfoil of tadpole-shaped and more enhanced aerodynamic performance.

Investigation on glass transition temperature of low density polyethylene by the characteristics of temperature dependent linear expansion (선팽창 온도특성에 의한 저밀도 폴리에틸렌의 유리 천이온도에 대한 고찰)

  • 김봉흡;강도열;김재환
    • 전기의세계
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    • v.30 no.7
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    • pp.441-447
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    • 1981
  • As a preceeding work for the study on dielectric characterstics of a kind of low density polyethylene introduced morphological change by mechanical method, glass transition temperature which is regarded as a macroscopic aspect for relaxation of molecular chain segments has been observed by means of temperature dependent dilatometric measurement. The origina specimen clearly shows two knees which correspond to two peaks (.gamma. and .betha. peak) in the intenal friction measurement, suggesting the existence of separated glass transition temperatures at 150.deg.k and 260.deg.k respectively. On the specimen irradiated to 100 Mrad both glass transition temperatures tend to shift towards high temperature sides because of crosslinking by irradiation. furthemore an evidence can be seen that radiation effect, even in amorphous phase, is also slelctive depending on slight morphological differences. The specimen extended to four times in length shows a peculiar nature such as negative linear thermal expansion coefficient increasing with temperature between 220.deg.k and ambient temperature and that this fact is interpreted by considering that c axis of the lattice aligns along the extended direction by drawing, further c axis inherently possesses the characteristics of negative linear thermal expansion coefficient. For the observations that the relatively small positive linear expansion on the specimen extended to ca. two times as well as the part below 220.deg.k of the specimen extended to four times, it is considered for the reason of the facts that the incompletely oriented region indicated as the middle part of Peterlin's model tends to restore partially to orginal arrangement-a kind of phase transition-as increasing with temperature.

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