• Title/Summary/Keyword: chemical composition analysis

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The Chemical COmposition Analysis by AES and XPS of PbTiO$_3$ Thin Films Fabricated by CVD (화학증착법에 의해 제조된 PbTiO$_3$ 박막의 AES와 XPS에 의한 조성분석)

  • Soon Gil Yoon;Ho Gi Kim
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1989.06a
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    • pp.83-86
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    • 1989
  • Lead titanate thin films with a perovskite structure were successfully structure were successfully fabricated on titanium substrate by Chemical Vapour Deposition(CVD). Analyses of Auger Electron Spectroscopy(AES) and X-ray Photoelectron Spectroscopy (XPS) have been performed in order to find a chemical composition of lead titanate films. The analysis of chemical composition by AES and XPS was investigated for variations of deposition temperature and Ti(C$_2$H$_{5}$O)$_4$ fractions. The chemical composition of PbTiO$_3$by XPS analysis was almost constant regardless of deposition parameters and the comparison of chemical composition by AES and XPS was performed.d.

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Relationship between Classification of Sa-Sang Constitutional Medicine and Chemical Composition of Samgye-Tang Ingredients and Other Food (삼계탕 재료 및 각종 식품의 사상의학적 분류와 화학조성과의 상관관계)

  • 유익종;전기홍;박우문;조혜연;최성유
    • Food Science of Animal Resources
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    • v.21 no.2
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    • pp.97-102
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    • 2001
  • The characteristic fitness of food to each Sa-sang constitution and the relationship between Han-Yeoul characteristics and chemical composition after classifying Samgye-tang ingredients and other food into Ohn-Yeoul-Ryang-Han characteristic were assessed. When the suitable constitution to the each characteristic was investigated after classifying Samgye-tang ingredients and other food into Han, Ryang, Pyound, Ohn and Yeoul of which fitness case for Soeumin was 44∼63% but fitness case for Soyangin and Taeyangin was only 0∼18%. When the relationship between Samgye-tang ingredients and other food classified into Ohn-Yeoul-Ryang-Han and chemical composition of fatty acid, amino acid, vitamin and mineral was investigated, the value of correlation coefficient was extremely low. There was not the relationship between chemical composition and Han-Yeoul classification. Therefore it should be further investigated the relationship between characteristic and chemical composition by additional analysis index.

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The Effect of Chemical Composition on a Hardenability of Steel (강의 화학조성이 경화능에 미치는 영향)

  • Shin, Seung Ho;Chae, Jae Ho
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.4
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    • pp.40-46
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    • 1989
  • The hardenability of steel is related to its chemical composition. About this relationship, multiple regression analysis of hardenability data was proposed to explain the effect of chemical composition on a hardenability of steel. To establish the formula for calculation hardenability, given hardenability curve(U.S.S. Atlas) were quantitatively analyzed by multiple regression analysis program of computer. The established hardenability model was applied to predict the hardenability of commercial steel fair well. The effect of chemical composition was also expressed quantitatively.

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Chemical Analysis of Woody Resource Seperated from Municipal Soild Waste (도시 고체 폐기물에서 분리한 목질계 자원의 화학적 분석)

  • Shin, Soo-Jeong;Park, Jong-Moon;Choi, Tea-Ho;Kim, Byung-Ro;Cho, Dae-Haeng;Kim, Yong-Hwan
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2011.10a
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    • pp.43-47
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    • 2011
  • In woody waste separated from municipal solid waste, medium density fiberboard was major contributors with particleboard, paper, plywood and log, with different composition based on collected period. In chemical compositional analysis of woody waste, it was similar to softwood based on carbohydrate composition analysis. Based on the carbohydrate composition, saccharified solution from MWW could be good resource for biorefinery.

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Thermal and Mechanical Properties of Epoxy Composition Containing Modified Halosite Nanotubes with Silane Coupling Agent (실란 커플링제를 이용하여 개질한 할로이사이트 나노튜브가 함유된 에폭시 조성물의 열적·기계적 물성)

  • Kim, TaeHee;Lim, Choong-Sun;Kim, Jin Chul;Seo, Bongkuk
    • Journal of Adhesion and Interface
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    • v.18 no.2
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    • pp.68-74
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    • 2017
  • Epoxy resins are widely used in various fields due to their excellent thermal, mechanical and chemical properties. In order to improve the mechanical properties of the epoxy composition after curing, various materials are mixed in the epoxy resin. Among the nano materials, CNT is the most widely used. However, CNT has limitations in terms of manufacturing process and manufacturing cost. Therefore, there is a growing interest in naturally occurring HNTs having similar structure to that of CNT. In this study, the thermal and mechanical properties of epoxy compositions containing HNTs treated with two types of silane compounds were investigated. The mechanical properties of silane-treated HNT were measured by using a universal testing machine. The differential scanning calorimeter (DSC), thermogravimetric analysis (TGA), and thermomechanical analysis (TMA) were used to measure thermal properties. As a result of the above tests, when the HNT was surface-treated with aminosilane, the tensile strength of the epoxy composition containing the HNT was higher than that of the epoxy composition containing epoxy silane treated HNT. The linear thermal expansion coefficients (CTE) obtained from the thermomechanical analysis of the two epoxy compositions for the comparison of dimensional stability showed that the HNT composition treated with aminosilane showed a lower value of CTE than that of epoxy composition including the pristine HNT.

Chemical Characterization of Industrial Hemp (Cannabis sativa) Biomass as Biorefinery Feedstock

  • Shin, Soo-Jeong;Han, Gyu-Seong;Choi, In-Gyu;Han, Sim-Hee
    • Korean Journal of Plant Resources
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    • v.21 no.3
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    • pp.222-225
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    • 2008
  • Chemical composition and enzymatic saccharification characteristics of hemp woody core were investigated by their chemical composition analysis and enzymatic saccharification with commercially available cellulases (Celluclast 1.5L and Novozym 342). Hemp woody core have higher xylan and lower lignin contents than its bast fiber. Based on hemicelluloses and lignin composition, hemp woody core is similar with hardwood biomass. However, cellulose was more easily converted to glucose than xylan to xylose and this trend was confirmed both hemp woody core and yellow poplar. Hemp woody core biomass shows higher saccharification than yellow poplar (hardwood biomass) based on cellulose and xylan hydrolysis. With easier enzymatic saccharification in cellulose and xylan, and similar chemical composition, hemp woody core have better biorefinery feedstock characteristics than hardwood biomass.

Synthesis and Structural Characterization of the One-Dimensional Cadmium(II) Complex with Thiocyanate and 4-Methylimidazole Ligands (티오시아네이트 및 4-메틸이미다졸 리간드로 구성된 1차원 카드뮴(II) 착물의 합성과 구조 분석)

  • Moon, Hyoung-Sil;Kim, Chong-Hyeak;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.14 no.6
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    • pp.535-539
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    • 2001
  • One-dimensional coordination polymer of cadmium(II) complex, $[Cd(SCN)_2(C_4H_6N_2]_n$, has been prepared and characterized by X-ray single crystallography. Structure analysis reveals that each cadmium(II) atom is six-coordinated in distorted octahedral fashion with $CdS_2N_4$ composition. $CdS_2N_4$ composition contains two S and two N atoms from four thiocyanates and tow N atoms from two 4-methylimidazole ligands. Central cadmium(II) atoms are run in parallel to the a-axis and are doubly bridged with neighboring cadmium(II) atoms by the thiocyanate and isothiocyanate ligands. Thus, this complex has a one-dimensional polymer structure in which the 4-methylimidazole is in the trans conformation.

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물리정수법에 의한 형광 X선분석과 만장굴석주의 연대측정

  • 택훈
    • Proceedings of the Speleological Society Conference
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    • 1993.07a
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    • pp.163-172
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    • 1993
  • Cheju island is situated at about 90km south of southern most tip of the Korean peninsula. Its shape is an ellips with size of 80$\times$40$km^2$, and it is characterized by a symmetrical form whose peak is Mt. Halla (1950m). Major chemical composition of the rock samples from Manjang gul cave is determined by XRF using the fundamental parameter method consisting of fully auto quantitative analysis, semi quantitative analysis (order estimation) and group quantitative analysis. Judging from chemical composition ($SiO_2 = 53.07Wt% Fe_2 O_3=11.34Wt%, MgO=6.48Wt%, Na_2 O=3.07Wt%, K_2 O=1.05Wt%$), this rocks may belong to non alkalic basalt. K-Ar ages of two rocks samples from the Manjang gul cave are also determined. The discrepancy of K-Ar ages is found. They are 0.03Ma and 0.42Ma, respectively. This paper describes some problems experienced in dating young volcanic rocks and then discusses chemical composition, X-ray fluorescence analysis and the age of the formation of a lava tunnel such as Manjang gul cave in cheju Island.

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물리정수법에 의한 형광 X선분석과 만장굴석주의 연대측정

  • 택훈
    • Proceedings of the Speleological Society Conference
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    • 1994.11a
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    • pp.108-109
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    • 1994
  • Cheju island is situated at about 90km south of southern most tip of the Korean peninsula. Its shape is an ellips with size of 80$\times$$40km^2$, and it is characterized by a symmetrical form whose peak is Mt. Halla (1950m). Major chemical composition of the rock samples from Manjang gul cave is determined by XRF using the fundamental parameter method consisting of fully auto quantitative analysis, semi quantitative analysis (order estimation) and group quantitative analysis. Judging from chemical composition ($SiO_2=53.07Wt% Fe_2O_3=11.34Wt%, MgO=6.48Wt%, Na_2O=3.07Wt%, K_2O=1.05Wt%$), this rocks may belong to non alkalic basalt. K-Ar ages of two rocks samples from the Manjang gul cave are also determined. The discrepancy of K-Ar ages is found. They are 0.03Ma and 0.42Ma, respectively. This paper describes some problems experienced in dating young volcanic rocks and then discusses chemical composition, X-ray fluorescence analysis and the age of the formation of a lava tunnel such as Manjang gul cave in cheju Island.

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