• 제목/요약/키워드: chemical analysis tests

검색결과 419건 처리시간 0.031초

Antimicrobial Efficacy of Penicillium amestolkiae elv609 Extract Treated Cotton Fabric for Diabetic Wound Care

  • Rozman, Nur Amiera Syuhada Binti;Hamin, Nurhanis Syafiqah Binti Mohd Nor;Ring, Leong Chean;Nee, Tan Wen;Mustapha, Mahfuzah Binti;Yenn, Tong Woei
    • Mycobiology
    • /
    • 제45권3호
    • /
    • pp.178-183
    • /
    • 2017
  • Diabetes mellitus is a chronic disorder which affects millions of population worldwide. Global estimates published in 2010 reported the world diabetic prevalence as 6.4%, affecting 285 million adults. Foot ulceration and wound infection are major forms of disabilities arising from diabetic diseases. This study was aimed to develop a natural antimicrobial finishing on medical grade textile that meets American Association of Textiles Chemists and Colorists (AATCC) standard. The textile samples were finished with the ethanolic extract of Penicillium amestolkiae elv609, an endophytic fungus isolated from Orthosiphon stamineus Benth (common name: cat's whiskers). Endophyte is defined as microorganism that reside in the living plant tissue, without causing apparent disease symptom to the host. The antimicrobial efficacy of the ethanolic extract of P. minioluteum was tested on clinical pathogens isolated from diabetic wound. The extract exhibited significant inhibitory activity against 4 bacteria and 1 yeast with the minimal inhibitory concentration ranged from 6.25 to 12.5 mg/mL. The results indicate different susceptibility levels of the test microorganism to the ethanolic extract. However, the killing activity of the extract was concentration-dependent. The finished medical textile showed excellent antimicrobial efficacy on AATCC test assays. All the microbial cultures treated with the textile sample displayed a growth reduction of 99.9% on Hoheinstein Challenge Test. The wash durability of the finished textile was found good even after 50 washes with commercial detergent. Besides, the gas chromatography mass spectrometry analysis showed that 6-octadecenoic acid and diethyl phthalate were the main bioactive constituents of the extract. In conclusion, the developed medical textile showed good antimicrobial efficacy on laboratory tests. This work can be extended to in vivo trials for developing healthcare textile products for antimicrobial applications.

PVA/H-β zeolite mixed matrix membranes for pervaporation dehydration of isopropanol-water mixtures

  • Huang, Zhen;Ru, Xiao-Fei;Guo, Yu-Hua;Zhu, Ya-Tong;Teng, Li-Jun
    • Membrane and Water Treatment
    • /
    • 제10권2호
    • /
    • pp.165-178
    • /
    • 2019
  • Mixed matrix membranes (MMMs) of poly (vinyl alcohol) (PVA) containing certain amounts of H-${\beta}$ zeolite for pervaporation were manufactured by using a solution casting protocol. These zeolite-embedded membranes were then characterized with scanning electron microscope (SEM), X-ray diffraction (XRD) and swelling tests. The membrane separation performance has been examined by means of isopropanol (IPA) dewatering from its highly concentrated aqueous solutions via response surface methodology (RSM). The results have demonstrated that the influences of feed IPA composition (85-95 wt.%), feed temperature ($50-70^{\circ}C$), zeolite loading (15-25 wt.%) and their interactive influences are all statistically significant on both pervaporation flux ($398-1228g/m^2{\cdot}h$) and water/isopropanol separation factor (617-2001). The quadratic models based on the RSM analysis have performed excellently to correlate experimental data with very high determination coefficients and very low relative standard deviations. The optimal pervaporation predictions given by using the RSM models demonstrate a total flux of $953g/m^2{\cdot}h$ and separation factor of 1458, and are excellently verified by experimental results. As reflected by these results, PVA MMMs embedded with hydrophilic $H-{\beta}$ zeolite entities have performed considerably better than its pure counterpart and indicated great potential for isopropanol dehydration applications.

Effect of damage on permeability and hygro-thermal behaviour of HPCs at elevated temperatures: Part 1. Experimental results

  • Gawin, D.;Alonso, C.;Andrade, C.;Majorana, C.E.;Pesavento, F.
    • Computers and Concrete
    • /
    • 제2권3호
    • /
    • pp.189-202
    • /
    • 2005
  • This paper presents an analysis of some experimental results concerning micro-structural tests, permeability measurements and strain-stress tests of four types of High-Performance Concrete, exposed to elevated temperatures (up to $700^{\circ}C$). These experimental results, obtained within the "HITECO" research programme are discussed and interpreted in the context of a recently developed mathematical model of hygro-thermal behaviour and degradation of concrete at high temperature, which is briefly presented in the Part 2 paper (Gawin, et al. 2005). Correlations between concrete permeability and porosity micro-structure, as well as between damage and cracks' volume, are found. An approximate decomposition of the thermally induced material damage into two parts, a chemical one related to cement dehydration process, and a thermal one due to micro-cracks' development caused by thermal strains at micro- and meso-scale, is performed. Constitutive relationships describing influence of temperature and material damage upon its intrinsic permeability at high temperature for 4 types of HPC are deduced. In the Part II of this paper (Gawin, et al. 2005) effect of two different damage-permeability coupling formulations on the results of computer simulations concerning hygro-thermo-mechanical performance of concrete wall during standard fire, is numerically analysed.

멤브레인 LNG 저장탱크용 STS304L의 인장 및 피로강도 (Tensile and Fatigue Strengths of STS304L for LNG Membrane Storage Tank)

  • 나성현;김영균;김재훈
    • 한국안전학회지
    • /
    • 제31권4호
    • /
    • pp.9-14
    • /
    • 2016
  • STS304L of membrane structure has been used for a LNG storage tank and has exposed long time under the cryogenic temperature. The purposes of this study are to evaluate the mechanical properties of base and used materials for STS304L of membrane. The tensile and high cycle fatigue tests were investigated for STS304L of membrane used over 20 years at room temperature and $-162^{\circ}C$. In addition, the test of base STS304L was performed in order to compare with used material properties. The chemical composition and phase change were investigated from EDS and XRD. From results of tensile test, yield and ultimate tensile strengths of used STS304L are smaller than those of base STS304L. S-N curves were obtained from fatigue tests at both temperatures. Also, P-S-N curves were presented with statistical method recommend by JSME-S002. Fractography was conducted for analysis of fracture mechanisms.

도시하수중 유기인자의 상호기관에 관한 연구 (A Study on the Correlation of Organic Factors in Municipal Waste Water)

  • 황상용;손종열;우완기
    • 한국환경보건학회지
    • /
    • 제16권2호
    • /
    • pp.55-61
    • /
    • 1990
  • Laboratory methods commonly used today are biochemical oxygen demand, chemical oxygen demand, and total organic carbon. Establishment of constant relationships among the various measures of organic content depends primarily on the nature of the wastewater and its source. Of all the measures, the most difficult to correlate to the others is the BODs test, because of the problems associated with biological tests. The results were summarized as follwos, 1. For typical municipal wastes, however, the SBOD$_{5}$/SCOD$_{cr}$ ratio varies from 0.14 to 0.34(mean 0.21), SBOD$_{5}$/STOC ratio varies from 0.35 to 1.19(mean 0.69) 2. Correlation analysis between the SBOD$_{5}$ and SCOD$_{cr}$ gave good correlation coefficient r = 0.903 and the equation Y = 3.756X + 16,221 was obtained. 3. The correlation between the SBOD$_{5}$ and STOC was well presented with equation : Y = 1,070X + 7,637, and also correlation coefficient r = 0.821 4. The correlation between the SCOD$_{cr}$ and STOC was well presented with equation : Y = 0.256X +5.513 and also correlation coefficient r = 0.816. 5. Because of the rapidity with which the TOC test can be conducted, it is anticipated that more use will be made of these tests in the future.

  • PDF

Audit Committee, Board of Independent Commissioner, and Institutional Ownership on Earnings Quality with Strengthening of Earnings Growth

  • Muhammad Wahyuddin ABDULLAH;Muh. IKBAL;Raodahtul JANNAH;Andi Yustika Manrimawagau BAYAN;Hadriana HANAFIE
    • 유통과학연구
    • /
    • 제22권6호
    • /
    • pp.11-22
    • /
    • 2024
  • Purpose: Thisstudy aimsto analyze the distribution of audit committee, independent board of commissioners, and institutional ownership on earnings quality with strengthening earnings growth. Research Design data and Methodology: This quantitative research uses a comparative causal approach. The research population consists of manufacturing companies in the basic and chemical industry sector listed on the Indonesia Stock Exchange in 2016-2022. Samples were obtained as many as 112 using purposive sampling method. The analysis technique to test the hypothesis uses multiple linear regression tests and moderation tests with an absolute difference approach. Results: The results showed that the audit committee and board of commissioners provide a significant positive distribution on earnings quality, while institutional ownership provides a significant negative distribution on earnings quality. Earnings growth strengthens the distribution of the audit committee and independent board of commissioners on earnings quality. However, earnings growth does not strengthen the distribution of institutional ownership on earnings quality. Conclusions: Audit oversight from audit committee and management performance oversight from the independent board of commissioners improves the credibility of earnings quality. Management oversight from institutional ownership reduces earnings quality. The interaction of earnings growth with maximum supervision can improve earnings quality, except for supervision from institutional ownership.

활성탄소섬유의 기공구조가 기계적 특성에 미치는 영향 (Effect of Pore Structure of Activated Carbon Fiber on Mechanical Properties)

  • 최윤정;이영석;임지선
    • 공업화학
    • /
    • 제29권3호
    • /
    • pp.318-324
    • /
    • 2018
  • 본 연구에서는 물리적 활성화법인 수증기 활성화법을 이용하여 PAN (Polyacrylonitrile)계 활성탄소섬유를 제조하였다. 활성화는 온도와 시간을 변수로 하였으며, 활성화 온도(700, 750, $800^{\circ}C$)에 도달하였을 때 200 mL/min의 수증기 유량의 조건으로 PAN 탄소섬유의 활성화를 진행하였다. 제조된 활성탄소섬유의 기공구조를 분석하기 위하여 질소가스의 흡 탈 등온선을 통한 비표면적($S_{BET}$) 측정과 표면분석을 위한 AFM 분석을 실시하였다. 또한 인장시험을 실시하여 활성화 결과 형성된 기공구조가 섬유의 기계적 특성에 미치는 영향을 고찰하였다. 그 결과, 활성화 후 섬유의 비표면적($S_{BET}$)은 $448{\sim}902m^2/g$의 값을 나타냈으며, 인장강도는 58.16~84.92%, 탄성계수는 69.81~83.89%의 감소를 보였다.

디젤엔진 배출가스 질소산화물 저감을 위한 Solid SCR의 반응률에 관한 연구 (A Study on Reaction Rate of Solid SCR for NOx Reduction of Exhaust Emissions in Diesel Engine)

  • 이호열;윤천석;김홍석
    • 한국자동차공학회논문집
    • /
    • 제21권6호
    • /
    • pp.183-194
    • /
    • 2013
  • Liquid urea based SCR has been used in the market to reduce NOx in the exhaust emission of the diesel engine vehicle. This system has several problems at low temperature, which are freezing below $-12^{\circ}C$, solid deposit formation in the exhaust, and difficulties in dosing system at exhaust temperature below $200^{\circ}C$. Also, it is required complicated exhaust packaging equipment and mixer due to supply uniform ammonia concentration. In order to solve these issues, solid urea, ammonium carbonate, and ammonium carbamate are selected as ammonia sources for the application of solid SCR. In this paper, basic research on reaction rate of three ammonia-transporting materials was performed. TGA (Thermogravimetric Analysis) and DTA (Differential Thermal Analysis) tests for these materials are carried out for various heating conditions. From the results, chemical kinetic parameters such as activation energy and frequency factor are obtained from the Arrhenius plot. Additionally, from test results of DSC (Differential Scanning Calorimeter) for these materials, chemical kinetic parameters using the Kissinger method are calculated. Activation energies of solid SCR from this experiment are compared with proper data of literature study, then obtained data of this experiment are used for the design of reactor and dosing system for candidate vehicle.

미생물에 의한 축산 폐기물 퇴비화에 미치는 영향 (Effect on Livestock Manure Composting by the Enriched Microbial Population)

  • 신혜자
    • 생명과학회지
    • /
    • 제12권2호
    • /
    • pp.129-135
    • /
    • 2002
  • 여러 종류의 호열성, 호기성 간균(Bacillus genus)군, 중금속 leaching 미생물군(Thiobacillus, T. ferooxidans), 그리고 여러 가지 난분해성 물질을 분해하는 미생물군 (Pseudomonas genus)을 활용하여 퇴비화의 조건을 연구하고 이를 이용하여 축산폐기물의 퇴비화에 미치는 효과를 연구하였다. 35∼40의 C/N비, 50∼65%의 함수율 범위에서 실험실용 회전드럼형 반응조에서의 퇴비화는 온도상승이 수동식 반응조보다 낮으며 느리게 일어났다. 퇴비화 후 성분분석에서 높은 수준의 광물질을 함유하는 것으로 화학비료 대체효과를 보여주며 퇴비화 전후 중금속 분석에서 As는 모든 퇴비에서, Cr은 돈분, ph은 축분, Hg은 계분, 그리고 Cu는 축분퇴비에서 규제값 이하를 보여주었다. 여러 가지 부숙도 분석에서 퇴비의 숙성도를 나타내었다. SS 또는 EMB agar plate을 이용한 살모넬라균과 대장균의 검사에서 병원균에 대한 퇴비의 안전성이 확인되었다. 이러한 결과는 금속 및 다른 난분해성 물질을 생분해하는 미생물을 투입하여 퇴비의 중금속감소와 퇴비화 속도증가의 가능성을 시사한다.

C12E8 비이온 계면활성제 수용액에 의한 탄화수소 오일의 가용화에 관한 연구 (Solubilization of Hydrocarbon Oils by C12E8 Nonionic Surfactant Solution)

  • 임종주
    • Korean Chemical Engineering Research
    • /
    • 제45권3호
    • /
    • pp.219-225
    • /
    • 2007
  • 비이온 계면활성제 $C_{12}E_8$ 수용액의 탄화수소 오일에 대한 가용화도(equilibrium solubilization capacity)를 $30^{\circ}C$에서 기체 크로마토그래피(GC)를 이용하여 측정하였다. 탄화수소 오일의 가용화도를 실험에 사용한 계면활성제의 농도로 나눈 값으로 표시한 molar solubilization ratio(MSR)는 순수한 단일 성분의 탄화수소 오일 경우, 탄화수소 오일의 탄소수(ACN)가 증가함에 따라 거의 선형적으로 감소함을 알 수 있었다. 한편 탄화수소 오일의 이성분 시스템은 사용한 두 탄화수소 오일의 탄소수(alkane carbon number, ACN) 차이에 따라 선택적 가용화 혹은 비선택적 가용화 경향을 나타내었다. 본 연구에서 가용화도 실험을 수행한 n-octane/n-nonane과 n-nonane/n-decane 혼합물 시스템의 경우, 비선택적 (non-selective) 가용화 경향을 나타내었으며, 반면에 n-octane/n-decane 혼합물 시스템의 경우에는 선택적(selective) 가용화 경향을 따르는 것을 GC 분석 결과로부터 확인할 수 있었다.