• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.291-292
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• 2006

A steel/cemented carbide couple is selected to generate a tough/hard two layers material. Sintering temperature and composition are deduced from phase equilibria, and experimental studies are used to determine optimal conditions. Liquid migration from the hard layer to the tough one is observed. Microstructure evolution during sintering of the tough material (TEM, SEM, image analysis) evidences coupled mechanisms of pore reduction and WC dissolution. Liquid migration, as well as interface crack formation due to differential densification are limited by suitable temperature and time conditions.

• Tribology and Lubricants
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• 제11권5호
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• pp.26-30
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• 1995

Sliding experiments have been conducted on alumina and silicon carbide ceramics. Wear and friction data of both materials indicate that wear proceeds in two distinct stages. The wear occurs by a relatively mild plastic-grooving process in the initial stage, but eventually gives way to a severe grain pull-out process after a defined period of sliding test. The datails of the transition mechanism are presented. The effects of grain size and second phase particle on the wear transition are also presented.

• Journal of Welding and Joining
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• 제19권1호
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• pp.95-103
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• 2001

The properties of the detonation sprayed cermet coating are investigated through the mechanical, corrosion and erosion test. The test results are also compared with the properties of the substrate materials, STS 329J1, dual phase stainless steel and the plasma sprayed cermet coatings. The two kinds of carbide cermet power, WC+NiCr, Cr$_3$C$_2$+NiCr were used in this experiment. The experimental results showed that the anti-corrosive and anti-erosive properties of the detonation sprayed cermet coatings are superior to the plasma sprayed cermet coatings. The WC+NiCr cermet coating appears to be more effective than Cr$_3$C$_2$+NiCr cermet coating in abrasive erosion environment, whereas the Cr$_3$C$_2$+NiCr cermet coatings are more effective in cavitation erosion environment.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.631-632
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• 2006

Cr-C-Ni composites were synthesized in situ from elemental powders of Cr, Ni and C by high energy milling followed by reactive sintering. The milled powders with the grain size in nano-scale were pressed to compacts and sintered. During the following thermal treatment at first the chromium carbide was formed and then the $Cr_3C_2-Ni$ cermets were sintered in one cycle. The interface between the binder phase and the carbide grains of the in situ composite has a good bonding strength as it is not contaminated with oxidation films or other detrimental surface reactions.

• 한국분말재료학회지
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• 제21권6호
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• pp.467-472
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• 2014

RBSC (reaction-bonded silicon carbide) represents a family of composite ceramics processed by infiltrating with molten silicon into a skeleton of SiC particles and carbon in order to fabricate a fully dense body of silicon carbide. RBSC has been commercially used and widely studied for many years, because of its advantages, such as relatively low temperature for fabrication and easier to form components with near-net-shape and high relative density, compared with other sintering methods. In this study, RBSC was fabricated with different size of SiC in the raw material. Microstructure, thermal and mechanical properties were characterized with the reaction-sintered samples in order to examine the effect of SiC size on the thermal and mechanical properties of RBSC ceramics. Especially, phase volume fraction of each component phase, such as Si, SiC, and C, was evaluated by using an image analyzer. The relationship between microstructures and physical properties was also discussed.

• 한국세라믹학회:학술대회논문집
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• 한국세라믹학회 2003년도 춘계총회 및 연구발표회 초록집
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• pp.69.1-69
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• 2003

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 1994년도 춘계학술대회강연 및 발표대회 강연및 발표논문 초록집
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• pp.33-33
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• 1994

• 한국재료학회지
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• 제11권6호
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• pp.502-507
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• 2001

일방향응고법으로 IN792+Hf 초내열합금의 응고속도에 따른 응고거동의 변화에 대해 연구하였다. 조직관찰을 통해 각 상의 응고과정과 석출거동을 분석하였다 일방향응고시 응고속도가 감소하면 문자형의 탄화물은 면상 탄화물로 변화하였고 ${\gamma}$상과 탄화물의 결합은 탄화물의 수지상 성장에 의한 것임을 확인할 수 있었다. 긴 막대형상의 탄화물이 0.5$\mu\textrm{m}$/s의 응고속도에서 입계를 따라 형성되었으며 잔류액상지역에서 ${\gamma}$'형성원소가 풍부한 구역과 고갈된 구역이 발견되었다. 공정 ${\gamma}$/${\gamma}$'은 형성원소가 풍부한 구역에서 핵생성하였으며 공정 ${\gamma}$/${\gamma}$'의 형성은 잔류액상지역의 (Ti+Hf+Ta+W)/Al 비율을 높여 η상의 석출을 유발하였다. 느린 응고속도에서는 잔류액상지역으로부터의 충분한 역확산으로 (Ti+Hf+Ta+W)/Al 비율이 낮아져 η상의 석출이 억제되었다.

• 접착 및 계면
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• 제10권1호
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• pp.30-34
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• 2009

Two-phase 복합재료 계에서 성형압력이 열전도도에 미치는 영향을 고찰하였다. Polypropylene (PP) 고분자에 열전도성 필러인 Silicon carbide (SiC)를 40 vol% 첨가하여 압력을 0 MPa부터 20 MPa까지 시키면서 PP/SiC 복합재료의 계면과 열전도도의 변화를 관찰하였다. PP/SiC (40 vol%)에서 압력을 0에서 20 MPa를 증가시킴에 따라 복합재료 내부의 기포가 적어지고 고분자-필러와 필러-필러 계면에서의 접촉이 용이해져 포논산란이 감소되고 열전도도는 1.31 W/mK에서 1.86 W/mK로 약 40% 증가함을 확인하였다. 실험을 통하여 얻어진 열전도도 값과 Maxwell식과 Agari식을 이용한 Two-Phase계의 열전도도 예측값을 비교한 결과, 필러간의 상호작용을 고려하는 Agari예측식의 경우에 실험결과와 잘 일치하는 것을 확인하였다.

• Corrosion Science and Technology
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• 제2권3호
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• pp.117-126
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• 2003

Due to excellent corrosion resistance and mechanical properties, austenitic stainless steel is widely used as the material for chemical plants. nuclear power plants, and food processing facilities. But, the zone affected by heat in the range of 400 to $800^{\circ}C$ during welding loses corrosion resistance and tensile strength since Cr-carbide precipitation like $Cr_{23}C_6$ forms at the grain boundary and thereby takes place the intergranular corrosion. In this study, AISI 304 stainless steel with the added Nb of 0.3 to 0.7 wt% was solutionized at $1050^{\circ}C$ and sensitized at $650^{\circ}C$. Specimen was welded by MIG. The phase and the microstructure of the specimens were examined by an optical microscope, a scanning electron microscope, and a x-ray diffractometer. The corrosion characteristics of specimens were tested by electrolytic etching and by double loop electrochemical potentiokinetic reactivation method(EPR) in the mixed solution of 0.5M $H_2SO_4$ + 0.01M KSCN. The melting zone had dendritic structure constituted of austenitic phase and $\delta$-ferrite phase. Cr carbide at the matrix did not appear, as Nb content increased. At the grain boundaries of the heat affected zone, the precipitates decreased and the twins appeared. The hardness increased, as Nb content increased. The hardness was highest in the order of the heat affected zone>melted zone>matrix. According to EPR curve, as the Nb content decreased, the reactivation current density(Ir) and the activation current density(la) were highest in the order of the melted zone