• 제목/요약/키워드: carbide phase

검색결과 266건 처리시간 0.027초

전기화학적 방법에 의한 AISI 304 스테인리스강 용접부의 내식성 평가 (A Corrosion Resistance Evaluation of Welded AISI 304 Stainless Steel by Electrochemical Methods.)

  • 백신영;김관휴
    • Journal of Advanced Marine Engineering and Technology
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    • 제14권1호
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    • pp.83-89
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    • 1990
  • Electrochemical methods have been proposed as non-destructive, rapid and quantitative means for determining the degree of sensitization associated with Chromium depleted zones surrounding precipitates of Cr carbide and formation of secondary phase in stainless steel. In this study, the specimen of AISI 304 stainless steel and its welded sections, which welded by TIG, MIG, $CO_2$ and ARC, were tested corrosion resistance by electrochemical methods in 0.5N HCl and 1N $H_2SO_4$ with or without 0.01N KSCN. The results were confirmed that electrochemical methods could be used as a test method of corrosion resistance evaluation for the welded AISI 304 stainless steel.

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원자로 압력용기 용접열영향부의 미세조직 및 재료물성 예측 (Estimation of Microstructures and Material Properties of HAZ in SA508 Reactor Pressure Vessel)

  • 이승건;김종성;진태은
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 춘계학술대회논문집A
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    • pp.138-143
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    • 2001
  • To perform the rigorous integrity evaluation of RPV, it is necessary to consider metallurgical factors such as microstructure evolution during multi-pass welding process and PWHT. The microstructures of the heat affected zone(HAZ) of SA508 steel were predicted by a combination of simulated thermal analysis and a simple kinetic models for austenite grain growth and austenite-ferrite transformation. Phase equilibrium of SA508 steel were calculated using a Thermo-Calc package. Carbide growth in th HAZ were predicted by a empirical model, taking into account the predicted microstructure evolution.

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수산 탄탈륨 용액을 이용한 초미립 TaC 분말의 합성 (Synthesis of Ultrafine TaC Powders Using Tantalum Oxalate Solution)

  • 권대환;홍성현;김병기
    • 한국재료학회지
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    • 제13권12호
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    • pp.806-811
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    • 2003
  • Ultrafine TaC powders were synthesised by spray drying using tantalum oxalate solution. The spray dried powders were spherical shape and less than 30 $\mu\textrm{m}$ in size. The powders calcined at 500 and X$700^{\circ}C$ showed amorphous structures and $Ta_2$$O_{5}$ phase was obtained by calcining at $700^{\circ}C$. The particle size and shape remains constant after calcination. The calcined spherical powders were composed of an agglomerate of primary particles under 50 nm in size. The complete formation of TaC could be achieved by heat treatment at $1050^{\circ}C$ for 6 hrs. The observed size of TaC powders by TEM was less than 200 nm.

Si(100)기판상에 3C-SiC결정성장 (Crystal growth of 3C-SiC on Si(100) Wafers)

  • 정연식;정귀상
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2002년도 하계학술대회 논문집 C
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    • pp.1593-1595
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    • 2002
  • Single crystal 3C-SiC(cubic silicon carbide) thin-films were deposited on Si(100) wafers up to a thickness of 4.3 ${\mu}m$ by APCVD method using HMDS(hexamethyildisilane) at $1350^{\circ}C$. The HMDS flow rate was 0.5 sccm and the carrier gas flow rate was 2.5 slm. The HMDS flow rate was important to get a mirror-like crystal surface. The growth rate of the 3C-SiC films was 4.3 ${\mu}m/hr$. The 3C-SiC epitaxial films grown on Si(100) were characterized by XRD, AFM, RHEED, XPS and raman scattering, respectively. The 3C-SiC distinct phonons of TO(transverse optical) near 796 $cm^{-1}$ and LO(longitudinal optical) near $974{\pm}1cm^{-1}$ were recorded by raman scattering measurement. The hetero-epitaxially grown films were identified as the single crystal 3C-SiC phase by XRD spectra($2{\theta}=41.5^{\circ}$).

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페로 소재로 만들어진 고크롬계 내마모재의 미세조직과 경도 (Microstructure and Hardness of High Cr Wear Resistance Materials Made by Ferro Materials)

  • 김광수
    • 한국재료학회지
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    • 제16권1호
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    • pp.5-10
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    • 2006
  • This study was performed to investigate the characteristics of the synthesized powder type ferro materials for wear resistant hardfacing. The powder type filler materials were made from ferro Cr and ferro Mn. Those ferro materials are two types, such as high carbon and low carbon contained. The alloy composed of high carbon ferro Cr and high carbon ferro Mn exhibited the best properties in terms of microstructure and hardeness for wear characteristics. Further, the alloys produced by the synthesized powders and wire type filler, were also evaluated in terms of microstructures and microhardness measurements. The results indicated that the synthesized powders displayed reasonable properties compared to commercial grade materials. The hardness value of the alloy produced by the synthesized powders were approached about 90% of the commercial grade's hardness. The hardness values of the alloys closely depended on the amount of the dissolution of the ferro Cr, the hardness and the volume of the eutectic phase.

분말 고속도공구강의 소결 조건에 따른 치밀화 거동연구 (The Effect of Sintering Parameters on the Densification Behavior of PM High Speed Steel)

  • 김용진
    • 한국분말재료학회지
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    • 제1권2호
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    • pp.190-197
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    • 1994
  • The densification behavior during a sintering of M2 and T15 grade high speed steel powder compacts was reported. Sintered densities over 98% theoretical were achieved by a liquid phase sintering in vacuum for both grades. The optimum sintering temperature range where full densification could be achieved without excessive carbide coarsening and incipient melting was much narrower in M2 than in T15 grade. The sintering response was mainly affected by the type of carbides present. The primary carbides in M2 were identified as $M_6C$ type whereas those in T15 were MC type which provides wider sintering range. The addition of elemental carbon up to 0.3% lowered the optimum sintering temperature for both grades, but had little effect on expanding the sintering range and sintered structure.

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수열합성된 Al-Cr-N-O계 도포층의 열전도 측정과 수학적 해석 (Determination of Thermal Conductivity and Numerical Analysis of Al-Cr-N-O Composites Layer Formed by Hydro-thermal Process)

  • 김마로;양소은;이종재;김병두;최용
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2014년도 추계학술대회 논문집
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    • pp.215-215
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    • 2014
  • Composites layer of Al-Cr-Ni-O system was prepared on a steel plate by hydro-thermal process at $700^{\circ}C$ for 12 hours, which phase identification and thermal conductivity were determined. The composites layer consisted of aluminum nitride, alumina, chromium carbide and aluminium, which density was $3.7kg/m^3$. The thermal conductivity of the coating layer determined by thermal data acquisition system was about 98.0 W/m/ which depended on the AlN content. Numerical modelling of the heat transfer behavior of the coating layer was well agreement with the empirical data.

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단일전구체(1,3-DSB)에 의한 저온 SiC박막 성장에 관한 연구 (A Study on the Low Temperature Growth of SiC Film with a 1,3-DSB Precursor)

  • 양재웅;노대호;윤진국;김재수
    • 한국표면공학회지
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    • 제36권2호
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    • pp.141-147
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    • 2003
  • Silicon carbide thin film was deposited in APCVD and LPCVD system with 1,3-DSB precursor 1,3-DSB is the single precursor to deposit SiC on Si at low temperature. SiC film was deposited at $850^{\circ}C$ lower than ordinary temperature ($1000~1200^{\circ}C$) in CVD process. SiC thin film glowed to high oriented (111) plane in APCVD system. In LPCVD system, SiC film groved to preferred (220) plane at same temperature. This discrepancy between preferred planes can be described by the difference of deposition mechanism. Amorphous phase and crystal defect were observed in APCVD system with the main growth mechanism of mass transport limited region. But in LPCVD system, we got the SIC film of uniform, faceted structure and high quality.

반응소결에 의한 SiC의 소결과 그 특성에 관한 연구 (초기 소결과정에서의 B4C 및 Y2O3의 첨가 영향) (Sintering of Silicon Carbide by Reaction Bonding and its Characteristics (Effect of Addition of B4C and Y2O3 in Initial Sintering Precess))

  • 백용혁
    • 한국세라믹학회지
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    • 제25권6호
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    • pp.609-614
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    • 1988
  • This study was carried out to investigate the effects of B4C or Y2O3 additives on the tendency of sintering, $\beta$-SiC synthesis and mineral phase changes by reaction bonding of SiC at 145$0^{\circ}C$. At the sintering temperature of 145$0^{\circ}C$, the additives such as B4C or Y2O3 did not improved porosity and bending strength. Added more than 1.5% of Y2O3, 0.5-0.3% of B4C, the formation of $\beta$-SiC was increased. At higher temperature above 145$0^{\circ}C$, it seems that the bodies added B4C, contained 3C form of SiC were denser than that of Y2O3 added. Because the transition of 3Clongrightarrow4Hlongrightarrow6H promoted sintering.

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전기자동차 급속 충전기를 위한 커플드 인덕터를 적용한 고효율 2상 인터리브드 벅 컨버터 설계 (High efficiency two-phase interleaved buck converter with coupled inductor design for EV rapid charger applications)

  • 강현지;조영훈
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2019년도 추계학술대회
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    • pp.25-27
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    • 2019
  • 본 논문은 전기 자동차 급속 충전기 구현을 위한 커플드 인덕터 기반 18kW급 2상 인터리브드 벅 컨버터 설계에 관하여 설명한다. 전류 리플 및 물리적인 크기 감소를 위한 2상 커플드 인덕터와 고효율 달성을 위한 Silicon Carbide(SiC) MOSEFT 기반 2상 인터리브드 벅 컨버터의 설계에 관하여 상세히 기술한다. 제안하는 2상 인터리브드 벅 컨버터의 동작을 위하여 모의 실험과 실험을 진행하였고 이론적인 설계 방법과 실제 실험 결과가 일치하는 것을 확인하였다.

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