• 제목/요약/키워드: carbide analysis

검색결과 332건 처리시간 0.023초

고내열 페라이트계 스테인레스 주강의 고온인장특성 평가 (High Temperature Tensile Properties of Heat-resistant Cast Ferritic Stainless Steels)

  • 정현경;이동근
    • 열처리공학회지
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    • 제34권1호
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    • pp.10-16
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    • 2021
  • Exhaust manifold is a very important component that is directly connected to air environment pollution and that requires strict mechanical properties such as high temperature fatigue and oxidation. Among stainless steels, the ferritic stainless steel with body-centered cubic structure shows excellent resistance of stress-corrosion cracking, ferromagnetic at room temperature, very excellent cold workability and may not be enhanced by heat treatment. The microstructural characteristics of four cast ferritic stainless steels which are high heat-resistant materials, were analyzed. By comparing and evaluating the mechanical properties at room temperature and high temperature in a range of 400℃~800℃, a database was established to control and predict the required properties and the mechanical properties of the final product. The precipitates of cast ferritic stainless steels were analyzed and the high-temperature deformation characteristics were evaluated by comparative analysis of hardness and tensile characteristics of four steels at room temperature and from 400℃ to 800℃.

Effect of different tungsten compound reinforcements on the electromagnetic radiation shielding properties of neopentyl glycol polyester

  • Can, Omer;Belgin, Ezgi Eren;Aycik, Gul Asiye
    • Nuclear Engineering and Technology
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    • 제53권5호
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    • pp.1642-1651
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    • 2021
  • In this study, isophtalic neopentyl glycol polyester (NPG-PES) based composites with different loading ratios of pure tungsten metal (W), tungsten (VI) oxide (WO3), tungsten boron (WB) and tungsten carbide (WC) composites were prepared as alternative shielding materials for ionizing electromagnetic radiation (IEMR) shielding. Structural characterizations of the composites were done. Gamma spectrometric analysis of composites for 80-2000 keV energy range was performed and their usability as IEMR shielding was discussed. As a result, the produced composites showed a shielding performance of 60-100% of the lead (the most widely used IEMR shielding material) depending on the reinforcement material, reinforcement loading rate and experimental conditions. Thus, it was reported that produced composites could be an alternative to lead shieldings that have several disadvantages as toxic properties, difficulty of processing and inelasticity.

Investigation of Sweet and Sour Corrosion of Mild Steel in Oilfield Environment by Polarization, Impedance, XRD and SEM Studies

  • Paul, Subir;Kundu, Bikramjit
    • Corrosion Science and Technology
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    • 제17권5호
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    • pp.249-256
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    • 2018
  • Metallic structures in the oil and gas production undergo severe degradation due to sweet and sour corrosion caused by the presence of $CO_2$ and $H_2S$ in the fluid environment. The corrosion behavior of 304 austenitic stainless was investigated in the presence of varying concentrations of $CO_2$ or $H_2S$ and $CO_2+H_2S$ to understand the effect of the parameters either individually or in combination. Potentiodynamic polarization study revealed that a small amount of $CO_2$ aided in the formation of calcareous deposit of protective layer on passive film of 304 steel, while increase in $CO_2$ concentration ruptured the layer resulting in sweet corrosion. The presence of $S^{2-}$ damaged the passive and protective layer of the steel and higher levels increased the degradation rate. Electrochemical impedance studies revealed lower polarization resistance and impedance at higher concentration of $CO_2$ or $H_2S$, supporting the outcomes of polarization study. XRD analysis revealed different types of iron carbides and iron sulphides corresponding to sweet and sour corrosion as the corrosion products, respectively. SEM analysis revealed the presence of uniform, localized and sulphide cracking in sour corrosion and general corrosion with protective carbide layer amid for sweet corrosion.

Effect of atmospheric plasma versus conventional surface treatments on the adhesion capability between self-adhesive resin cement and titanium surface

  • Seker, Emre;Kilicarslan, Mehmet Ali;Deniz, Sule Tugba;Mumcu, Emre;Ozkan, Pelin
    • The Journal of Advanced Prosthodontics
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    • 제7권3호
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    • pp.249-256
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    • 2015
  • PURPOSE. The aim of this study was to evaluate the effects of atmospheric plasma (APL) versus conventional surface treatments on the adhesion of self-adhesive resin cement to Ti-6Al-4V alloy. MATERIALS AND METHODS. Sixty plates of machined titanium (Ti) discs were divided into five groups (n=12): 1) Untreated (CNT); 2) Sandblasted (SAB); 3) Tribochemically treated (ROC); 4) Tungsten CarbideBur (TCB); 5) APL treated (APL). SEM analysis and surface roughness (Ra) measurements were performed. Self-adhesive resin cement was bonded to the Ti surfaces and shear bond strength (SBS) tests, Ra and failure mode examinations were carried out. Data were analyzed by one-way analysis of variance and chi-squared test. RESULTS. The lowest SBS value was obtained with CNT and was significantly different from all other groups except for APL. The ROC showed the highest SBS and Ra values of all the groups. CONCLUSION. It was concluded that the effect of APL on SBS and Ra was not sufficient and it may not be a potential for promoting adhesion to titanium.

마이크로 압입시험기법의 응용을 통한 탄성체 고분자 소재의 역학적 특성화 및 계면 접합에너지 평가기법 연구 (Characterization of Elastic Modulus and Work of Adhesion in Elastomeric Polymer through Micro Instrumented Indentation Technique)

  • 이규제;강승균;강인근;권동일
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.1744-1748
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    • 2007
  • In this study, the Johnson-Kendall-Roberts (JKR) theory was combined with the instrumented indentation technique (IIT) to evaluate work of adhesion and modulus of elastomeric polymer. Indentation test was used to obtain the load-displacement data for contacts between Tungsten Carbide indenter and elastomeric polymer. And the JKR contact model, contrived to take viscoelastic effects of polymer into account, was applied to compensate the contact area and the elastic modulus which Hertzian contact model would underestimate and overestimate, respectively. Besides, we could obtain the thermodynamic work of adhesion by considering the surface energy in this contact model. In order to define the relation between JKR contact area and applied load without optical measuring of contact area, we used the relation between applied load and contact stiffness by examining the correlation between JKR contact area and stiffness through dimensional analysis with 14 kinds of elastomeric polymer. From this work, it could be demonstrated that the interfacial work of adhesion and elastic modulus of compliant polymer can be obtained from a simple instrumented indentation testing without area measurement, and provided as the main algorithm of compliant polymer characterization.

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Vibration and damping behaviors of symmetric layered functional graded sandwich beams

  • Demir, Ersin
    • Structural Engineering and Mechanics
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    • 제62권6호
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    • pp.771-780
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    • 2017
  • In this study, free vibration and damping behaviors of multilayered symmetric sandwich beams and single layered beams made of Functionally Graded Materials were investigated, experimentally and numerically. The beams were composed of Aluminum and Silicon Carbide powders and they were produced by powder metallurgy. Three beam models were used in the experiments. The first model was isotropic, homogeneous beams produced by using different mixing ratios. In the second model, the pure metal layers were taken in the middle of the beam and the weight fraction of the ceramic powder of each layer was increased towards to the surfaces of the beam in the thickness direction. In the third model, the pure metal layers were taken in the surfaces of the beam and the weight fraction of the ceramic powder of each layer was increased towards to middle of the beam. Then the vibration tests were performed. Consequently, the effects of stacking sequence and mixing ratio on the natural frequencies and damping responses of functionally graded beams were discussed from the results obtained. Furthermore, the results obtained from the tests were supported with a finite-element-based commercial program, and it was found to be in harmony.

보론을 포함한 고체 연료 연소와 사이클 해석 (Boron-Containing Solid Fuel Combustion and Cycle Analysis)

  • 이태호
    • 한국추진공학회지
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    • 제19권1호
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    • pp.18-24
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    • 2015
  • 흡입 공기 온도가 연소 효율에 미치는 효과를 조사하기 위하여, 보론 카바이드가 충전된 그레인을 사용하여 실험을 수행하였다. 시험 결과 무차원화한 연소 효율은, 보론 입자의 증가된 연소 결과로 흡입 공기 온도가 올라감에 따라 증가하였다. 연소 효율은 증가하고 있지만, 반-실험적 방법에 의한 전반적인 효율은 온도가 올라감에 따라 감소하고 있다. 열입력 매개 변수와 연소실 마하 수를 변수로 브레이튼 사이클을 적용하여 분석하였으며 이들 두 인자가 성능에 여향을 미치고 있고, 실험 결과에서도 같은 추세를 보였다.

11 wt% 크롬이 함유된 Ti 첨가 페라이트스테인리스강의 입계부식에 미치는 규소의 영향 (Effect of Silicon on Intergranular Corrosion Resistance of Ti-stabilized 11 wt% Cr Ferritic Stainless Steels)

  • 현영민;김희산
    • Corrosion Science and Technology
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    • 제12권6호
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    • pp.265-273
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    • 2013
  • Ti-stabilized 11 wt% Cr ferritic stainless steels (FSSs) for automotive exhaust systems have been experienced intergranular corrosion (IC) in some heat-affected zone (HAZ). The effects of sensitizing heat-treatment and silicon on IC were studied. Time-Temperature-Sensitization (TTS) curves showed that sensitization to IC was observed at the steels heat-treated at the temperature lower than $650^{\circ}C$ and that silicon improved IC resistance. The sensitization was explained by chromium depletion theory, where chromium is depleted by precipitation of chromium carbide during sensitizing heat-treatment. It was confirmed with the results from the analysis of precipitates as well as the thermodynamical prediction of stable phases. In addition, the role of silicon on IC was explained with the stabilization of grain boundary. In other words, silicon promoted the formation of the grain boundaries with low energy where precipitation was suppressed and consequently, the formation of Cr-depleted zone was retarded. The effect of silicon on the formation of grain boundaries with low energy was proved by the analysis of coincidence site lattice (CSL) grain boundary, which is a typical grain boundary with low energy.

롤러 기어 캠의 시제품 가공특성에 관한 연구 (A Study on the Machining Characteristics of Prototype of Roller Gear Cams)

  • 김진수;강성기;이동섭
    • 한국기계가공학회지
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    • 제11권5호
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    • pp.60-67
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    • 2012
  • In the study, the effect grinding condition on the workpiece arithmetical average roughness(Ra) to 10 steps leading to cutting each section with the spindle rotational speed 8000rpm and feed rate 150mm/min of grinding in GC(green silicon carbide) grinding processing after heat treatment and non heat treatment of SCM415 material. Also the following conclusions were obtained analysis of stress distribution displacement and finite elements method(FEM) on assemble parts with 3+2 axis simultaneous control through grinding and gave a load 11kg on ATC arm both sides gave a load of 11kg. For the centerline average roughness(Ra) in the heat and non-heat treatment work pieces, which were appeared the most favorable in the fifth section were $0.511{\mu}m$ and $0.514{\mu}m$, that were shown in the near the straight line section was the smallest deformation of curve. In addition, the bad surface roughness appeared on the path is too long by changing angle, the more inclined depth of cut, because the chip discharging is not smoothly.

마이크로 압입시험기법의 응용을 통한 탄성체 고분자 소재의 역학적 특성화 및 계면 접합에너지 평가기법 연구 (Mechanical Characterization of Elastomeric Polymer Through Micro Instrumented Indentation Technique)

  • 이규제;강승균;강인근;권동일
    • 대한기계학회논문집A
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    • 제31권9호
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    • pp.951-959
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    • 2007
  • In this study, the Johnson-Kendall-Roberts(JKR) theory was combined with the instrumented indentation technique (IIT) to evaluate work of adhesion and modulus of elastomeric polymer. Indentation test was used to obtain the load-displacement data for contacts between Tungsten Carbide indenter and elastomeric polymer. And the JKR contact model, contrived to take viscoelastic effects of polymer into account, was applied to compensate the contact area and the elastic modulus which Hertzian contact model would underestimate and overestimate, respectively. Besides, we could obtain the thermodynamic work of adhesion by considering the surface energy in this contact model. In order to define the relation between JKR contact area and applied load without optical measuring of contact area, we used the relation between applied load and contact stiffness by examining the correlation between JKR contact area and stiffness through dimensional analysis with 14 kinds of elastomeric polymer. From this work, it could be demonstrated that the interfacial work of adhesion and elastic modulus of compliant polymer can be obtained from a simple instrumented indentation testing without area measurement, and provided as the main algorithm of compliant polymer characterization.