• 제목/요약/키워드: bulk density

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유동성이 우수한 분체특성을 갖는 세파졸린 나트륨 진공동결건조 분말의 제조 (Preparation of Freeze-dried Cefazolin Sodium Bulk Powder with Good Flowability)

  • 조정식;정은주
    • 약학회지
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    • 제42권3호
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    • pp.284-289
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    • 1998
  • The effect of reaction condition, solvent addition and thermal treatment on the bulk density, crystallinity and chemical properties of the freeze-dried cefazohn sodium was inves tigated to prepare the cefazolin sodium powder for injection with good flowability. Crystalline cefazolin sodium powder with high untapped-bulk density (about 45%) and low compressibility (about 40%) was obtained by solvent addition to the very highly concentrated cefazohn sodium solution followed by subsequent thermal treatment before freeze-drying. The desirable solvent was low substituted alcohol such as isopropyl alcohol and anhydrous ethanol with the final concentration of about 9%. The pH adjustment and nitrogen gas purging during the reaction did not give significant effect on the chemical properties such as content, color, transmittance and pH of the reconstituted cefazolin sodium aqueous solution.

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우리나라 상토의 물리적 표준분석법 설정 연구 1. 입자밀도 및 용적밀도 (Development of Standard Analysis Methods for Physical Properties on Korean bedsoil 1. Particle density and Bulk density)

  • 김이열;조희기
    • 한국토양비료학회지
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    • 제35권6호
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    • pp.327-334
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    • 2002
  • 우리나라 유통상토에 대한 물리적 표준분석법을 설정하기 위한 연구를 실시하였다. 국내 시중에 유통되고 있는 53개 품목의 원예용 상토와 9개 품목의 수도용 상토를 대상으로 설정된 분석법을 적용하여 실험하였다. 입자밀도의 측정은 가스형 피크노메타 (Micromeritics Co. Model 1305)를 사용하면 속도와 정확성 면에서 매우 유리 하였다. 용적밀도는 구미에서 Sandbox법에 의한 용적밀도를 기본으로 하기 때문에 이와 유사한 성적을 얻을 수 있는 다양한 실험을 한 결과, 추다짐법 (Plunger compaction method)이 가장 유의성 있는 측정 방법으로 밝혀졌다. 한편 가스형 피크노메타법에 의한 우리나라 유통상토의 입자밀도는 원예용이 1.93, 수도용이 $2.43Mg\;m^{-3}$로 나타났으며, 추다짐법에 의한 용적밀도는 원예용이 0.22, 수도용이 $1.01Mg\;m^{-3}$로 각각 나타났다.

논 토양의 물리적 특성을 고려한 산물형 트레일러의 적정용량 예측 (Prediction of Bulk Type Trailer Capacity in Consideration of Soil Physical Properties of Paddy Field)

  • 박원엽;이규승
    • Journal of Biosystems Engineering
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    • 제28권1호
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    • pp.1-10
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    • 2003
  • A computer simulation was carried out to determinate the optimum capacity of bulk type trailer which is used as a tractor attachment. Soil physical properties. such as soil moisture content. bulk density, soil hardness and soil texture were measured in the 10 major rice production area for computer simulation. Mathematical model which include soil physical properties and vehicle factor was used for computer simulation. Most of the soil texture of the investigated area was silty loam. Soil moisture content ranged between 30 and 40% mostly. Soil bulk density was in the range of 1.500 to 1.700 kg/㎥. Soil hardness ranged between 1 to 18 kg/$\textrm{cm}^2$. Soil hardness incorporate the effects of many soil physical properties such as moisture content texture and bulk density, and so the range of soil hardness was greater than any other physical properties. The capacity of bulk type trailer was above 3000 kg$_{f}$ fer the most of the investigated area. and mostly in the range of 4000 to 6000 kg$_{f}$ depending upon the slip. But for the soft soil area such as Andong and Namyang. tractor itself had mobility problem and showed minus trailer capacity for some places. For this area. the capacity of bulk type trailer ranged between 1000 and 2000 kg$_{f}$ mostly so bulk type trailer should be designed as a small capacity compared to the other area.ared to the other area. area.

Density Functional Theory Calculations of Intercalated Lithium in MoS2 bulk

  • 심서현
    • EDISON SW 활용 경진대회 논문집
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    • 제3회(2014년)
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    • pp.459-463
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    • 2014
  • $MoS_2$ bulk에 Lithium을 intercalate했을 때 가장 안정한 위치와 그 위치에서의 결합에너지에 대한 분석을 진행하였다. 이를 위해 Density Functional Theory를 기반으로 한 계산을 실행하였으며 MoS2 bulk 내의 여러 위치에서의 에너지를 구하여 Li이 가장 안정하게 흡착되는 비율과 Li 원자가 안정한 흡착 위치를 계산했다. 그 결과 Li 원자가 1/4 monolayer을 형성할 때 가장 안정하며 그 때 Li 원자는 Hollow site에 결합한다는 결론을 얻었다.

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NiCuZn Ferrite의 제조공정 제어(제2보) - 성형압력 및 소성온도 변화에 따른 초기투자율과 겉보기밀도에 관한 고찰 (The Prodessing Control of NiCuZn Ferrite(II) - The Relationship between Initial Permeability and Bulk Density of NiCuZn Ferrite as Functions of Forming Pressure and Sintering Temperature.)

  • 류병환;김선희;최경숙;고재천
    • 한국자기학회지
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    • 제5권6호
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    • pp.937-946
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    • 1995
  • 본 연구에서는 NiCuZn Ferrite 제조공정의 제어를 위하여 제조공정 변수에 따른 NiCuZn Ferrite의 물성 및 자기적특성의 변화를 검토하여, 겉보기밀도(bulk density)와 초기투자율의 관계를 명확하게 하는 것을 목적으로 하였다. $700^{\circ}C$에서 3시간 하소 한 NiCuZn Ferrite를 약 60시간 볼밀링하여 약 $0.5\mu\textrm{m}$ 입자크기로 분쇄한 후 분무 건조하여 과립화하였다. 본 연구에서는 (1)NiCuZn Ferrite 과립의 크기와 성형압력 변화와 (2)일정한 성형조건에서 소성온도의 변화에 따른 성형체 및 소성체의 물성측정, 그리고 자기적 특성을 검토하였다. NiCuZn Ferrite의 green density는 과립의 크기보다는 성형압력에 더 의존하였으며, 과립의 크기가 $150\mu\textrm{m}$ 이하 일 때 성형압력이 증가 함에 따라 green density는 $2.484\;g/cm^{3}$에서 $3.002\;g/cm^{3}$로 크게 증가하 였다. NiCuZn Ferrite의 bulk density는 소성온도에 의하여 거의 직선적으로 $3.470\;g/cm^{3}$에서 $4.754\;g/cm^{3}$로 증가하였다. 성형압력 변화 및 소성온도 변화에 따른 NiCuZn Ferrite 초기투자율과 겉보기밀도 관계를 비교 검토한 결과, NiCuZn Ferrite의 초기투자율($\mu_{i}$)과 겉보기밀도($\rho$)의 관계를 $\mu_{i}=a+b_{\rho}+c_{\rho}^2$와 같이 실험식으로 표현할 수 있었다.

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The Fabrication of Artificial Fine Aggregates Using Stone Sludge and Spent Bleaching Clay

  • Kim, Kangduk
    • 한국세라믹학회지
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    • 제51권5호
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    • pp.492-497
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    • 2014
  • Artificial fine aggregates (denoted AFA) were fabricated using spent bleaching clay (denoted SBC) generated from processed vegetable oil and stone sludge (denoted SS) produced from crushed aggregate manufacturing materials for use as functional construction materials. Each raw material was crushed to particle size finer than $150{\mu}m$, and fine spherical pellets of approximately 1 ~ 4 mm in diameter were prepared by a pelletizing process. The physical properties of the AFA were measured with different types of sintering equipment. A new type of vertical furnace that sinters fine aggregates in a fluidized bed at high temperatures was designed and tested. AFA sintered in a rotary kiln at $1125^{\circ}C$ showed a bulk density of $1.5g/cm^3$ and a water absorption of 16%. AFA sintered in the vertical furnace at $1125^{\circ}C$ showed a bulk density of $1.9g/cm^3$ and water absorption of 8.5%. The bulk density of the AFA sintered in the vertical furnace showed a bulk density 27% higher and water absorption 47% lower than those of AFA sintered in the rotary kiln.

Effeet of Al2O3, MgO and SiO2 on Sintering and Hydration Behaviors of CaO Ceramics

  • Kim, Do-Kyung;Cho, Churl-Hee;Goo, Bong-Jin;Lee, Kee-Sung
    • 한국세라믹학회지
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    • 제39권6호
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    • pp.528-534
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    • 2002
  • CaO ceramics were prepared by conventional sintering process and their hydration behaviors were evaluated by measuring weight increment on saturated water vapor pressure at ambient temperature. CaCO$_3$ and limestone were used as CaO source materials and $Al_2$O$_3$, MgO and SiO$_2$ were added as sintering agents. $Al_2$O$_3$ was a liquid phase sintering agent to increase densification and grain growth rates, whereas MgO and SiO$_2$, densification and grain growth inhibitors. Regardless of composition, all of the prepared CaO ceramics showed the improved hydration resistance as bulk density increased. Especially, when bulk density was more than 3.0 g/㎤, there was no weight increment after 120 h of hydration. Therefore, to decrease contact area between CaO and water vapor by increasing bulk density with the $Al_2$O$_3$ sintering additive was effective for the improvement of CaO hydration resistance.

옥수수가루, 탈지 콩가루 및 오징어를 이용한 스낵제품의 물리화학적 특성연구 (Physical and Chemical Properties of Cornmeal Extrudates by Addition of Defatted Soy Flour and Squid)

  • 정복미;김은실;이기춘
    • 한국식품영양과학회지
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    • 제30권2호
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    • pp.292-298
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    • 2001
  • This study was conducted to investigate physicochemical properties of extrudates combining 4 levels of squid (0, 3, 5 and 7%) with 3 levels of defatted soy flour (0, 5, and 10%). Blends were adjusted to moisture content of 27% and then extruded in a single-screw laboratory extruder at 170rpm screw speed and 16$0^{\circ}C$ barrel temperature. The extruded materials were dried at 6$0^{\circ}C$ for 8hr to a moisture content of 3~4% and refrigerated at 4$^{\circ}C$ for 12 hour before examination for textural properties, expansion ratio, bulk density, shear force and Hunter color. Expansion ratio of extrudates decreased as squid content increased whereas bulk density and shear force increased. Expansion ratio of extrudates was not significantly different by defatted soyflour level. Bulk density of products decreased as defatted soyflour content increased but shear force of products increased as defatted soyflour content increased. In scores of sensory hedonic evaluation of snacks, appearance, flavor, texture and overall acceptability values had lowered as squid level increased. Therefore, according to materials contents on extrudates increased, nutritional contents of this products increased and also shear force and bulk density in physical properties increased whereas expansion ratio decreased.

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Interpretation of Physical Properties of Marine Sediments Using Multi­Sensor Core Logger (MSCL): Comparison with Discrete Samples

  • Kim, Gil-Young;Kim, Dae-Choul
    • Journal of the korean society of oceanography
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    • 제38권4호
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    • pp.166-172
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    • 2003
  • Multi­Sensor Core Logger (MSCL) is a useful system for logging the physical properties (compressional wave velocity, wet bulk density, fractional porosity, magnetic susceptibility and/or natural gamma radiation) of marine sediments through scanning of whole cores in a nondestructive fashion. But MSCL has a number of problems that can lead to spurious results depending on the various factors such as core slumping, gas expansion, mechanical stretching, and the thickness variation of core liner and sediment. For the verification of MSCL data, compressional wave velocity, wet bulk density, and porosity were measured on discrete samples by Hamilton Frame and Gravimetric method, respectively. Acoustic impedance was also calculated. Physical property data (velocity, wet bulk density, and impedance) logged by MSCL were slightly larger than those of discrete sample, and porosity is reverse. Average difference between MSCL and discrete sample at both sites is relatively small such as 22­24 m/s in velocity, $0.02­-0.08\;g/\textrm{cm}^3$ in wet bulk density, and 2.5­2.7% in porosity. The values also show systematic variation with sediment depth. A variety of factors are probably responsible for the differences including instrument error, various measurement method, sediment disturbance, and accuracy of calibration. Therefore, MSCL can be effectively used to collect physical property data with high resolution and quality, if the calibration is accurately completed.

신개간경사지 토양개량과 작물생육에 관한 연구 VI. 토양의 물리화학성 년차간 변화가 옥수수 청예수량에 미치는 영향 (The Soil Improvement and Plant Growth on the Newly-Reclaimed Sloped land VI. Relationship between annual change of soil phsico-chemical properties and yield of silage corn)

  • 허봉구;김무성
    • 한국초지조사료학회지
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    • 제11권1호
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    • pp.22-29
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    • 1991
  • This study was experimented to obtain the basic information on the changeable aspect and improvement of soil fertility in newly-reclaimed sloped land. Silage corn was cultivated under the six different treatments for 4 years. The relation between the amount or ratio of annual changes of soil physico-chemical properties and yield of silage corn were analyzed. Soil bulk density was decreased in 3rd year at topsoil, but that decreased in 4th year at subsoil. Soil organic matter also decreased in 2nd year at topsoil, and decreased continuously at subsoil. Bulk density and hardness of soil depths showed significant negative simple correlation with dry matter yield and cation exchange capacity showed positive. Correlation coefficient of chemical properties with dry matter yield were low. The range of annual changes of moisture percent, hardness and organic matter were wider than the other properties. The significantly different of physical properties were higher than the chemical properties, and those of topsoil were higher than subsoil. According to multiple regression between yield and physico-chemical properties of subsoil, bulk density and cation exchange capacity were in the greatest contribution at the variations, but bulk density was greatest at the ratios.

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